物理化学学报 >> 1992, Vol. 8 >> Issue (03): 293 -295 .doi: 10.3866/PKU.WHXB19920302

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原位X-射线衍射反应器的研制及应用

庞先杰; 钟前则; 贺仁近; 钟邦克   

  1. 暨南大学化学系,广州 510632
  • 收稿日期:1991-12-16 修回日期:1992-01-30 发布日期:1992-06-15
  • 通讯作者: 钟邦克

Study and Application of a Chamber Reactor with Simultaneous XRD

Pang Xian-Jie; Zhong Qian-Ze; He Ren-Jin; Zhong Bang-Ke   

  1. Chemistry Department, Jinan University, Guangzhou 516032
  • Received:1991-12-16 Revised:1992-01-30 Published:1992-06-15
  • Contact: Zhong Bang-Ke

关键词: 反应器, X-射线衍射,

Abstract: In this paper a chamber-reactor that makes it possible to investigate the kineties of catalytic reaction with simultaneous X-ray diffraction phase analysis of the catalyst during the reaction is described. Two samples, the phase trasformations of quartz powder during temperature variation and the reduction of CuO with H_2 were investigated by this chamber reactor. An analysis of XRD spectrum leads to the conclusion that use of a Beryllium window have some special advantages.

Key words: Reactor, XRD, Beryllium