物理化学学报 >> 1996, Vol. 12 >> Issue (11): 1049-1051.doi: 10.3866/PKU.WHXB19961120

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AIN纳米微粉的微波合成

戴长虹,张显鹏,张劲松,杨永进,曹丽华,夏非   

  1. 东北大学有色金属冶金系，沈阳 110006|中国科学院金属研究所，沈阳 110015
  • 收稿日期:1996-05-20 修回日期:1996-09-02 发布日期:1996-11-15
  • 通讯作者: 戴长虹

Microwave Synthesis of AIN Nanometer Powder

Dai Chang-Hong,Zhang Xian-Peng,Zhang Jin-Song,Yang Yong-Jin,Cao Li-Hua,Xia Fei   

  1. Northeastern University,Shenyang 110006|Institute of Metal Reserch,Chinese Academy of Sciences,Shenyang 110015
  • Received:1996-05-20 Revised:1996-09-02 Published:1996-11-15
  • Contact: Dai Chang-Hong

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关键词: AIN, 纳米微粉, 微波合成

Abstract:

Nanometer aluminum nitride powder with purity higher than 98wt% and diameter in the range of 5-80nm has been obtained by microwave heating using α-Al2O3、Al(OH)3、 colloidal Al(OH)3 as the source for aluminum, and phenolformaldehyde resin, char, nanometer carbon black powder as the source for carbon, respectively. The effect of the type of starting materials and synthesis conditions on the purity and the size of the nanometer AlN powder has been analyzed in this paper.

Key words: AIN, Nanometer powder, Microwave synthesis