物理化学学报 >> 1985, Vol. 1 >> Issue (03): 289-292.doi: 10.3866/PKU.WHXB19850314
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赵宝光; 林秀云; 叶蕴华
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Zhao Baoguang; Lin Xiuyun; Ye Yunhua
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Abstract: The crystal of tetrahydrothiazole-2-thione belongs to triongal system, space group R3c. There are six molecules in a unit cell with parameter a=b=1.5402(5), c=1.2528(19) nm, γ=120°. The three dimensional intensity data were obtained with PW-1100 four-circle diffractometer. 522 independent reflexions with I>1.3σ(I) were considered observed and used in structure analysis. The structure was solved by direct method(RANTAN) and refined by full matrix least-squares method, the final R=0.049, R_w=0.044. The crystal structure of tetrahydrothiazole-2-thione copper complex shows that Cu is four coordinated and has nearly tetrahedron configuration.
赵宝光;林秀云;叶蕴华. 四氢噻唑-2-硫酮铜络合物的晶体结构与分子结构[J]. 物理化学学报, 1985, 1(03): 289-292.
Zhao Baoguang; Lin Xiuyun; Ye Yunhua. THE CRYSTAL AND MOLECULAR STRUCTURE OF TETRAHYDROTHIAZOLE-2-THIONE COPPER COMPLEX[J]. Acta Phys. -Chim. Sin., 1985, 1(03): 289-292.
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