物理化学学报 >> 1992, Vol. 8 >> Issue (02): 266-269.doi: 10.3866/PKU.WHXB19920225

研究简报 上一篇    下一篇

微型拉曼电解池现场研究硫酰氯的电化学还原

钟发平; 杨汉西; 徐知三; 查全性   

  1. 武汉大学化学系,武汉 430072
  • 收稿日期:1990-11-02 修回日期:1991-05-06 发布日期:1992-04-15
  • 通讯作者: 杨汉西

In-Situ Raman Spectroscopic Investigation of the SO2Cl2 Electroreduction Using Micro-Raman Electrolytic Cell

Zhong Fa-Ping; Yang Han-Xi; Xu Zhi-San; Zha Quan-Xing   

  1. Department of Chemistry, Wuhan University, Wuhan 430072
  • Received:1990-11-02 Revised:1991-05-06 Published:1992-04-15
  • Contact: Yang Han-Xi

关键词: 硫酰氯, 电还原, 微型拉曼电解池, 现场研究

Abstract: A micro-Raman electrochemical cell was designed for in-situ study of the elec-troreduction of SO_2Cl_2. This type of microcell has advantages of low sample volume, easy manipulation and experimental safety. Therefore, it can be used conveniently for in-situ spectroscopic investigation of strongly oxidative and hazardous Li-liquid cathode electrochemical systems.

Key words: Sulfuryl chloride, Electroreduction, Micro-Raman electrolytic cell, In-situ Raman spectroscopic investigation