物理化学学报 >> 1993, Vol. 9 >> Issue (01): 5-7.doi: 10.3866/PKU.WHXB19930102

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粒度均匀镍-磷非晶超细微粒催化剂的制备与表征

胡征; 范以宁; 陈懿; 姜欣华   

  1. 南京大学化学系，南京 210008；江苏省地矿局测试应用研究所，南京 210018
  • 收稿日期:1992-08-17 修回日期:1992-09-26 发布日期:1993-02-15
  • 通讯作者: 胡征

Preparation and Characterization of Ni-P Ultrafine Catalyst Particles with Narrow Size Distribution

Hu Zheng; Fan Yi-Ning; Chen Yi; Jiang Xin-Hua   

  1. Department of Chemistry, Nanjing University, Nanjing 210008; Applied Institute for Analysis of Geological and Mineral Products of Jiangsu Province, Nanjign 210018
  • Received:1992-08-17 Revised:1992-09-26 Published:1993-02-15
  • Contact: Hu Zheng

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关键词: 非晶, 超细微粒催化剂, 均匀

Abstract: This note reports a successful preparation of a new catalyst particles through the reaction between Ni~(2+) and H_2PO_2~- in aqueoud solution at room temperature. X-ray diffraction pattern indicates that the particles are in amorphous and alloying state. Transmission electron micrograph shows that the particles are spherical and the size distribution is very narrow. The average diameter of the particles is determined to be about 100 nm which is in“ultrafine”scale.

Key words: Amorphous, Ultrafine particle catalyst, Narrow size distribution