物理化学学报 >> 1994, Vol. 10 >> Issue (02): 100-102.doi: 10.3866/PKU.WHXB19940202

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高层间距氧化铝柱层状钛酸盐的制备和表征

侯文华, 颜其洁, 傅献彩   

  1. 南京大学化学系，南京 210008
  • 收稿日期:1993-10-12 修回日期:1993-11-11 发布日期:1994-02-15
  • 通讯作者: 侯文华

Preparation and Characterization of Alumina-pillared Layered Titanate with a High Interlayer Spacing

Hou Wen-Hua, Yan Qi-Jie, Fu Xian-Cai   

  1. Department of Chemistry, Nanjing University, Nanjing 210008
  • Received:1993-10-12 Revised:1993-11-11 Published:1994-02-15
  • Contact: Hou Wen-Hua

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关键词: 高层间距, 氧化铝柱层状钛酸盐, 制备和表征

Abstract:

This note mainly reports a successful preparation of a alumina-pillared layered titanate with a high interlayer spacing through a step-wise exchange process. X-ray diffeaction patterns indicate that the resultant alumina-pillared layered titanate has an interlayer spacing of 1.70 nm, which is 0.17 nm higher than that of previously reported,and has a thermal stability over 500 ℃. The surface area (N2, BET method) of the product is determined to be 72.4 m2·g-1. The N2 adsorption and desorption isotherm of the product demonstrates that the resultant alumina-pillared layered titanate is porous, with both micropores and mesopores.

Key words: High interlayer spacing, Alumina-pillared Iayered titanate, Preparation and characterization