物理化学学报 >> 2003, Vol. 19 >> Issue (03): 265-267.doi: 10.3866/PKU.WHXB20030317

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直流电沉积Ni-Al2O3纳米阵列体系结构与性能

徐金霞;黄新民;钱利华   

  1. 合肥工业大学材料学院,合肥　230009
  • 收稿日期:2002-06-14 修回日期:2002-09-12 发布日期:2003-03-15
  • 通讯作者: 黄新民 E-mail:xmhuang@mail.hf.ah.cn

Structure and Properties of Ni-Al2O3 Nanochannel Array System by Direct Current Electro-deposition

Xu Jin-Xia;Huang Xin-Min;Qian Li-Hua   

  1. Department of Materials Science and Engineering, Hefei University of Technology, Hefei　230009
  • Received:2002-06-14 Revised:2002-09-12 Published:2003-03-15
  • Contact: Huang Xin-Min E-mail:xmhuang@mail.hf.ah.cn

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摘要： 用直流电沉积的方法成功地将Ni金属填入了用二次腐蚀方法制备的氧化铝模板纳米级孔洞中，分别用电子显微镜、X射线衍射仪和振动样品磁强计对Ni阵列体系进行结构观察和磁性表征.结果表明，用二次腐蚀方法制得的多孔氧化铝模板的孔洞排布的有序性很高.被组装的Ni呈单晶结构并具有一定的择优取向； Ni-Al2O3阵列体系有明显的垂直磁各向异性，适用于垂直磁记录介质.

关键词: 纳米材料, 直流电沉积, 氧化铝模板, 垂直磁记录

Abstract: Direct current electro-deposition was applied to add Nickel to the nano-scale holes of porous Alumina template prepared by two-step anodic oxidation. The structure and magnetic performance of Ni-Al2O3 array system were investigated by electron microscope, X-Ray and vibration sample magnetometer. The results indicated that the regularity of the holes’ arrangement in the porous Alumina membrane by two-step anodic oxidation was obviously better than that by one-step anodic oxidation. Nickel was in single crystal state in the nanochannal array system and had definite crystall selective-orientation. The array had obvious magnetic anisotropy, and was promising for perpendicular magnetic recording medium.

Key words: Nano-materials, Direct current electro-deposition, Alumina template, 　Perpendicular magnetic recording