物理化学学报 >> 1993, Vol. 9 >> Issue (06): 815-818.doi: 10.3866/PKU.WHXB19930617

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均分散胶体的研究 V. 锆化合物均分散颗粒的制备

王光信; 孙浩贤; 侯耀永; 陈宗淇   

  1. 青岛化工学院应用化学系，青岛 266042
  • 收稿日期:1992-04-20 修回日期:1992-07-14 发布日期:1993-12-15
  • 通讯作者: 王光信

Study on Monodispersed Colloid V. Preparation of Monodispersed Particles of Zirconium Compounds

Wang Guang-Xin; Sun Hao-Xian; Hou Yao-Yong; Chen Zong-Qi   

  1. Department of Applied Chemistry, Qingdao Institute of Chemical Technology, Qingdao 266042
  • Received:1992-04-20 Revised:1992-07-14 Published:1993-12-15
  • Contact: Wang Guang-Xin

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关键词: 均分散颗粒, 碱式碳酸锆, 氯化锆

Abstract: This paper describes the preparation of monodispersed sol of zirconium basic carbonate consisting of particles with diameter less than 0.6 μm by aging Zr(Ⅳ) solution at elevated temperature in the presence of urea and glycerol. The composition of the monodispersed particles has primarily been determined by the IR spectra and the weight-loss of the particles on calcination. The monodispersed particles of ZrO_2 were obtained by calcination of the monodispersed particles separated from the sol at 850 ℃ for 2 h.

Key words: Monodispersed colloid, Zirconium basic carbonate, Zirconium oxide