原位X-射线衍射反应器的研制及应用

doi:10.3866/PKU.WHXB19920302

Acta Phys. -Chim. Sin. ›› 1992, Vol. 8 ›› Issue (03): 293-295.doi: 10.3866/PKU.WHXB19920302

• Communication • Previous Articles Next Articles

Study and Application of a Chamber Reactor with Simultaneous XRD

Pang Xian-Jie; Zhong Qian-Ze; He Ren-Jin; Zhong Bang-Ke

Chemistry Department, Jinan University, Guangzhou 516032

Received:1991-12-16 Revised:1992-01-30 Published:1992-06-15
Contact: Zhong Bang-Ke

Abstract

Abstract: In this paper a chamber-reactor that makes it possible to investigate the kineties of catalytic reaction with simultaneous X-ray diffraction phase analysis of the catalyst during the reaction is described. Two samples, the phase trasformations of quartz powder during temperature variation and the reduction of CuO with H_2 were investigated by this chamber reactor. An analysis of XRD spectrum leads to the conclusion that use of a Beryllium window have some special advantages.

Key words: Reactor, XRD, Beryllium

Pang Xian-Jie; Zhong Qian-Ze; He Ren-Jin; Zhong Bang-Ke. Study and Application of a Chamber Reactor with Simultaneous XRD[J].Acta Phys. -Chim. Sin., 1992, 8(03): 293-295.

[1]	Qingguo Meng, Changling Liu, Chengfeng Li, Xiluo Hao, Gaowei Hu, Jianye Sun, Nengyou Wu. Effect of Common Guest Molecules on the Lattice Constants of Clathrate Hydrates [J]. Acta Physico-Chimica Sinica, 2020, 36(11): 1910010-.
[2]	Xinjie Luo, Xi Zhang, Yujun Feng. Liquid Marbles: Fabrication, Physical Properties, and Applications [J]. Acta Physico-Chimica Sinica, 2020, 36(10): 1910007-.
[3]	Zhenjie CHENG, Yayun MAO, Qingyu DONG, Feng JIN, Yanbin SHEN, Liwei CHEN. Fluoroethylene Carbonate as an Additive for Sodium-Ion Batteries: Effect on the Sodium Cathode [J]. Acta Physico-Chimica Sinica, 2019, 35(8): 868-875.
[4]	Wen-Jie. TIAN,Hong. WANG,Zhen. YIN,Ying. YANG,Jian-Xin. LI. Preparation of Nano-Manganite Loaded Titanium Electocatalytic Membrane for the Catalytic Oxidation of Benzyl Alcohol [J]. Acta Phys. -Chim. Sin., 2015, 31(8): 1567-1574.
[5]	WANG Wei-Gang, LI Kun, ZHOU Li, GE Mao-Fa, HOU Si-Qi, TONG Sheng-Rui, MU Yu-Jing, JIA Long. Evaluation and Application of Dual-Reactor Chamber for Studying Atmospheric Oxidation Processes and Mechanisms [J]. Acta Phys. -Chim. Sin., 2015, 31(7): 1251-1259.
[6]	ZHOU Han-Yang, YU Tian-Lin, AO Yin-Yong, PENG Jing, ZHAI Mao-Lin. Crystal Structure and Radiation Stability of Sr(NO₃)₂·DCH18C6 Complex [J]. Acta Phys. -Chim. Sin., 2014, 30(8): 1581-1586.
[7]	LUO Xiao-Lin, YANG De-Suo, YUAN Chun-Lan, LUO Xu-Mei, CHEN Ya-Shao. Catalytic Performance of Polycrystalline Cu₂O with Different Structures on the Thermal Decomposition of Ammonium Perchlorate [J]. Acta Phys. -Chim. Sin., 2014, 30(3): 520-526.
[8]	ZUO Yi, SONG Wan-Cang, WANG Meng-Li, XU Yong-Hai, WANG Xiang-Sheng, GUO Xin-Wen. Epoxidation of Propylene over Small-Crystal TS-1 Extrudate in a Fixed-Bed Reactor [J]. Acta Phys. -Chim. Sin., 2013, 29(01): 183-190.
[9]	YANG Zhi-Bin, DING Wei-Zhong. Reaction Pathway for Reforming Coke Oven Gas over NiO/MgO Catalyst in an Oxygen Permeation Membrane Reactor [J]. Acta Phys. -Chim. Sin., 2012, 28(04): 935-941.
[10]	SHAO Ju-Xiang, TAN Ning-Xin, LIU Wei-Xiong, LI Xiang-Yuan. Influence of H₂O and CO₂ in Air on the Combustion of Ethylene (II)——Reaction Mechanismand Kinetics Simulation [J]. Acta Phys. -Chim. Sin., 2010, 26(02): 270-276.
[11]	YANG Zhi-Bin, ZHANG Yu-Wen, ZHANG Yun-Yan, DING Wei-Zhong, SHEN Pei-Jun, LIU Yong, ZHOU Yu-Ding, HUANG Shao-Qing. Hydrogen Production fromCoke Oven Gas byMethane Reforming: Thermodynamic Analysis and Experimental Study [J]. Acta Phys. -Chim. Sin., 2010, 26(02): 350-358.
[12]	YANG Jiu-Long, LI Jian-Feng, LU Yong. Nitration of Benzene in a Continuous-Flow Microreactor Integrated with Microfiber-Structured Nafion/SiO₂ Solid Acid Catalyst [J]. Acta Phys. -Chim. Sin., 2009, 25(10): 2045-2049.
[13]	LI Jun, FENG Jie, LI Wen-Ying, CHANG Hai-Zhou, XIE Ke-Chang. Determining Influences of the Aggregative State of Deoxidized Coal on Its Extraction by Molecular Mechanics and Molecular Dynamics Analysis [J]. Acta Phys. -Chim. Sin., 2008, 24(12): 2297-2303.
[14]	XIAO Li-Hua, SUN Kun-Peng, XU Xian-Lun. Catalytic Combustion of Methane over CeO₂-MO_x (M=La³⁺, Ca²⁺) Solid Solution Promoted Pd/γ-Al₂O₃ Catalysts [J]. Acta Phys. -Chim. Sin., 2008, 24(11): 2108-2113.
[15]	LI Yuan-Pu; JIANG Xin. Influence of Interphase Distribution of Reactants on Preparation of Nano-CuO by Adsorption Phase Technique [J]. Acta Phys. -Chim. Sin., 2008, 24(03): 465-470.

Study and Application of a Chamber Reactor with Simultaneous XRD

PDF

Like

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Metrics

Recommended 0