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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2008,Vol.24>> Issue(11)>> 2019-2024     doi: 10.1016/S1872-1508(08)60079-0         中文摘要
Characterization of Visible Light Response N-F Codoped TiO2 Photocatalyst Prepared by Acid Catalyzed Hydrolysis
LI Xiao-Hui, LIU Shou-Xin
College of Material Science and Engineering, Northeast Forestry University, Harbin 150040, P. R. China
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N-FcodopedTiO2 (TONF) photocatalystswere prepared usingacidcatalyzed hydrolysismethod frommixed aqueous solution of TiCl4 and NH4F. The photocatalytic activity of the TONF was evaluated through the degradation of phenol under both visible and UVlight irradiation. X-ray photoelectron spectroscopy (XPS), UV-Vis diffuse reflectance spectroscopy (DRS), X-ray diffraction (XRD), scanning electron microscope (SEM), and N2 adsorption isotherm were used to characterize the obtained powders. The results showed that N-F co-doped TiO2 exhibited significant improvement of visible light catalytic activity. N-F co-doping could improve dispersion of TiO2, inhibit particle size agglomeration, and retard phase transformation. Doped N could extend the light response of TiO2 to visible light region. In addition, narrower band gap formed by F-doping was beneficial to the high visible light photocatalytic activity.

Keywords: TiO2   N-F codoping   Visible light   Photocatalyst  
Received: 2008-05-14 Accepted: 2008-07-03 Publication Date (Web): 2008-08-25
Corresponding Authors: LIU Shou-Xin Email: liushouxin@126.com


Cite this article: LI Xiao-Hui, LIU Shou-Xin. Characterization of Visible Light Response N-F Codoped TiO2 Photocatalyst Prepared by Acid Catalyzed Hydrolysis[J]. Acta Phys. -Chim. Sin., 2008,24 (11): 2019-2024.    doi: 10.1016/S1872-1508(08)60079-0
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91. YIN Yu-Xin; JIN Zheng-Guo; TAN Xin; HOU Feng; ZHAO Lin.Effect of Anions on the Electrochemical Formation of TiO2 Nanotube Arrays in a Glycerol Based Electrolyte[J]. Acta Phys. -Chim. Sin., 2008,24(11): 2133-2138
92. YAO Hui-Jun; MO Dan; DUAN Jing-Lai; CHEN Yan-Feng; ZHANG Ling; LIU Jie; HOU Ming-Dong; SUN You-Mei.Preparation and Optical Properties of Gold Nanowire Arrays[J]. Acta Phys. -Chim. Sin., 2008,24(10): 1922-1926
93. WANG Wei-Cheng, LI Shuo, WEN Yi-Yun, GONG Mao-Chu, ZHANG Lei, YAO Yan-Ling, CHEN Yao-Qiang.Synthesis and Characterization of TiO2/YFeO3 and Its Photocatalytic Oxidation of Gaseous Benzene[J]. Acta Phys. -Chim. Sin., 2008,24(10): 1761-1766
94. YU Jun, WU Gui-Sheng, MAO Dong-Sen, LU Guan-Zhong.Effect of La2O3 on Catalytic Performance of Au/TiO2 for CO Oxidation[J]. Acta Phys. -Chim. Sin., 2008,24(10): 1751-1755
95. CHEN Yu-Juan; HU Zhong-Hua; WANG Xiao-Jing; ZHAO Guo-Hua; LIU Ya-Fei; LIU Wei.Influence of Pore Size and Surface Area of Activated Carbon on the Performance of TiO2/AC Photocatalyst[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1589-1596
96. SUN Yi; XU Juan; CAI Wen-Bin; JIANG Zhi-Yu.Mechanism of Photokilling LoVo Cells by Nano TiO2 Photocatalytic Oxidation Combined with Immunity and Electroporation Method[J]. Acta Phys. -Chim. Sin., 2008,24(08): 1359-1365
97. SHI Jian; LI Jun; CAI Yun-Fa.Fabrication of C, N-Codoped TiO2 Nanotube Photocatalysts with Visible Light Response[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1283-1286
98. LIN Tao; ZHANG Qiu-Lin; LI Wei; GONG Mao-Chu; XING Yi-Xun; CHEN Yao-Qiang.Monolith Manganese-Based Catalyst Supported on ZrO2-TiO2 for NH3-SCR Reaction at Low Temperature[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1127-1131
99. PAN Hai-Bo; WANG Fang; HUANG Jin-Ling; CHEN Nai-Sheng.Binding Characteristics of CoPc/SnO2 by In-situ Process and Photocatalytic Activity under Visible Light Irradiation[J]. Acta Phys. -Chim. Sin., 2008,24(06): 992-996
100. TANG Yu-Xin; TAO Jie; TAO Hai-Jun; WU Tao; WANG Ling; ZHANG Yan-Yan; LI Zhuan-Li; TIAN Xi-Lin.Fabrication and Characterization for Transparent Electrodes of TiO2 Nanotube Arrays on Fluorine-Doped Tin Oxide-Coated Glass[J]. Acta Phys. -Chim. Sin., 2008,24(06): 1120-1126
101. WANG Ting; JIANG Xin; WU Yan-Xiang.Crystallization of Nano TiO2 Prepared by Adsorption Phase Reaction Technique and Photo-degradation of Gaseous Toluene[J]. Acta Phys. -Chim. Sin., 2008,24(05): 817-822
102. FENG Cai-Xia; WANG Yan; JIN Zhen-Sheng; ZHANG Shun-Li.Kinetic Behavior of Visible Light Photocatalytic Oxidation of Propylene for N-Doped Nano-TiO2[J]. Acta Phys. -Chim. Sin., 2008,24(04): 633-638
103. LU Han-Feng; ZHOU Ying; XU Bo-Qing; CHEN Yin-Fei; LIU Hua-Zhang.Effect of Gold Doping on the Photocatalytic Activity of the Anatase TiO2[J]. Acta Phys. -Chim. Sin., 2008,24(03): 459-464
104. LIU Shou-Xin; CHEN Xiao-Yun.Effect of Pore Structure of Activated Carbon on the Photocatalytic Activity of TiO2/AC Composite Photocatalyst[J]. Acta Phys. -Chim. Sin., 2008,24(03): 533-538
105. LIN Tao; LI Wei; GONG Mao-Chu; YU Yao; DU Bo; CHEN Yao-Qiang.Prepareration of ZrO2-TiO2-CeO2 and Its Application in the Selective Catalytic Reduction of NO with NH3[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1851-1856
106. LI Jing; YUN Hong; LIN Chang-Jian.The Fe-doped TiO2 Nanotube Arrays as a Photoanode for Cathodic Protection of Stainless Steel[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1886-1892
107. LIU Fu-Sheng; JI Ren; WU Min; SUN Yue-Ming.Hydrogen Production from Water Splitting Using Perylene Dye-Sensitized Pt/TiO2 Photocatalyst[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1899-1904
108. MAN Yi; ZONG Rui-Long; ZHU Yong-Fa.Preparation and Photoelectrochemical Properties of Bi2MoO6 Films[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1671-1676
109. YIN Yu-Xin; JIN Zheng-Guo; HOU Feng.Fabrication and Properties of TiO2 Nanotube Arrays Using Glycerol-DMSO-H2O Electrolyte[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1797-1802
110. ZHANG Tian-Yong; FAN Qiao-Fang; ZENG Miao; WANG Zheng; XIA Wen-Juan; CHI Li-Feng.Photocatalytic Degradation of Light Fast Scarlet BBN and Surfactant Bicomponents[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1803-1807
111. ZHANG Wei; WANG Shu-Liang; MA Yun-Qing; WANG Cui-Ping; LIU Xing-Jun.Influence of Interface Diffusion between Al Substrate and TiO2 Filmon Photocatalytic Activity[J]. Acta Phys. -Chim. Sin., 2007,23(09): 1347-1352
112. WANG Ting; JIANG Xin; LI Xi.Preparation of TiO2 Nanoparticles on Surface of Different Supports by Adsorption Phase Reaction Technique[J]. Acta Phys. -Chim. Sin., 2007,23(09): 1375-1380
113. WU Liang-Zhuan; ZHI Jin-Fang.One-step Synthesis of Anatase-Crystalline Titania Hollow Spheres in Aqueous Solution[J]. Acta Phys. -Chim. Sin., 2007,23(08): 1173-1177
114. LI Jing-Yi; MA Jun-Hua; BAI Tu-Ya; SUYOU Le-Ma.Effect of Fluoride Ion on the Photocatalytic Degradation of Sulforhodamine B on TiO2/Bentonite[J]. Acta Phys. -Chim. Sin., 2007,23(08): 1213-1218
115. TIAN Bao-Zhu; TONG Tian-Zhong; CHEN Feng; ZHANG Jin-Long.Effect of Water Washing Treatment on the Photocatalytic Activity of Au/TiO2 Catalysts[J]. Acta Phys. -Chim. Sin., 2007,23(07): 978-982
116. ZHAO Meng; WANG Jin-Xing; FENG Cai-Hui; ZOU Bo; CHEN Cheng; WANG Zhu-Yi; WU Feng-Qing; ZOU Le-Hui.Preparation and Gas Sensing Properties to Formaldehyde of TiO2/Ag2O Nanocrystalline[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1003-1006
117. ZHANG Xia; ZHAO Yan; ZHANG Cai-Bei; MENG Hao.Synthesis and Characterization of TiO2 Nano-crystalline with Different Morphologies by Low-temperature Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2007,23(06): 856-860
118. TAI Hui-Ling; JIANG Ya-Dong; XIE Guang-Zhong; DU Xiao-Song; CHEN Xuan.Preparation and Gas Sensitive Properties of Polyaniline/Titanium Oxide Composite Thin Films[J]. Acta Phys. -Chim. Sin., 2007,23(06): 883-888
119. LI Wei; PAN Gang; CHEN Hao; ZHANG Mei-Yi; HE Guang-Zhi; LI Jin; YANG Yu-Huan.Temperature Effects on Adsorption-Desorption Irreversibility of Zn(II) onto Anatase[J]. Acta Phys. -Chim. Sin., 2007,23(06): 807-812
120. LI Hong-Jian; CHEN Gang; LI Zhong-Hua; ZHOU Chao.Synthesis and Photocatalytic Decomposition of Water under Visible Light Irradiation of La2Ti2-xCoxO7 with Pyrochlore Structure[J]. Acta Phys. -Chim. Sin., 2007,23(05): 761-764
121. WU Lun-Peng; ZHAO Lian-Hua; ZHANG Hai-Ming; ZHAO Qing-Nan.Effects of the Adsorption of Oxygen on the Photocatalytic Activity of TiO2 Films Using PhotocurrentMethod[J]. Acta Phys. -Chim. Sin., 2007,23(05): 765-768
122. CHEN Xiao-Yun; LIU Shou-Xin.Preparation and Characterization of S-doped Ti1-xSyO2 Photocatalyst withWide Range Light Response[J]. Acta Phys. -Chim. Sin., 2007,23(05): 701-708
123. FANG Shu-Mei; OU Yan; LIN Jing-Dong; LIAO Dai-Wei.Preparation of Cu/Sr3Ti2O7 and Its Photocatalytic Activity of Watersplitting for Hydrogen Evolution[J]. Acta Phys. -Chim. Sin., 2007,23(04): 601-604
124. TIAN Meng-Kui; JIANG Li; SHANGGUAN Wen-Feng; WANG Shi-Jie2;OUYANG Zi-Yuan.Electronic Structures of the Visible-light Driven Photocatalysts K4Ce2Ta10O30, K4Ce2Nb10O30 and Their Solid Solution Compounds[J]. Acta Phys. -Chim. Sin., 2007,23(04): 466-472
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126. YAO Wei;WU Bao-Yan;GAO Li-Hua;WANG Ke-Zhi .DNA-Binding Studies of a Fluorenyl-Containing Ru(II) Complex[J]. Acta Phys. -Chim. Sin., 2007,23(02): 237-241
127. LI Jing-Yi;SIQIN Gao-Wa;LIU Li-Na.Photocatalytic Degradation of Organic Pollutants on TiO2/Bentonite[J]. Acta Phys. -Chim. Sin., 2007,23(01): 16-20
128. SHI Qiu-Jie;LEI Jing-Xin;ZHANG Ning.Modification of Ni-B/TiO2-Al2O3(S) Amorphous Alloy Catalyst by Mo for Liquid-phase Furfural Hydrogenation[J]. Acta Phys. -Chim. Sin., 2007,23(01): 98-102
129. ZHANG Shi-Cheng;YAO Wen-Qing;ZHU Yong-Fa;SHI Li-Yi.Preparation and Photoelectrochemical Properties of Bi2WO6 Films with Visible Light Response[J]. Acta Phys. -Chim. Sin., 2007,23(01): 111-115
130. CHU Dao-Bao;YIN Xiao-Juan;FENG De-Xiang;LIN Hua-Shui;TIAN Zhao-Wu.Electrocatalytic Oxidation of Ethanol on Pt/nanoTiO2-CNT Complex Catalysts[J]. Acta Phys. -Chim. Sin., 2006,22(10): 1238-1242
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133. YANG Ying;GONG Chu-Qing;XIAO Si;GONG Hong-Mei;WANG Qu-Quan;ZHONG Jia-Cheng.Influences of Titania Concentration on the Structure and the Three-order Nonlinear Optical Properties of Core-shell Ag/TiO2 Nanocomposites[J]. Acta Phys. -Chim. Sin., 2006,22(07): 791-796
134. ZHANG Ai-Ping;FANG Yan.The Effect of Anions on Silver Colloids Aggregation[J]. Acta Phys. -Chim. Sin., 2006,22(06): 756-760
135. ZHOU Li-Jun;YAN Shan-Shan;TIAN Bao-Zhu;CHEN Feng;ZHANG Jin-Long;HUANG Jia-Zhen.Preparation and Characterization of Anatase-Brookite TiO2 Film on the PET Surface[J]. Acta Phys. -Chim. Sin., 2006,22(05): 569-573
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142. PENG Feng; CHEN Shui-hui; ZHANG Lei; WANG Hong-juan; XIE Zhi-yong.Preparation of Visible-light Response Nano-sized ZnO Film and Its Photocatalytic Degradation to Methyl Orange[J]. Acta Phys. -Chim. Sin., 2005,21(08): 944-948
143. Chen Feng; Zhu Yi-Ping; Ma Hong-Liao; Bo Zi-Long; Zhang Jin-Long.Preparation and Characterization of TiO2--CdS-MCM-41 Nano-composite[J]. Acta Phys. -Chim. Sin., 2004,20(11): 1292-1296
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145. Zhang Jin-Long;Zhao Wen-Juan;Chen Hai-Jun;Xu Hua-Sheng;Chen Ai-Ping;Anpo Masa-Kazu.Study of Loaded Photocatalysts by Precious Metals on the Photocatalytic Reactivity[J]. Acta Phys. -Chim. Sin., 2004,20(04): 424-427
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