ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2007,Vol.23>> Issue(06)>> 877-882     doi: 10.3866/PKU.WHXB20070616         中文摘要
Capacitance Properties of Porous Polypyrrole Thick Films Prepared Electrochemically by Multi-step Polymerization
WANG Jie; XU You-Long; SUN Xiao-Fei; XIAO Fang; MAO Sheng-Chun

School of Electronic and Information Engineering, Xi’an Jiaotong University, Xi’an 710049, P. R. China

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To obtain polypyrrole (PPy) films with high area specific capacitance as electrode material for supercapacitors, the multi-step polymerization method was proposed for preparing PPy thick films with polymerization charge of 8, 10, and 12 mAh·cm-2, doped with Cl- and p-toluenesulfonate (TOS-), respectively. The capacitance properties of the PPy films were investigated by galvanostatic charge/discharge, cyclic voltammetry (CV), and electrochemical impedance spectrum (EIS) technologies. The section morphology of the PPy films was observed by using field emission electron scanning microscope (SEM). The results showed that two kinds of even porous PPy films with area specific capacitance up to 5 F·cm-2 could be obtained by multi-step method. Moreover, the mass specific capacitance (referring to the masses of polymer and doping ions) of PPy-Cl could reach 330 F·g-1, and the value of PPy-TOS could reach 191 F·g-1, which were similar with that of PPy thin films. However, the discharge rate of the PPy-TOS film was more rapid than that of the PPy-Cl film. In addition, the growth processes of PPy films from one-step
polymerization method and multi-step polymerization method were discussed.

Keywords: Polypyrrole   Supercapacitors   Capacitance   Morphology   Porous  
Received: 2006-12-29 Accepted: 2007-02-07 Publication Date (Web): 2007-04-28
Corresponding Authors: XU You-Long Email:

Cite this article: WANG Jie; XU You-Long; SUN Xiao-Fei; XIAO Fang; MAO Sheng-Chun. Capacitance Properties of Porous Polypyrrole Thick Films Prepared Electrochemically by Multi-step Polymerization[J]. Acta Phys. -Chim. Sin., 2007,23 (06): 877-882.    doi: 10.3866/PKU.WHXB20070616
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92. GUO Pei-Zhi, JI Qian-Qian, ZHANG Li-Li, ZHAO Shan-Yu, ZHAO Xiu-Song.Preparation and Characterization of Peanut Shell-Based Microporous Carbons as Electrode Materials for Supercapacitors[J]. Acta Phys. -Chim. Sin., 2011,27(12): 2836-2840
93. OUYANG Jing, SONG Xing-Lin, LIN Ming-Yue, ZOU Ju, LI Jing-Jing, ZHU Jiang-Ping, YANG Hua-Ming.Effect of Oxygen Vacancy on the Optical Properties of Porous Zirconia[J]. Acta Phys. -Chim. Sin., 2011,27(12): 2900-2906
94. CHEN Ke, BAO Zhi-Hao, LIU Dong, ZHU Xiu-Rong, ZHANG Zhi-Hua, ZHOU Bin.Confined Synthesis and Properties of Porous Silicon from Silica Aerogel Templates by Magnesiothermic Reduction[J]. Acta Phys. -Chim. Sin., 2011,27(11): 2719-2725
95. XUE Rong, YAN Jing-Wang, TIAN Ying, YI Bao-Lian.Lanthanum Doped Manganese Dioxide/Carbon Nanotube Composite Electrodes for Electrochemical Supercapacitors[J]. Acta Phys. -Chim. Sin., 2011,27(10): 2340-2346
96. XU Shou-Dong, ZHUANG Quan-Chao, SHI Yue-Li, ZHU Ya-Bo, QIU Xiang-Yun, SUN Zhi.Electrochemical Impedance Spectra of Intercalation Compound Electrodes: Models and Theoretical Simulations[J]. Acta Phys. -Chim. Sin., 2011,27(10): 2353-2359
97. XIA Hui-Yun, ZHANG Ying, GAO Li-Ning, YAN Lu-Ke.Ag-P(AM-co-MAA) Composite Microspheres Based on Morphology Transcription Method[J]. Acta Phys. -Chim. Sin., 2011,27(10): 2485-2492
98. LU Xiang-Jun, DOU Hui, YANG Su-Dong, HAO Liang, ZHANG Fang, ZHANG Xiao-Gang.Fabrication and Electrochemical Capacitive Behavior of Freestanding Graphene/Polyaniline Nanofibre Film[J]. Acta Phys. -Chim. Sin., 2011,27(10): 2333-2339
99. NIE Ping, SHEN Lai-Fa, CHEN Lin, SU Xiao-Fei, ZHANG Xiao-Gang, LI Hong-Sen.Sol-Gel Synthesis and Electrochemical Performance of Porous LiMnPO4/MWCNT Composites[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2123-2128
100. LI Xue-Fei, ZHAO Yun, JIAO Qing-Ze, LI Han-Sheng, WU Hong-Yu, LIU Hong-Bo, CUI Wen-Jia.Preparation of One-Dimensional Titanate Nanomaterials Using Different Titania Sources[J]. Acta Phys. -Chim. Sin., 2011,27(08): 1996-2000
101. TONG Xin, CHEN Rui, CHEN Tie-Hong.Photocatalytic Activity of TiO2 with Micrometer-Sized Macropores[J]. Acta Phys. -Chim. Sin., 2011,27(08): 1941-1946
102. WANG Sen-Lin, ZHANG Yi.Preparation and Electrocatalytic Performance of Ni-Mo/LaNi5 Porous Composite Electrode toward Hydrogen Evolution Reaction[J]. Acta Phys. -Chim. Sin., 2011,27(06): 1417-1423
103. CAO Yan-Li, DING Xiao-Long, LI Hong-Chen, YI Zhao-Guang, WANG Xiang-Fu, ZHU Jie-Jun, KAN Cai-Xia.Morphology-Controllable Noble Metal Nanoparticles: Synthesis, Optical Property and Growth Mechanism[J]. Acta Phys. -Chim. Sin., 2011,27(06): 1273-1286
104. LI Zhao, XU Ju-Liang, LI Xu-Yan, GUO Li-Fang, LI Jin, JIANG Yi-Ming.Preparation of Manganese Dioxide for Electrodes of Supercapacitors Based on Duplex Stainless Steel[J]. Acta Phys. -Chim. Sin., 2011,27(06): 1424-1430
105. ZHOU Jin, LI Wen, XING Wei, ZHUO Shu-Ping.Capacitive Performance of Tunable Ordered Mesoporous Carbons in Organic and H2SO4 Electrolytes[J]. Acta Phys. -Chim. Sin., 2011,27(06): 1431-1438
106. LIU Yu, ZHAO Jia-Fei, GUO Chang-Song, SONG Yong-Chen, LIU Wei-Guo, CHENG Chuan-Xiao, YE Chen-Cheng, XUE Kai-Hua.Memory Effects of Structure I and II Gas Hydrates[J]. Acta Phys. -Chim. Sin., 2011,27(06): 1305-1311
107. TIAN Ying, WANG Jing-Ri, LIU Ming, SHI Kun, YANG Feng-Lin.Redox Stability of Polypyrrole in Aqueous Electrolyte Solutions by a Recurrent Potential Pulse Technique[J]. Acta Phys. -Chim. Sin., 2011,27(05): 1116-1121
108. Lü Rong-Guan, YANG Jun, WANG Jiu-Lin, NULI Yan-Na.Electrodeposition and Electrochemical Property of Porous Li-Si Film Anodes for Lithium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2011,27(04): 759-763
109. SHAN Zhi-Chao, LIU Si-Yu, LI Cai-Jin, ZHU Long-Feng, MENG Xiang-Ju, XIAO Feng-Shou.High-Temperature Synthesis of Zeolite Y[J]. Acta Phys. -Chim. Sin., 2011,27(04): 959-964
110. KONG De-Shuai, WANG Jian-Ming, PI Ou-Yang, SHAO Hai-Bo, ZHANG Jian-Qing.Electrochemical Fabrication and Pseudocapacitive Performance of a Porous Nanostructured Nickel-Based Complex Film Electrode[J]. Acta Phys. -Chim. Sin., 2011,27(04): 764-768
111. MI Juan, WANG Yu-Ting, GAO Peng-Cheng, LI Wen-Cui.Effects of Thermal Treatment on the Electrochemical Behavior of Manganese Dioxide[J]. Acta Phys. -Chim. Sin., 2011,27(04): 893-899
112. YU Li-Qiu, CHEN Shu-Li, CHANG Sha, LI Yun-Hu, GAO Yin-Yi, WANG Gui-Ling CAO Dian-Xue.Supercapacitance of NiCo2O4 Nanowire Arrays Grown on Nickel Foam[J]. Acta Phys. -Chim. Sin., 2011,27(03): 615-619
113. LI Wen, ZHOU Jin, XING Wei, ZHUO Shu-Ping, Lü Yi-Min.Preparation of Microporous Carbon Using a Zeolite HY Template and Its Capacitive Performance[J]. Acta Phys. -Chim. Sin., 2011,27(03): 620-626
114. TIAN Ying, YAN Jing-Wang, XUE Rong, YI Bao-Lian.Influence of Electrolyte Concentration and Temperature on the Capacitance of Activated Carbon[J]. Acta Phys. -Chim. Sin., 2011,27(02): 479-485
115. ZHANG Hai-Jun, ZHANG Xiao-Gang, YUAN Chang-Zhou, GAO Bo, SUN Kang, FU Qing-Bin, LU Xiang-Jun, JIANG Jian-Chun.Preparation of Water Soluble Chitosan-Based Porous Carbon/NiO Composites and Their Electrochemical Capacitive Behavior[J]. Acta Phys. -Chim. Sin., 2011,27(02): 455-460
116. HUANG Rong, CHEN Ming-An, LU Xue-Bin.Chemical Oxidative Polymerization of Polypyrrole and Its Corrosion Resistance on the AZ31 Magnesium Alloy[J]. Acta Phys. -Chim. Sin., 2011,27(01): 113-119
117. ZHANG Qi-Bo, HUA Yi-Xin.Effect of the Ionic Liquid Additive-[BMIM]HSO4 on the Kinetics of Oxygen Evolution during Zinc Electrowinning[J]. Acta Phys. -Chim. Sin., 2011,27(01): 149-155
118. ZHANG Lei-Yong, HE Shui-Jian, CHEN Shui-Liang, GUO Qiao-Hui, HOU Hao-Qing.Preparation and Electrochemical Properties of Polyaniline/Carbon Nanofiber Composite Materials[J]. Acta Phys. -Chim. Sin., 2010,26(12): 3181-3186
119. ZHANG Fang, YUAN Chang-Zhou, ZHANG Xiao-Gang, ZHANG Luo-Jiang, XU Ke.5-Sulfosalicylic Acid-Assisted Hydrothermal Synthesis and Supercapacitive Properties of Co-Ni Layered Double Hydroxides[J]. Acta Phys. -Chim. Sin., 2010,26(12): 3175-3180
120. ZHANG Xiao-Bo, CHEN Ming-Hai, ZHANG Xiao-Gang, LI Qing-Wen.Preparation of Porous Carbon Nanofibers by Electrospinning and Their Electrochemical Capacitive Behavior[J]. Acta Phys. -Chim. Sin., 2010,26(12): 3169-3174
121. LI Mei-Chao, WANG Wu-Yang, ZHU Wan-Xia, MA Chun-An.Electrocatalytic Oxidation of Ascorbic Acid on a PPy-HEImTfa/Pt Electrode and Its Mechanism[J]. Acta Phys. -Chim. Sin., 2010,26(12): 3212-3216
122. WAN Qun-Yi, FAN Shuan-Shi, YUE Xian-Jun, LANG Xue-Mei, XU Wen-Dong, LI Jing, FENG Chun-Hua.Improved Capacitive Performance of Polypyrrole Doped with 9,10-Anthraquinone-2-sulfonic Acid Sodium Salt[J]. Acta Phys. -Chim. Sin., 2010,26(11): 2951-2956
123. GAN Li-Hua, LIU Ming-Xian, CHEN Long-Wu, HU Jun, LIU Hong-Lai.Effect of Catalysts on the Morphologies of Carbon Materials Synthesized by an Emulsion Templating Method[J]. Acta Phys. -Chim. Sin., 2010,26(10): 2666-2671
124. TIAN Ying, YAN Jing-Wang, LIU Xiao-Xue, XUE Rong, YI Bao-Lian.Electrochemical Capacitance of Composites with MnOx Loaded on the Surface of Activated Carbon Electrodes[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2151-2157
125. YANG Xiao-Deng, SHEN Qiang, XU Gui-Ying.Crystallization of Calcium Carbonate Using Water-Soluble Macromolecules[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2087-2095
126. ZHANG Jing, KONG Ling-Bin, CAI Jian-Jun, YANG Zhen-Sheng, LUO Yong-Chun, KANG Long.Novel Polypyrrole/Mesoporous Carbon Nanocomposite Electrode for an Electrochemical Hybrid Capacitor[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1515-1520
127. LI Qiao-Ling, CHANG Chuan-Bo, JING Hong-Xia, YANG Xiao-Feng.Synthesis and Magnetic Property of Shape-Controlled Nano-SrFe12O19[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1699-1704
128. LI Li-Min, LIU En-Hui, LI Jian, YANG Yan-Jing, SHEN Hai-Jie, HUANG Zheng-Zheng, XIANG Xiao-Xia.Polyaniline-Based Carbon for a Supercapacitor Electrode[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1521-1526
129. JI Qian-Qian, GUO Pei-Zhi, ZHAO Xiu-Song.Preparation of Chitosan-Based Porous Carbons and Their Application as Electrode Materials for Supercapacitors[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1254-1258
130. LI Sheng, QIU Yu-Bing, GUO Xing-Peng.Electrochemical Impedance of Polypyrrole Films under Different Conditions[J]. Acta Phys. -Chim. Sin., 2010,26(03): 601-609
131. ZANG Yang, HAO Xiao-Gang, WANG Zhong-De, ZHANG Zhong-Lin, LIU Shi-Bin.Copolymerization and Capacitive Performance of Composite Carbon Nanotubes/Polyaniline/Nickel Hexacyanoferrate Films[J]. Acta Phys. -Chim. Sin., 2010,26(02): 291-298
132. PANG Xu, MA Zheng-Qing, ZUO Lie.Sn Doped MnO2 Electrode Material for Supercapacitors[J]. Acta Phys. -Chim. Sin., 2009,25(12): 2433-2437
133. LI Li-Ying, SONG Wen-Hua, CHEN Tie-Hong.Synthesis of Hydroxyapatite Nanoplates by the Hydrothermal Reaction Method with Anionic Amino Acid Surfactant[J]. Acta Phys. -Chim. Sin., 2009,25(11): 2404-2408
134. TIAN Ying, WU Yan-Bo, WANG Jing-Ri, YANG Feng-Lin.Catalytic Reduction of Cu(II) by Polypyrrole[J]. Acta Phys. -Chim. Sin., 2009,25(11): 2249-2255
135. FU Qing-Bin, GAO Bo, SU Ling-Hao, YUAN Chang-Zhou, LU Xiang-Jun, ZHANG Xiao-Gang.Preparation of Polypyrrole/Benzenesulfonic Functionalized Multi-Walled Carbon Nanotubes Induced by Hydrogen Bonding and Their Electrochemical Behavior[J]. Acta Phys. -Chim. Sin., 2009,25(11): 2199-2204
136. SUN Zhe, LIU Kai-Yu, ZHANG Hai-Feng, LI Ao-Sheng, XU Xiao-Cun.Study on Meso-C/MnO2 Asymmetric Supercapacitors[J]. Acta Phys. -Chim. Sin., 2009,25(10): 1991-1997
137. ZHAO Yan-Chun, LAN Huang-Xian, TIAN Jian-Niao, YANG Xiu-Lin, WANG Feng-Yang.Electrocatalytic Oxidation of Methanol on Pt Nanoparticles Supported on Porous Poly(N-acetylaniline) Nanofibrils[J]. Acta Phys. -Chim. Sin., 2009,25(10): 2050-2054
138. WANG Run-Han, JIANG Ji-Sen, HU Ming.Controlled Syntheses of FeNi3 Alloy Nanostructures via Reverse Microemulsion-Directed Hydrothermal Motheds[J]. Acta Phys. -Chim. Sin., 2009,25(10): 2167-2172
139. WANG Yue-Juan, JIN Wei-Yang, WANG Xue-Li, JIN Ling-Yun, LU Ji-Qing, LUO Meng-Fei.Synthesis of Spherical SBA-15 Particles under Mixed and Dilute Electrolyte Conditions[J]. Acta Phys. -Chim. Sin., 2009,25(08): 1550-1554
140. MA Shan-Shan, ZHANG Ying-Jiu, HU Xiao-Yang, CHENG Liang, ZHOU Hui-Hua, TIAN Yong-Tao, LI Xin-Jian, ZHU Jing.Surface-Enhanced Raman Spectrum and Preparation of One-Dimensional Copper(Core)-Nickel(Shell) Nanostructure[J]. Acta Phys. -Chim. Sin., 2009,25(07): 1337-1341
141. HUANG Zhi-Hai, DONG Yin-Sheng, LIN Ping-Hua.Depositing an Apatite Coating in/on Massive Chitosan Porous Scaffolds by an Alternate Soaking Method[J]. Acta Phys. -Chim. Sin., 2009,25(07): 1285-1289
142. LEI Jian-Fei, LI Wei-Shan.Photoelectrocatalytic Performance of Arrayed Porous TiO2/Ti[J]. Acta Phys. -Chim. Sin., 2009,25(06): 1173-1178
143. FAN Xiao-Yong, ZHUANG Quan-Chao, WEI Guo-Zhen, KE Fu-Sheng, HUANG Ling, DONG Quan-Feng, SUN Shi-Gang.Fabrication and Performance of Cu6Sn5 Alloy Anode Using Porous Cu as Current Collector[J]. Acta Phys. -Chim. Sin., 2009,25(04): 611-616
144. JIANG Qi, ZHAO Xiao-Feng, HUANG Bin, DU Bing, ZHAO Yong.Effect of the Activated Carbon Reactivation on Its Electrochemical Capacitance[J]. Acta Phys. -Chim. Sin., 2009,25(04): 757-761
145. DU Xiao-Ming, WU Er-Dong.Behavior of Adsorbed Hydrogen Molecules on Zeolites[J]. Acta Phys. -Chim. Sin., 2009,25(03): 549-554
146. DU Bing, JIANG Qi, ZHAO Xiao-Feng, LIN Sun-Zhong, MU Pei-Shan, ZHAO Yong.Preparation of PPy/CNTs Composite Based on the Electrostatic Absorption Effect[J]. Acta Phys. -Chim. Sin., 2009,25(03): 513-518
147. LI Yang; XIE Hua-Qing; TU Jiang-Ping.SnS with Various Morphologies and Sizes as Anode Material for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2009,25(02): 365-370
148. WANG Rui; ZHANG Tong; HE Yuan; GENG Wang-Chang; NIU Li-Gang; LI Xiao-Tian.Complex Impedance Analysis of the Humidity Sensing Properties of Polypyrrole[J]. Acta Phys. -Chim. Sin., 2009,25(02): 327-330
149. CHEN Li; ZHANG Xiao-Gang; YUAN Chang-Zhou; CHEN Sheng-Yao.Electrochemical Properties of Poly(3,4-ethylenedioxythiophene)/Manganese Oxide Synthesized by Interfacial Polymerization[J]. Acta Phys. -Chim. Sin., 2009,25(02): 304-308
150. JIANG Qi; ZHANG Qian; DU Bing; ZHAO Xiao-Feng; ZHAO Yong.Preparation and Electrochemical Properties of CNTs-PANI Composite Material via Finite Field Polymerization[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1719-1723
151. LI Ming-Li, XU Ming-Xia, LIANG Hui, LI Xiao-Lei, XU Ting-Xian.Preparation and Dielectric Properties of Mn-Doped Ba0.6Sr0.4TiO3-MgTiO3 Composite Ceramics[J]. Acta Phys. -Chim. Sin., 2008,24(08): 1405-1410
152. SU Yue-Feng; WU Feng; ZANG Ge; BAO Li-Ying; CHEN Shi.Porous Carbon as Template for Synthesis of Li4Ti5O12 and Its Lithiation Performance[J]. Acta Phys. -Chim. Sin., 2008,24(06): 1002-1006
153. YANG Hai-Bo; HU Ming; LIANG Ji-Ran; ZHANG Xu-Rui; LIU Zhi-Gang.Microstructure, Nano-Mechanical and Temperature Sensitive Properties of VOx/Porous Silicon/Si Structure[J]. Acta Phys. -Chim. Sin., 2008,24(06): 1017-1022
154. TIAN Ying; LI Zhe-Qi; XU Hong-Feng; WU Yan-Bo; YANG Feng-Lin.Effects of Different Electrolyte Solutions on Characteristics of Polypyrrole-Modified Films[J]. Acta Phys. -Chim. Sin., 2008,24(04): 612-618
155. CHEN Yu-Ting; ZHANG Hai-Yan; ZHANG Guo-Qing; CHEN Yi-Ming; ZHU Qing-Feng.Influence of Addition of Carbon Nanotubes in the Hydrogen Storage Alloy Electrode on the Performance of SC High Power Batteries[J]. Acta Phys. -Chim. Sin., 2008,24(03): 527-532
156. ZENG Wen-Wen; HUANG Ke-Long; YANG You-Ping; LIU Su-Qin; LIU Ren-Sheng.Solvothermal Synthesis and Capacitance Performance of Co3O4 with Different Morphologies[J]. Acta Phys. -Chim. Sin., 2008,24(02): 263-268
157. YANG Hao-Wei; ZHANG Zhang; DUAN Xiao-Nan; YU Hong-Kun; JIN Qing-Yuan.Fabrication of Ultra Thin Porous Alumina Membrane on Silicon Substrate[J]. Acta Phys. -Chim. Sin., 2008,24(02): 313-316
158. YANG Jing; LIU Ya-Fei; CHEN Xiao-Mei; HU Zhong-Hua; ZHAO Guo-Hua.Carbon Electrode Material with High Densities of Energy and Power[J]. Acta Phys. -Chim. Sin., 2008,24(01): 13-19
159. LI Wei; Tong-Ge-La-Ge; MU Qi-Yong; QI Lu; GUO Jin.Chemical Pattern Recognition Applied to the Analysis of Effect of Technology Factors on the Properties of Li-Mn-O Spinel Oxide[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 10-13
160. HOU Xian-Quan; JIANG Wei-Jun; QI Lu; HAN Li-Juan.Synthesis and Properties of Layered LiNi0.8Co0.2-xMgxO2 Cathode Material[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 40-45
161. YAN Na; ZHANG Cun-Zhong; WU Feng; LIU Jing-Jing; CHEN Jun-Zheng.Influence of Electropolymerized Current Density on Polypyrrole Electrode of Lithium Ion Cells[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1747-1752
162. YANG Jian-Jun; HUANG Jun-Jie; JIANG Zhi-Yu.Supercapacitance of MnO2 Thin Film Electrodes Prepared Using Jet Printing Method[J]. Acta Phys. -Chim. Sin., 2007,23(09): 1365-1369
163. WANG Ting; JIANG Xin; LI Xi.Preparation of TiO2 Nanoparticles on Surface of Different Supports by Adsorption Phase Reaction Technique[J]. Acta Phys. -Chim. Sin., 2007,23(09): 1375-1380
164. YANG Hui; SHEN Qian-Hong; GAO Ji-Wei.Morphology Control of Anatase TiO2 Films Prepared at Low Temperature Using 4,4’-isopropylidenediphenol[J]. Acta Phys. -Chim. Sin., 2007,23(08): 1269-1274
165. FAN Xiao-Yong; ZHUANG Quan-Chao; JIANG Hong-Hong; HUANG Ling; DONG Quan-Feng; SUN Shi-Gang.Three-dimensional Porous Cu6Sn5 Alloy Anodes for Lithium-ion Batteries[J]. Acta Phys. -Chim. Sin., 2007,23(07): 973-977
166. ZHANG Hui; GUO Yu-Peng; LIU Yan-Hua; ZHAO Xu; DENG Yan-Hui; WANG Zi-Chen; JIANG Lei.Adsorption of Creatinine on Porous Carbon Prepared from Rice Husk[J]. Acta Phys. -Chim. Sin., 2007,23(06): 825-829
167. ZHOU Zhi-Hua; RUAN Jian-Ming; ZHOU Zhong-Cheng; ZOU Jian-Peng.Influence of Non-isothermal Melt Crystallization on the Thermal Behavior and Morphology of Poly-L-lactide[J]. Acta Phys. -Chim. Sin., 2007,23(05): 647-650
168. HUANG Ke-Long; LIU Ren-Sheng; YANG You-Ping; LIU Su-Qin; WANG Li-Ping.Shape-controlled Synthesis and Formation Mechanism of Co3O4 by Solvothermal Method[J]. Acta Phys. -Chim. Sin., 2007,23(05): 655-658
169. LIU Yong; WEI Zi-Dong; CHEN Si-Guo; FENG Yong-Chao; YIN Guang-Zhi; SUN Cai-Xin.PEMFC Electrodes Platinized by Modulated Pulse Current Electrodeposition[J]. Acta Phys. -Chim. Sin., 2007,23(04): 521-525
170. YIN Li-Song;CHEN Min-Tao;LI Ting;ZHOU Ke-Sheng;GAO Song-Hua.Preparation of Rhombic MgO Nanoflakes from Dolomites[J]. Acta Phys. -Chim. Sin., 2007,23(03): 433-437
171. WANG Jie;XU You-Long;CHEN Xi;DU Xian-Feng;LI Xi-Fei.Effect of Doping Ions on Electrochemical Capacitance Properties of Polypyrrole Films[J]. Acta Phys. -Chim. Sin., 2007,23(03): 299-304
172. TIAN Juan;ZHENG Dan;ZHANG Xi-Gui;ZHANG Bao-Hong;XIA Bao-Jia;YANG Hui.Preparation of Pt Nanoparticle Modified Porous Silicon Electrode and Its Electrocatalytic Performance[J]. Acta Phys. -Chim. Sin., 2007,23(01): 68-72
173. LI Qiang;LI Kai-Xi;SUN Guo-Hua;FAN Hui;GU Jian-Yu.A New Kind of Redox Electrolyte Electrochemical Capacitor System[J]. Acta Phys. -Chim. Sin., 2006,22(12): 1445-1450
174. ZHAO Chun-Xia;CHEN Wen;LIU Qi;TIAN Gao.Influence of HCl on the Mesostructure and Morphology of the Ordered Mesoporous Silica[J]. Acta Phys. -Chim. Sin., 2006,22(10): 1201-1205
175. PENG Jun-Xia;ZHANG Ying;XIA Hui-Yun;BAI Chao-Liang;FANG Yu.Studies on the Template Composition Dependence of the Surface Morphology of the Metal Sulfides-P(NIPAM-co-MAA) Composite Microspheres[J]. Acta Phys. -Chim. Sin., 2006,22(04): 424-429
176. MEI Yan;HAN Ye-Bin;NIE Zuo-Ren.The Influence of Reaction Temperature on the Morphology and Formation Mechanism of Ce2(C2O4)3•10H2O Powders[J]. Acta Phys. -Chim. Sin., 2006,22(04): 492-495
177. LIU Ling; ZHAO Yao-Min; YANG Jie; ZHAO Chong-Jun; JIANG Zhi-Yu.Photoeletrochemical Behavior of Polypyrrole Nanofiber Array Electrodes[J]. Acta Phys. -Chim. Sin., 2006,22(03): 261-264
178. XU Guo-Rong; REN Feng-Lian; SI Shi-Hui; YI Qing-Feng.Study on Removal of the Barrier between Al Substrate and Porous Anodic Alumina by Electrochemical Approach[J]. Acta Phys. -Chim. Sin., 2006,22(03): 341-344
179. XU Meng-Qing; ZUO Xiao-Xi; LI Wei-Shan; ZHOU Hao-Jie; LIU Jian-Sheng; YUAN Zhong-Zhi.Effect of Butyl Sultone on the Li-ion Battery Performance and Interface of Graphite Electrode[J]. Acta Phys. -Chim. Sin., 2006,22(03): 335-340
180. YANG Xiao; NI Jiang-feng; HUANG You-yuan; CHEN Ji-tao; ZHOU Heng-hui; ZHANG Xinxiang.Effect of Ti-Doping on Different Morphologic LiCoO2[J]. Acta Phys. -Chim. Sin., 2006,22(02): 183-188
181. REN Xin; HUANG Xin-min; ZHANG Hu-hai.Fabrication of Ni-P Nanowire and Nanotube Ordered Arrays by Electroless Deposition[J]. Acta Phys. -Chim. Sin., 2006,22(01): 102-105
182. WEN Jing-bang; ZHOU Hai-hui; LI Song-lin; LUO Sheng-lian; CHEN Jin-hua; KUANG Ya-fei.Growth Process of Nano-fibrous Polyaniline Film on Stainless Steel[J]. Acta Phys. -Chim. Sin., 2006,22(01): 106-109
183. ZHANG Lu; YAO Su-wei; ZHANG Wei-guo; WANG Hong-zhi.Preparation and Formation Mechanism of Alumina Nanowires[J]. Acta Phys. -Chim. Sin., 2005,21(11): 1254-1258
184. TANG Xin-cun; HUANG Bo-yun; HE Yue-hui.Dependence of Li+ Diffusion Coefficients in LiMn2O4 on Charge/Discharge Cycles[J]. Acta Phys. -Chim. Sin., 2005,21(09): 957-960
185. YANG Hong-Sheng; ZHOU Xiao; ZHANG Qing-Wu.Electrochemical Performances of Supercapacitor with Polyaniline Particles with Hierarchy as Active Electrode Material[J]. Acta Phys. -Chim. Sin., 2005,21(04): 414-418
186. Wang Juan; Zhang Chang-Rui; Feng Jian.Modification of Nanoporous Silica Film by Trimethylchlorosilane[J]. Acta Phys. -Chim. Sin., 2004,20(12): 1399-1403
187. Yu Chun-Ling;Zhai Jin;Ge Hong-Li;Wan Mei-Xiang;Jiang Lei;Li Ze-Sheng;Li Tie-Jin.Ordered Self-assembly of Polymer Nano-structure[J]. Acta Phys. -Chim. Sin., 2004,20(10): 1258-1261
188. Ni Jiang-Feng;Zhou Heng-Hui;Chen Ji-Tao;Su Guang-Yao.Effect on the Electrochemical Performance of Lithium Iron Phosphate by Cr3+ Ion Doping[J]. Acta Phys. -Chim. Sin., 2004,20(06): 582-586
189. Liu Xiu-Lin;Xu Hong-Yan;Meng Xian-Ping;Li Mei;Cui De-Liang;Song Yun-Jing;Bai Jian-Qiang;Li Mu-Sen.Preparation of Porous Hydroxyapatite Nanosolid by Solvent Hot Press Method[J]. Acta Phys. -Chim. Sin., 2004,20(06): 608-611
190. Jiang Qi;Lu Xiao-Ying;Zhao Yong;Yu Zuo-Long.Effect of Microstructure’s Change on Electrochemical Capacitance of Carbon Nanotubes[J]. Acta Phys. -Chim. Sin., 2004,20(05): 546-549
191. Liu Xian-Ming;Zhang Yi-He;Zhang Xiao-Gang;Fu Shao-Yun.The Supercapacitive Properties of Ni-Ru Oxide Composites[J]. Acta Phys. -Chim. Sin., 2004,20(04): 417-420
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