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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2007,Vol.23>> Issue(12)>> 1917-1921     doi: 10.3866/PKU.WHXB20071216         中文摘要
Preparation, Characterization and Photo-catalytic Behavior of TiO2 Catalysts with Oxygen Vacancies
CHEN Qi-Yuan; TONG Hai-Xia; YIN Zhou-Lan; HU Hui-Ping; LI Jie; LIU Liang-Liang
College of Chemistry and Chemical Engineering, Central South University, Changsha 410083, P. R. China
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The rutile TiO2 catalysts with oxygen vacancies were obtained under 927 ℃calcination using a mixed gas of saturation water vapor and H2 at 69 ℃. The catalysts were identified using X-ray diffraction (XRD), specific surface (BET), electron paramagnetic resonance spectroscopy (EPR), UV-Vis diffuse refraction spectroscopy (DRS), and X-ray photoelectron spectrum (XPS) measurements. The effect of calcination time on photocatalytic activity of TiO2 with different oxygen vacancies for O2 evolution was studied. The result indicated that appropriate oxygen vacancies could obviously improve the photocatalytic activity of rutile TiO2. The maximumO2 evolution speed of rutile TiO2 with oxygen vacancies was 222 μmol·L-1·h-1.

Keywords: TiO2   Calcination   Oxygen vacancies   Photocatalytic activity  
Received: 2007-06-14 Accepted: 2007-08-27 Publication Date (Web): 2007-09-21
Corresponding Authors: CHEN Qi-Yuan Email: cqy@mail.csu.edu.cn


Cite this article: CHEN Qi-Yuan; TONG Hai-Xia; YIN Zhou-Lan; HU Hui-Ping; LI Jie; LIU Liang-Liang. Preparation, Characterization and Photo-catalytic Behavior of TiO2 Catalysts with Oxygen Vacancies[J]. Acta Phys. -Chim. Sin., 2007,23 (12): 1917-1921.    doi: 10.3866/PKU.WHXB20071216
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