Article
Preparation Conditions of LiMn0.45Ni0.45Co0.1O2 via Hydroxide Co-precipitation
DAI Ke-Hua; WANG Yin-Jie; FENG Hua-Jun; XIE Yan-Ting; QI Lu
New Energy Materials and Technology Laboratory, Department of Applied Chemistry, College of Chemistry and Molecular Engineering, Peking University, Beijing 100871, P. R. China; National Laboratory of Flame Retarded Materials, Beijing Institute of Technology, Beijing 100081, P. R. China
New Energy Materials and Technology Laboratory, Department of Applied Chemistry, College of Chemistry and Molecular Engineering, Peking University, Beijing 100871, P. R. China; National Laboratory of Flame Retarded Materials, Beijing Institute of Technology, Beijing 100081, P. R. China
Ni0.45Co0.1Mn0.45(OH)2was prepared via improved hydroxide co-precipitation. The effect of reaction condition on the shape of the product, and the effect of F- ion on the morphology and tap-density of the product were studied. LiMn0.45Ni0.45Co0.1O2 and LiMn0.45Ni0.45Co0.1O1.96F0.04 were prepared by mixing this metal hydroxide with 5% excess LiOH followed by heat-treatment. The effect of F doping on the cycling performance of the prodct was investigated. The morphology and tap-density of the product were improved through the addition of F- in co-precipitation system. The product was characterized using X-ray diffraction (XRD), scanning electron microscope (SEM) and charge-discharge tests. It can be seen from the SEMresults that the product has a good shape. The XRD studies showed that the material had a well-ordered layered structure without impurity phase. The initial capacities of both LiMn0.45Ni0.45Co0.1O2 and LiMn0.45Ni0.45Co0.1O1.96F0.04 are 157 mAh·g-1 at a charging potential between 2.8 and 4.4 V and a current density of 30 mA·g -1. The 72.6% and 86.0% discharge capacities were retained at the end of 50 charge-discharge cycles, respectively. It is shown that the F doping can obviously improve the cycling performance of the product.
Keywords: Lithiumion secondary battery Cathodematerial Co-precipitation LiMn0.5-xNi0.5-xCo2xO2 F doping
Received: 2007-09-17 Accepted: 2007-10-09 Publication Date (Web): 2007-10-25
Corresponding Authors: QI Lu Email: qilu@pku.edu.cn
Cite this article: DAI Ke-Hua; WANG Yin-Jie; FENG Hua-Jun; XIE Yan-Ting; QI Lu. Preparation Conditions of LiMn0.45Ni0.45Co0.1O2 via Hydroxide Co-precipitation[J]. Acta Phys. -Chim. Sin., 2007,23 (12): 1927-1931. doi: 10.3866/PKU.WHXB20071218
Keywords: Lithiumion secondary battery Cathodematerial Co-precipitation LiMn0.5-xNi0.5-xCo2xO2 F doping
Received: 2007-09-17 Accepted: 2007-10-09 Publication Date (Web): 2007-10-25
Corresponding Authors: QI Lu Email: qilu@pku.edu.cn
Cite this article: DAI Ke-Hua; WANG Yin-Jie; FENG Hua-Jun; XIE Yan-Ting; QI Lu. Preparation Conditions of LiMn0.45Ni0.45Co0.1O2 via Hydroxide Co-precipitation[J]. Acta Phys. -Chim. Sin., 2007,23 (12): 1927-1931. doi: 10.3866/PKU.WHXB20071218
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84． Zhao Shi-Xi;Min Xin-Min;Liu Han-Xing;Li Qiang;Ouyang Shi-Xi.The Structural Stability of S-M (M=Al, Co) Co-doped Spinel LiMn2O4 Cathode Materials[J]. Acta Phys. -Chim. Sin., 2004,20(03): 233-236
85． Yang Hong-Ping;Wang Xian-You;Wang Xing-Yan;Huang Wei-Guo;Luo Xu-Fang;Zhuo Hai-Tao.Preparation and Performance of Electrode Materials for Super-iron (VI) Battery[J]. Acta Phys. -Chim. Sin., 2003,19(12): 1150-1153
86． Tang Zhi-Yuan;Xu Guo-Xiang.The Application of Poly (1-aminoanthraquinone) for Positive Electrode Material in Lithium Secondary Battery[J]. Acta Phys. -Chim. Sin., 2003,19(04): 307-310
87． Wu Yu-Ping, Jiang Chang-Yin, Wan Chun-Rong, Fang Shi-Bi, Jiang Ying-Yan.Effects of the Addition of Crosslinker on Properties of Carbon Anode Materials[J]. Acta Phys. -Chim. Sin., 1999,15(12): 1106-1111
88． Wu Yu-Ping, Fang Shi-Bi, Jiang Ying-Yan, Wan Chun-Rong.Modification of Carbon Anode of Lithium lon Secondary Battery[J]. Acta Phys. -Chim. Sin., 1999,15(02): 133-137
89． Luo Sheng-Cheng,Gui Lin-Lin,Tang You-Qi.The Comparative Study on TiO2-Al2O3 Composites[J]. Acta Phys. -Chim. Sin., 1996,12(01): 7-11
90． HUANG Wei, WU Chun-Yang, ZENG Yue-Wu, JIN Chuan-Hong, ZHANG Ze.Surface Analysis of Lithium-Rich Cathode Material Li1.2Mn0.54Co0.13Ni0.13NaxO2 by Advanced Electron Microscopy[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
2． WUAi-Ming, XIA Guo-Feng, SHEN Shui-Yun, YIN Jie-Wei, MAO Ya, BAI Qing-You, XIE Jing-Ying, ZHANG Jun-Liang.Recent Progress in Non-Aqueous Lithium-Air Batteries[J]. Acta Phys. -Chim. Sin., 2016,32(8): 1866-1879
3． HUANG Wei, WU Chun-Yang, ZENG Yue-Wu, JIN Chuan-Hong, ZHANG Ze.Electron Microscopy Study of Surface Reconstruction and Its Evolution in P2-Type Na0.66Mn0.675Ni0.1625Co0.1625O2 for Sodium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2016,32(6): 1489-1494
4． YANG Zu-Guang, HUAWei-Bo, ZHANG Jun, CHEN Jiu-Hua, HE Feng-Rong, ZHONG Ben-He, GUO Xiao-Dong.Enhanced Electrochemical Performance of LiNi0.5Co0.2Mn0.3O2 Cathode Materials at Elevated Temperature by Zr Doping[J]. Acta Phys. -Chim. Sin., 2016,32(5): 1056-1061
5． KOU Jian-Wen, WANG Zhao, BAO Li-Ying, SU Yue-Feng, HU Yu, CHEN Lai, XU Shao-Yu, CHEN Fen, CHEN Ren-Jie, SUN Feng-Chun, WU Feng.Layered Lithium-Rich Cathode Materials Synthesized by an Ethanol-Based One-Step Oxalate Coprecipitation Method[J]. Acta Phys. -Chim. Sin., 2016,32(3): 717-722
6． SUN Xiao-Fei, XU You-Long, ZHENG Xiao-Yu, MENG Xiang-Fei, DING Peng, REN Hang, LI Long.Triple-Cation-Doped Li3V2(PO4)3 Cathode Material for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2015,31(8): 1513-1520
7． SHI Xia-Xing, LIAO Shi-Xuan, YUAN Bing, ZHONG Yan-Jun, ZHONG Ben-He, LIU Heng, GUO Xiao-Dong.Facile Synthesis of 0.6Li2MnO3-0.4LiNi0.5Mn0.5O2 with Hierarchical Micro/Nanostructure and High Rate Capability as Cathode Material for Li-Ion Battery[J]. Acta Phys. -Chim. Sin., 2015,31(8): 1527-1534
8． ZHANG Ji-Bin, HUAWei-Bo, ZHENG Zhuo, LIU Wen-Yuan, GUO Xiao-Dong, ZHONG Ben-He.Preparation and Electrochemical Performance of Li[Ni1/3Co1/3Mn1/3]O2 Cathode Material for High-Rate Lithium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2015,31(5): 905-912
9． HUANG Zhi-Peng, GUO Lin-Yu, GUO Chao, ZHAO Meng-Meng, WANG Xue-Hua, JIN Zhao, LUO Jin-Hua, WANG Xin, FENG Ji-Jun.Synthesis of Fluorinated Polyanionic Lithium Ion Insertion/Extraction Material LiVPO4F/C by Carbon Thermal Reduction Assisted Sol-Gel Method[J]. Acta Phys. -Chim. Sin., 2015,31(4): 700-706
10． REN Xiang-Zhong, LIU Tao, SUN Ling-Na, ZHANG Pei-Xin.Preparation and Electrochemical Performances of Li1.2Mn0.54-xNi0.13Co0.13ZrxO2 Cathode Materials for Lithium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2014,30(9): 1641-1649
11． HUA Wei-Bo, ZHENG Zhuo, LI Long-Yan, GUO Xiao-Dong, LIU Heng, SHEN Chong-Heng, WU Zhen-Guo, ZHONG Ben-He, HUANG Ling.Synthesis of Nanostructured LiNi1/3Co1/3Mn1/3O2 by Ammonia-Evaporation-Induced Synthesis and Its Electrochemical Properties as a Cathode Material for a High-Power Li-Ion Battery[J]. Acta Phys. -Chim. Sin., 2014,30(8): 1481-1486
12． YAN Jing-Sen, WANG Hai-Yan, ZHANG Jing-Ru, XU Hui-Juan.Effect of TiO2-Al2O3 Support Preparation Technique on Hydrodenitrogenation of Ni2P/TiO2-Al2O3 Catalysts[J]. Acta Phys. -Chim. Sin., 2014,30(7): 1309-1317
13． YU Zai-Lu, XIE Peng-Fei, TANG Xing-Fu, YUE Ying-Hong, HUA Wei-Ming, GAO Zi.Selective Catalytic Reduction of NO with NH3 over MnOx-CeO2-WO3-ZrO2：Effect of Calcination Temperature[J]. Acta Phys. -Chim. Sin., 2014,30(6): 1175-1179
14． ZHU Zhi, QI Lu, LI Wei, LIAO Xi-Ying.Preparation and Electrochemical Performance of 5 V LiNi0.5Mn1.5O4 Cathode Material by the Composite Co-Precipitation Method for High Energy/High Power Lithium Ion Secondary Batteries[J]. Acta Phys. -Chim. Sin., 2014,30(4): 669-676
15． CHEN Lai, CHEN Shi, HU Dao-Zhong, SU Yue-Feng, LI Wei-Kang, WANG Zhao, BAO Li-Ying, WU Feng.Crystal Structure and Electrochemical Performance of Lithium-Rich Cathode Materials xLi2MnO3·(1-x)LiNi0.5Mn0.5O2 (x=0.1-0.8)[J]. Acta Phys. -Chim. Sin., 2014,30(3): 467-475
16． YANG Wen-Chao, BI Yu-Jing, YANG Bang-Cheng, WANG De-Yu, SHI Si-Qi.Preparation and Electrochemical Characterization of Nano-LiMnPO4[J]. Acta Phys. -Chim. Sin., 2014,30(3): 460-466
17． WU Yue, LIU Xing-Quan, ZHANG Zheng, ZHAO Hong-Yuan.Preparation and Characterization of M(Ⅱ) and M(Ⅳ) Iso-Molar Co-Doped LiMn1.9Mg0.05Ti0.05O4 Cathode Materials for Lithium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2014,30(12): 2283-2290
18． ZHENG Jie-Yun, WANG Rui, LI Hong.Fabrication and Electrochemical Behavior of a Pure-Phase Li2MnO3 Thin Film for Cathode Material of Li-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2014,30(10): 1855-1860
19． SU Chang, HUANG Qi-Fei, XU Li-Huan, ZHANG Cheng.Preparation and Performances of C-LiFePO4/Polytriphenylamine Composite as Cathode Material for Lithium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2014,30(1): 88-94
20． CHEN Qiang, NULI Yan-Na, GUOWei, YANG Jun, WANG Jiu-Lin, GUO Yu-Guo.PTMA/Graphene as a Novel Cathode Material for Rechargeable Magnesium Batteries[J]. Acta Phys. -Chim. Sin., 2013,29(11): 2295-2299
21． ZHONG Yan-Jun, LI Jun-Tao, WU Zhen-Guo, ZHONG Ben-He, GUO Xiao-Dong, HUANG Ling, SUN Shi-Gang.Synthesis of Na2MnPO4F/C with Different Carbon Sources and Their Performances as Cathode for Lithium Ion Battery[J]. Acta Phys. -Chim. Sin., 2013,29(09): 1989-1997
22． CAO Yan-Bing, LUO Liang, DU Ke, PENG Zhong-Dong, HU Guo-Rong, JIANG Feng.Synthesis and Electrochemical Properties of LiFe1-xNbxPO4/C Composite Cathode Material by Two-Step Synthesis Route[J]. Acta Phys. -Chim. Sin., 2013,29(07): 1507-1514
23． YUAN Zhi-Hong, MA Jun, CHEN Xing, LIU Kai-Yu.P123-Assisted Rheological Phase Reaction Synthesis and Electrochemical Performance of Li3V2(PO4)3/C Cathode[J]. Acta Phys. -Chim. Sin., 2012,28(12): 2898-2904
24． SUN Xiao-Fei, XU You-Long, LIU Yang-Hao, LI Lu.Optimizing the Hydrothermal Synthesis of Micro-Sized Olivine LiFePO4[J]. Acta Phys. -Chim. Sin., 2012,28(12): 2885-2892
25． LI Jie-Bin, XU You-Long, DU Xian-Feng, SUN Xiao-Fei, XIONG Li-Long.Improved Electrochemical Stability of Zn-Doped LiNi1/3Co1/3Mn1/3O2 Cathode Materials[J]. Acta Phys. -Chim. Sin., 2012,28(08): 1899-1905
26． CAO Yan-Bing, DUAN Jian-Guo, JIANG Feng, HU Guo-Rong, PENG Zhong-Dong, DU Ke.Synthesis of LiFePO4 Cathode Materials by Mechanical-Activation-Assisted Polyol Processing[J]. Acta Phys. -Chim. Sin., 2012,28(05): 1183-1188
27． XIONG Li-Long, XU You-Long, ZHANG Cheng, TAO Tao.Doping-Coating Surface Modification of Spinel LiMn2O4 Cathode Material with Al3+ for Lithium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2012,28(05): 1177-1182
28． CHE Qian, ZHANG Fang, ZHANG Xiao-Gang, LU Xiang-Jun, DING Bing, ZHU Jia-Jia.Preparation of Ordered Mesoporous Carbon/NiCo2O4 Electrode and Its Electrochemical Capacitive Behavior[J]. Acta Phys. -Chim. Sin., 2012,28(04): 837-842
29． WANG Zhao, WU Feng, SU Yue-Feng, BAO Li-Ying, CHEN Lai, LI Ning, CHEN Shi.Preparation and Characterization of xLi2MnO3·(1-x)Li[Ni1/3Mn1/3Co1/3]O2 Cathode Materials for Lithium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2012,28(04): 823-830
30． ZHAO Lei, WANG An-Bang, WANG Wei-Kun, YU Zhong-Bao, CHEN Shi, YANG Yu-Sheng.Preparation and Electrochemical Performance of Aminoanthraquinone Derivative as Cathode Materials in Rechargeable Lithium Batteries[J]. Acta Phys. -Chim. Sin., 2012,28(03): 596-602
31． WANG Shao-Liang, TANG Zhi-Yuan, SHA Ou, YAN Ji.Synthesis and Electrochemical Performance of LiCoPO4 by Sol-Gel Method[J]. Acta Phys. -Chim. Sin., 2012,28(02): 343-348
32． GAO Ping, TAN Zhuo, CHENG Fu-Quan, ZHOU Heng-Hui, TAN Song-Ting.Effect of Doping with Ti4+ Ion on the Electrochemical Performance of LiFe0.6Mn0.4PO4/C[J]. Acta Phys. -Chim. Sin., 2012,28(02): 338-342
33． GONG Qiang, WANG Hong, LIAO Xiao-Zhen, MA Wei, HE Yu-Shi, MA Zi-Feng.Electrochemical Performance of Vanadium Modified LiFe0.5Mn0.5PO4/C Cathode Materials for Lithium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2012,28(01): 100-104
34． LI Jie-Bin, XU You-Long, XIONG Li-Long, WANG Jing-Ping.Improvement of LiNi1/3Co1/3Mn1/3O2 Cathode Materials by Nano-MgO Doping[J]. Acta Phys. -Chim. Sin., 2011,27(11): 2593-2599
35． WEI Yi, WANG Li-Juan, YAN Ji, SHA Ou, TANG Zhi-Yuan, MA Li.Calcination Temperature Effects on the Electrochemical Performance of Li2MnSiO4/C Cathode Material for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2011,27(11): 2587-2592
36． YAN Hui, ZHANG Huan, ZHANG Ding, ZHU Zhi, QI Lu.Hydrothermal Synthesis of Spherical Li4Ti5O12 as Anode Material for High Power Lithium-Ion Secondary Battery[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2118-2122
37． CHU Dao-Bao, LI Yan, SONG Qi, ZHOU Ying.Synthesis and Properties of LiFePO4/C Cathode Material with a New Carbon Source[J]. Acta Phys. -Chim. Sin., 2011,27(08): 1863-1867
38． SU Ya-Ling, LI Yi, DU Ying-Xun, LEI Le-Cheng.Visible-Light-Driven Catalytic Properties and First-Principles Study of Fluorine-Doped TiO2 Nanotubes[J]. Acta Phys. -Chim. Sin., 2011,27(04): 939-945
39． TANG Yan, ZHONG Ben-He, GUO Xiao-Dong, LIU Heng, ZHONG Yan-Jun, NIE Xiang, TANG Hong.Effects of Mixed Solvents on the High-Rate Performance of Li3V2(PO4)3/C Prepared by Sol-Gel Method[J]. Acta Phys. -Chim. Sin., 2011,27(04): 869-874
40． ZHANG Qiu-Mei, SHI Zhi-Cong, LI Yi-Xiao, GAO Dan, CHEN Guo-Hua, YANG Yong.Recent Advances in Fluorophosphate and Orthosilicate Cathode Materials for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2011,27(02): 267-274
41． WANG Xiao-Ya, CHENG Qian, HUANG Tao, YU Ai-Shui.Effect of Calcination Atmosphere on Li/Ni Disorder and Electrochemical Performance of Layered LiNi0.5Mn0.5O2[J]. Acta Phys. -Chim. Sin., 2011,27(02): 437-442
42． CHANG Zhao-Rong, DAI Dong-Mei, LI Bao, TANG Hong-Wei.Effect of Hydrazine on the Performance of LiNi0.5Mn1.5O4Cathode Materials[J]. Acta Phys. -Chim. Sin., 2010,26(10): 2633-2637
43． DAI Ke-Hua, MAO Jing, ZHAI Yu-Chun.High Rate Capability of 5 V LiNi0.5Mn1.5O4 Cathode Materials Synthesized via a Gel-Combustion Method[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2130-2134
44． CUI Wen-Yu, AN Mao-Zhong, YANG Pei-Xia.Preparation of an Ionic Liquid Gel Polymer Electrolyte and Its Compatibility with a LiFePO4 Cathode[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1233-1238
45． CHANG Zhao-Rong, YU Xu, TANG Hong-Wei, WEI Wen-Qiang, DAI Dong-Mei.Influence of Al Doping Content on the Structure and Electrochemical Properties of LiNi1/3Co2/3-xAlxO2[J]. Acta Phys. -Chim. Sin., 2010,26(03): 567-572
46． WANG Wei-Kun, ZHANG Yong-Yong, WANG An-Bang, YU Zhong-Bao, HAN Min-Fang, YANG Yu-Sheng.Electrochemical Performance of 1,4,5,8-Tetrahydroxy-9,10-anthraquinone as Cathode Material in Lithium Batteries[J]. Acta Phys. -Chim. Sin., 2010,26(01): 47-50
47． LU Hua-Quan, WU Feng, SU Yue-Feng, LI Ning, CHEN Shi, BAO Li-Ying.Electrochemical Performance of LiNi0.5Mn0.5O2 as Cathode Material for Lithium-Ion Batteries Prepared by Oxalate Co-Precipitation Method[J]. Acta Phys. -Chim. Sin., 2010,26(01): 51-56
48． YU Hong-Ming, ZHENG Wei, CAO Gao-Shao, ZHAO Xin-Bing.Effects of Optimized Carbon-Coating on High-Rate Performance of LiFePO4/C Composites[J]. Acta Phys. -Chim. Sin., 2009,25(11): 2186-2190
49． ZHENG Jun-Chao, LI Xin-Hai, WANG Zhi-Xing, LI Jin-Hui, WU Ling, LI Ling-Jun, GUO Hua-Jun.A Coalescence Mechanism for the Composite Cathode Material xLiFePO4·yLi3V2(PO4)3[J]. Acta Phys. -Chim. Sin., 2009,25(09): 1916-1920
50． ZHONG Mei-E, ZHOU Zhi-Hui, ZHOU Zhen-Tao.Electrochemical Performance of High-Density LiFePO4/C Composites Synthesized by Solid State-Carbothermal Reduction Method[J]. Acta Phys. -Chim. Sin., 2009,25(08): 1504-1510
51． FENG Ji-Jun, LIU Xiang-Zhe, LIU Xiao-Zhen, JIANG Jian-Zhuang, ZHAO Jing.Hydrothermal Syntheses and Properties of LiV3-xMnxO8 as Cathode Materials for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2009,25(08): 1490-1494
52． HU Guo-Rong, CAO Yan-Bing, PENG Zhong-Dong, DU Ke, JIANG Qing-Lai.Preparation of Li2FeSiO4 Cathode Material for Lithium-Ion Batteries by Microwave Synthesis[J]. Acta Phys. -Chim. Sin., 2009,25(05): 1004-1008
53． WANG Wei-Cheng, LI Shuo, WEN Yi-Yun, GONG Mao-Chu, ZHANG Lei, YAO Yan-Ling, CHEN Yao-Qiang.Synthesis and Characterization of TiO2/YFeO3 and Its Photocatalytic Oxidation of Gaseous Benzene[J]. Acta Phys. -Chim. Sin., 2008,24(10): 1761-1766
54． YANG Shun-Yi; WANG Xian-You; WEI Jian-Liang; LI Xiu-Qin; TANG An-Ping.Preparation and Electrochemical Performance of Na-Mn-O Cathode Materials[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1669-1674
55． ZHANG Lei, ZHENG Ling-Min, GUO Jia-Xiu, WU Dong-Dong, GONG Mao-Chu, WANG Jian-Li, CHEN Yao-Qiang.Structure Evolution Process of Ce0.65Zr0.25Y0.1O1.95 Prepared by Oxidation-Coprecipitation Method[J]. Acta Phys. -Chim. Sin., 2008,24(08): 1342-1346
56． CHANG Zhao-Rong; CHEN Zhong-Jun; WU Feng; TANG Hong-Wei; ZHU Zhi-Hong.Synthesis of LiNi1/3Co1/3Mn1/3O2 Cathode Material by Eutectic Molten Salt LiOH-LiNO3[J]. Acta Phys. -Chim. Sin., 2008,24(03): 513-519
57．
DU Guo-Dong; NULI Yan-Na; FENG Zhen-Zhen; WANG Jiu-Lin; YANG Jun
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59． ZHANG Chun-Ling; JIANG Wei-Jun; ZHANG Jing; QI Lu.Performance of LiMn1.5Ni0.5-xCuxO4 as 5V Cathode Material for Lithium-ion Battery[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 31-35
60． HOU Xian-Quan; JIANG Wei-Jun; QI Lu; HAN Li-Juan.Synthesis and Properties of Layered LiNi0.8Co0.2-xMgxO2 Cathode Material[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 40-45
61． CHEN Yong-Chong; XU Xing-Jun; CUI Hong-Zhi; DAI Ke-Hua; SONG Zhao-Shuang; JIANG Wei-Jun; QI Lu.Synthesis Mechanisms and Properties of Cathode Material LiNixMn2-xO4[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 26-30
62． JIANG Wei-Jun; Sai-Xi-Ya-Le-Tu; Wu-Yun-Bi-Li-Ge; QI Lu; SHANG Shi-Bo.Performance of Nonstoichiometric Li1+xCoO2 Cathode Materials[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 56-59
63．
WANG Jian; QI Yu-Jun; LI Yong-Wei; QI Lu
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65． DENG Zheng-Hua; LI Ren-Gui; WANG Lu; DENG Jia-Min; GAO Jian-Dong; MA Zhi-Gang; DU Hong-Chang; SUO Ji-Shuan.Research and Development of Separators for Lithium-ion Battery[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 90-93
66． CHEN Yong-Chong; XU Xing-Jun; CUI Hong-Zhi; DAI Ke-Hua; SONG Zhao-Shuang; JIANG Wei-Jun; QI Lu.Preferred Orientation of Crystals and the Intensity Ratios of XRD Peaks of Cathode Material LiCoO2[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1948-1953
67． HOU Chun-Ping; YUE Min.A Novel Cathode Material Lithium Vanadium Phosphate Synthesized by Liquid-phase Sphericizing Granulation[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1954-1957
68． WEI Ying-Jin; LI Xu; WANG Chun-Zhong; ZHAN Shi-Ying; CHEN Gang.Preparation and Electrochemical Properties of Cu Doped V2O5[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1090-1094
69． LIU Su-Qin; LI Shi-Cai; HUANG Ke-Long; CHEN Zhao-Hui.Effect of Doping Ti4+ on the Structure and Performances of Li3V2(PO4)3[J]. Acta Phys. -Chim. Sin., 2007,23(04): 537-542
70． WANG Jun; FAN Mei-Qing; YANG Piao-Ping; YU Wei; JING Xiao-Yan; ZHANG Mi-Lin; LIU Tian-Fu; DUAN Xue.Preparation and Characterization of Magnetic Solid Superacid SO2-4/ZrO2/Fe3O4/Al2O3[J]. Acta Phys. -Chim. Sin., 2007,23(04): 595-600
71． FENG Zhen-Zhen;NULI Yan-Na;YANG Jun.Conductive Sulfur-Containing Material/Polyaniline Composite for Cathode Material of Rechargeable Magnesium Batteries[J]. Acta Phys. -Chim. Sin., 2007,23(03): 327-331
72． ZHUANG Da-Gao;ZHAO Xin-Bing;XIE Jian;TU Jian;ZHU Tie-Jun;CAO Gao-Shao.One-step Solid-state Synthesis and Electrochemical Performance of Nb-doped LiFePO4/C[J]. Acta Phys. -Chim. Sin., 2006,22(07): 840-844
73． ZHAO Jing; LI Huai-Xiang; WANG An-He; ZHOU Hong-Wei; ZUO Xiang-Qing.A Study of CaSiO3∶Pb, Mn Phosphors Coated by ZnO∶Al[J]. Acta Phys. -Chim. Sin., 2006,22(03): 286-290
74． WANG Yan; JING Zhi-hong; WU Shi-hua; HUANG Wei-ping; ZHANG Shou-min; WANG Shu-rong.The Effect of Au-doping by Different Methods on Gas-sensing Properties of α-Fe2O3 Nanopowders[J]. Acta Phys. -Chim. Sin., 2006,22(01): 114-117
75． TANG Ding-guo; LIU Jian-hong; CI Yun-xiang; QI Lu.Preparation and Performances of a Novel Gel Polymer Electrolyte[J]. Acta Phys. -Chim. Sin., 2005,21(11): 1263-1268
76． TANG Zhi-yuan; LU Xing-he; ZHANG Na.The Anion-cation Multiple Doping Effect of Spinel Cathode Materials on Electrochemical Speciality[J]. Acta Phys. -Chim. Sin., 2005,21(08): 934-938
77． TAO Bin-Wu;LIU Jian-Hua;LI Song-Mei;ZHAO Liang.Electrochemical Properties of a V2O5/C Composite in Aqueous Solution Used for Zinc Secondary Battery[J]. Acta Phys. -Chim. Sin., 2005,21(03): 338-342
78． LU Jun-Biao; TANG Zi-Long; ZHANG Zhong-Tai; JIN Yong-Zhu.Influence of Mg Ion Doping on the Battery Properties of LiFePO4/C[J]. Acta Phys. -Chim. Sin., 2005,21(03): 319-323
79． Wang Wei-Kun; Wang An-Bang; Cao Gao-Ping; Yang Yu-Sheng.Electrochemical Performance of a Novel Cathode Material Phenyl Polysulfide for Lithium Batteries[J]. Acta Phys. -Chim. Sin., 2004,20(12): 1440-1444
80． Gou Guo-Jing;Ma Pei-Hua;Chu Min-Xiong.Kinetics of Synthetic of Cl－ Type Hydrotalcitelike with Coprecipitation Reaction[J]. Acta Phys. -Chim. Sin., 2004,20(11): 1357-1363
81． Han Xiang-Yun;Wang Zun-Yao;Wang Lian-Sheng;Yang Chun-Sheng;Yu Bin.Kinetics of Synthetic of Cl－ Type Hydrotalcitelike with Coprecipitation Reaction[J]. Acta Phys. -Chim. Sin., 2004,20(11): 1364-1368
82． Chang Xiao-Yan;Wang Zhi-Xing;Li Xin-Hai;Kuang Qiong;Peng Wen-Jie;Guo Hua-Jun;Zhang Yun-He.Synthesis and Performance of LiMnPO4 Used as Cathode Material for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2004,20(10): 1249-1252
83． Ni Jiang-Feng;Zhou Heng-Hui;Chen Ji-Tao;Su Guang-Yao.Effect on the Electrochemical Performance of Lithium Iron Phosphate by Cr3＋ Ion Doping[J]. Acta Phys. -Chim. Sin., 2004,20(06): 582-586
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