ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2008,Vol.24>> Issue(01)>> 171-175     doi: 10.3866/PKU.WHXB20080131         中文摘要
Synthesis of High Surface Area Silicon Carbide and Its Application in CO Oxidation Reaction
ZHAN Ying-Ying; CAI Guo-Hui; ZHENG Yong; SHEN Xiao-Nv; ZHENG Ying; WEI Ke-Mei
National Engineering Research Center of Chemical Fertilizer Catalyst at Fuzhou University, Fuzhou 350002, P. R. China; College of Chemistry and Materials Science, Fujian Normal University, Fuzhou 350007, P. R. China
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A sol-gel process was employed to prepare SiC precursors, using tetraethyl orthosilicate (TEOS) and sucrose as raw materials. And oxalic acid, ferric nitrate, and nickel nitrate were added respectively as catalyst for hydrolysis and polymeration reactions. The effects of catalyst, reaction temperature, and reaction time on the gel formation were studied. The results showed that ferric nitrate was optimal for gel formation. SiC of 133 m2·g-1 was obtained by further carbonthermal reduction of the xerogel from the sol-gel system involved ferric nitrate, at 1350 ℃ in an Ar flow for 10 h. Such SiC was then used as catalyst support for CO oxidation. Wet impregnation method was adopted to obtain Pt/SiC catalyst. The as-prepared Pt/SiC catalyst showed good activity and stability for CO oxidation. It was also found that its performance could be improved significantly with the synergistic action of Ni promoter.

Keywords: Sol-gel   Silicon carbide   High surface area   CO oxidation   Support  
Received: 2007-08-26 Accepted: 2007-09-11 Publication Date (Web): 2007-10-24
Corresponding Authors: WEI Ke-Mei Email:

Cite this article: ZHAN Ying-Ying; CAI Guo-Hui; ZHENG Yong; SHEN Xiao-Nv; ZHENG Ying; WEI Ke-Mei. Synthesis of High Surface Area Silicon Carbide and Its Application in CO Oxidation Reaction[J]. Acta Phys. -Chim. Sin., 2008,24 (01): 171-175.    doi: 10.3866/PKU.WHXB20080131
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88. JIN Ling-Yun; LU Ji-Qing; LUO Meng-Fei; XIE Guan-Qun; HE Mai.CeO2-Y2O3 Washcoat and Supported Pd Catalysts for the Combustion of Volatile Organic Compounds (VOCs)[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1691-1695
89. WANG Feng; HAO Ya-Juan; JIN Guo-Qiang; GUO Xiang-Yun.Effects of the Reaction Conditions in Preparation of Si3N4 Nanowires[J]. Acta Phys. -Chim. Sin., 2007,23(10): 1503-1507
90. ZHANG Wei; WANG Shu-Liang; MA Yun-Qing; WANG Cui-Ping; LIU Xing-Jun.Influence of Interface Diffusion between Al Substrate and TiO2 Filmon Photocatalytic Activity[J]. Acta Phys. -Chim. Sin., 2007,23(09): 1347-1352
91. WANG Ting; JIANG Xin; LI Xi.Preparation of TiO2 Nanoparticles on Surface of Different Supports by Adsorption Phase Reaction Technique[J]. Acta Phys. -Chim. Sin., 2007,23(09): 1375-1380
92. HUANG Dong-Sheng; ZENG Ren-Jie; CHEN Chao-Feng; LI Yu-Hua.Hydrophilicity of TiO2 Thin Films Codoped with Iron and Nitrogen[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1037-1041
93. ZHAO Meng; WANG Jin-Xing; FENG Cai-Hui; ZOU Bo; CHEN Cheng; WANG Zhu-Yi; WU Feng-Qing; ZOU Le-Hui.Preparation and Gas Sensing Properties to Formaldehyde of TiO2/Ag2O Nanocrystalline[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1003-1006
94. CHEN Jian; HUANG Zheng-Ren; DONG Shao-Ming; JIANG Dong-Liang.Adsorption of Polyethylene Glycol on Silicon Carbide Measured by Thermal Gravimetric and Differential Thermal Analysis[J]. Acta Phys. -Chim. Sin., 2007,23(06): 926-928
95. LI Hong-Jian; CHEN Gang; LI Zhong-Hua; ZHOU Chao.Synthesis and Photocatalytic Decomposition of Water under Visible Light Irradiation of La2Ti2-xCoxO7 with Pyrochlore Structure[J]. Acta Phys. -Chim. Sin., 2007,23(05): 761-764
96. WU Lun-Peng; ZHAO Lian-Hua; ZHANG Hai-Ming; ZHAO Qing-Nan.Effects of the Adsorption of Oxygen on the Photocatalytic Activity of TiO2 Films Using PhotocurrentMethod[J]. Acta Phys. -Chim. Sin., 2007,23(05): 765-768
97. ZHANG Xiao-Fei; HU Rui-Sheng; GAO Guan-Jun; MENG He; SU Hai-Quan.Influence of Two Complexants on Structure and Performance of Ce-Sn-O Complex Oxides[J]. Acta Phys. -Chim. Sin., 2007,23(05): 659-663
98. WANG Huan-Ping; ZHANG Qi-Long; YANG Hui; SUN Hui-Ping.Synthesis and Microwave Dielectric Properties of (Ca1-xMgx)SiO3 Ceramic by Sol-Gel Process[J]. Acta Phys. -Chim. Sin., 2007,23(04): 609-613
99. ZHOU Hong-Wei;LI Huai-Xiang;JIANG Zheng-Wei;ZUO Xiang-Qing.Treatment of ZnS:Mn Phosphors by Partial Sublimation of SnO2:Sb Xerogel[J]. Acta Phys. -Chim. Sin., 2007,23(01): 88-91
100. QIAO Bin;TANG Zi-Long;ZHANG Zhong-Tai;CHEN Lei.Photoluminescent and Electroluminescent Characteristics of ZnGa2O4:Cr3+ Red Phosphor[J]. Acta Phys. -Chim. Sin., 2006,22(10): 1291-1295
101. FENG Chun-Bo;DU Zhi-Ping;Zhao Yong-Hong;TAI Xiu-Mei;LI Qiu-Xiao .Photocatalytic Activity of Au Modified Nano-TiO2 for NPE-10 Degradation[J]. Acta Phys. -Chim. Sin., 2006,22(08): 953-957
102. GUAN Hong-Bo;WANG Pei;WANG Hui;ZHAO Bi-Ying;ZHU Yue-Xiang;XIE You-Chang.Preparation of Nanometer Magnesia with High Surface Area and Study on the Influencing Factors of the Preparation Process[J]. Acta Phys. -Chim. Sin., 2006,22(07): 804-808
103. LIU Yi-An;XUE Cheng-Shan;ZHUANG Hui-Zhao;ZHANG Xiao-Kai;TIAN De-Heng;WU Yu-Xin;SUN Li-Li;AI Yu-Jie;WANG Fu-Xue.Structure and Synthesis of GaN Powder by Sol-Gel Method[J]. Acta Phys. -Chim. Sin., 2006,22(06): 657-660
104. ZHANG Xue-Hong;TANG Xing-Hua;CHENG Xin-Sun.Synthesis and Application of Ce-doped Mesoporous TiO2[J]. Acta Phys. -Chim. Sin., 2006,22(05): 532-537
105. YE Qing; XU Bo-Qing.Textural and Structure Characterizations of Ce1-xMnxO2Prepared by Citric Acid Sol-Gel Method[J]. Acta Phys. -Chim. Sin., 2006,22(03): 345-349
106. YE Qing; WANG Rui-pu; XU Bo-qing.Structure and Oxygen Mobility of Ce1-xZrxO2 Prepared by Citric Acid Sol-gel Method[J]. Acta Phys. -Chim. Sin., 2006,22(01): 33-37
107. LIU Rui-quan; XIE Ya-hong; LI Zhi-jie; WANG Ji-de; SUN Yi-gang.Application of Proton Conductors (Ce0.8La0.2)1-xCaxO2-δ in Synthesis of Ammonia[J]. Acta Phys. -Chim. Sin., 2005,21(09): 967-970
108. PENG Feng; CHEN Shui-hui; ZHANG Lei; WANG Hong-juan; XIE Zhi-yong.Preparation of Visible-light Response Nano-sized ZnO Film and Its Photocatalytic Degradation to Methyl Orange[J]. Acta Phys. -Chim. Sin., 2005,21(08): 944-948
109. LI Li-chun; GUAN Jian-guo; CHENG Hai-bin; TAO Jian-qing.Preparation of Poly(ethylene glycol)-coated Carbonyl Iron Particles for Aqueous Magnetorheological Suspension[J]. Acta Phys. -Chim. Sin., 2005,21(07): 817-821
110. LI Yong-Xin; GUO Yu-Hua; JI Yong-Qiang.Catalytic Activity of M/(MgO)y(CeO2)1-y (M=Ni, Co, Cu) Catalysts for Methane Combustion[J]. Acta Phys. -Chim. Sin., 2005,21(05): 468-473
111. JING Li-Qiang; FU Hong-Gang; WANG De-Jun; WEI Xiao; SUN Jia-Zhong.Surface Photoinduced Charge Separation and Photocatalytic Activity of Sn Doped TiO2 Nanoparticles[J]. Acta Phys. -Chim. Sin., 2005,21(04): 378-382
112. GE Xiu-Tao;FANG Da-Ru;LIU Xing-Qin.The Preparation and Gas-sensing Properties of Ga2O3-NiO Complex Oxide by Sol-gel Method[J]. Acta Phys. -Chim. Sin., 2005,21(01): 10-15
113. YANG Xiao-Guang;DONG Peng;ZHOU Ya-Song;LIU Tao;ZHANG Jing;XIEYa-Ning;HU Tian-Dou.The Local Structure of Titania-Silica Composite Oxides[J]. Acta Phys. -Chim. Sin., 2005,21(01): 33-37
114. TIAN Na;CHEN Wei;SUN Shi-Gang.Spectroscopic Characterization and Electrocatalytic Properties of Core-Shell Au-Pt Nanoparticles[J]. Acta Phys. -Chim. Sin., 2005,21(01): 74-78
115. Zhou Xing-Fu; Zhao Jun-Feng; He Hui; Chu Dao-Bao.Electrochemical Dissolution of Tin in Ethylene Glycol Monomethyl Ether and Direct Hydrolysis of the Electrolyte for Preparation of Nano-sized SnO2[J]. Acta Phys. -Chim. Sin., 2004,20(12): 1472-1475
116. Wang Juan; Zhang Chang-Rui; Feng Jian.Modification of Nanoporous Silica Film by Trimethylchlorosilane[J]. Acta Phys. -Chim. Sin., 2004,20(12): 1399-1403
117. Zhang Shi-Cheng;Li Chun-He;Li Xing-Guo.Size Control and Characterization of ZnO Nanoparticles[J]. Acta Phys. -Chim. Sin., 2004,20(08S): 902-905
118. Liu Ying-Xin;Wei Zuo-Jun;Chen Ji-Xiang;Zhang Ji-Yan;Li Xin-Xue;Wei Xiong-Hui.Sol-gel Preparation,Characterization and Hydrogenation Property of Silica Supported Ni Catalyst[J]. Acta Phys. -Chim. Sin., 2004,20(07): 780-784
119. Wang Shu-Rong;Wu Shi-Hua;Shi Juan;Zheng Xiu-Cheng;Huang Wei-Ping.Preparation and Catalytic Activity of Au/SnO2 for Low-temperature CO Oxidation[J]. Acta Phys. -Chim. Sin., 2004,20(04): 428-431
120. Wang Hui;Zhang Xiu-Juan;Zhang Xiao-Hong;Wu Shi-Kang.The Preparation of Nano-sized Silica Gel Suspension and the Recognition of Transition Metal Cations[J]. Acta Phys. -Chim. Sin., 2004,20(03): 313-317
121. Zeng Li;Wang Chun-Ming;Wei Ji-Ying;Zhu Yue-Xiang;Xie You-Chang.Preparation and Characterization of CrOx/ZrO2 with High Thermal Stability and High Specific Surface Area[J]. Acta Phys. -Chim. Sin., 2004,20(03): 251-255
122. Li You-Ji;Cao Feng;Tian Hong-Xian;Li Xiao-Dong;Yu Yu-Xi.The Preparation and Properties of High Temperature Resistant SiC(Al) Fibers[J]. Acta Phys. -Chim. Sin., 2003,19(11): 1039-1043
123. He Chong-Heng;Wang Ren.The Properties of Pd Catalysts Prepared by Sol-gel Method[J]. Acta Phys. -Chim. Sin., 2003,19(10): 952-956
124. Zhao Yong-Xiang;Qin Xiao-Qin;Hou Xi-Cai;Xu Xian-Lun;Liu Dian-Sheng.Preparation,Characterization and Properties of Selective Hydrogenation on Ni-based Catalysts[J]. Acta Phys. -Chim. Sin., 2003,19(05): 450-454
125. Zhang Min;Jin Zhen-Sheng;Wang Shou-Bin;Zhang Shun-Li;Zhang Zhi-Jun.The Photocatalytic Enhancement Effect of CO on Pd/TiO2[J]. Acta Phys. -Chim. Sin., 2003,19(02): 100-104
126. Zhang Wen-Hua;Peng Jiang-Jie;Ma Yun-Sheng;Hao Li-Qing;Zhuang Shu-Xian.Catalytic Reduction of SO2 by CO on Sulfided CoMo/ Al2O3-TiO2 Catalysts[J]. Acta Phys. -Chim. Sin., 2002,18(10): 901-906
127. Zhou Xing-Fu;Han Ai-Jie;Chu Dao-Bao;Lin Chang-Jian;Tian Zhong-Qun.Preparation of Nanocrystalline NiO by Electrochemical Dissolution of Nickel[J]. Acta Phys. -Chim. Sin., 2002,18(07): 613-616
128. Zhao Zhuan-Qing;Yao Su-Wei;Zhang Wei-Guo;Gong Zheng-Lie.Preparation and Photoelectrochemical Performance of Photoelectrode of TiO2 Film on Nickel[J]. Acta Phys. -Chim. Sin., 2002,18(05): 473-476
129. Zhang Ye;Wu Dong;Sun Yu-Han;Peng Shao-Yi.Synthesis and Properties of Hydrophobic & Antireflective Silica Coating[J]. Acta Phys. -Chim. Sin., 2002,18(04): 355-358
130. Zhang Jun-Ling;Ren Jie;Chen Jian-Gang;Sun Yu-Han.Effect of Manganese Promoter on the Performance of Co/Al2O3 Catalysts for FischerTropsch Synthesis[J]. Acta Phys. -Chim. Sin., 2002,18(03): 260-263
131. Ma Jian-Hua;Wu Guang-Ming;Cheng Yin-Bing;Sun Qi;Wang Jun-Ling;Shen Jun;Wang Jue.Preparation of Hydrophobic Optical Silica Thin Film with Sol-gel Method[J]. Acta Phys. -Chim. Sin., 2001,17(12): 1112-1116
132. Liu Zhen-Lin;Meng Ming;Fu Yi-Lu;Jiang Ming;Hu Tian-Dou;Xie Ya-Ning;Liu Tao.Structure Characterization of γ-Mo2N and Mo Nitrides Supported on Zeolites[J]. Acta Phys. -Chim. Sin., 2001,17(07): 631-635
133. Zou Ling;Wu Xue-Dong;Chen Hai-Gang;Wang Da-Pu.Structural Characterization and Formation Mechanism of SurfaceModified Titanium Dioxide Nanoparticles[J]. Acta Phys. -Chim. Sin., 2001,17(04): 305-309
134. Yu Jia-Guo;Zhao Xiu-Jian;Chen Wen-Mei;Lin Li;Zhang Ai-Li.Photocatalytic Activity and Hydrophilic Property of TiO2/SiO2 Composite Nanometer Thin Films[J]. Acta Phys. -Chim. Sin., 2001,17(03): 261-264
135. Shui Miao;Yue Lin-Hai;Xu Zhe-De.Photocatalytic Activity of Iron Doping TiO2 Prepared by Several Methods[J]. Acta Phys. -Chim. Sin., 2001,17(03): 282-285
136. Zhang Yu-Hong;Xiong Guo-Xing;Yang Wei-Shen;Fu Xian-Zhi.Preparation of MxOy-TiO2 Photocatalysts by Sol-gel Method[J]. Acta Phys. -Chim. Sin., 2001,17(03): 273-277
137. Wu Hong-Ying;Wang Xi-Gui;Xie Da-Tao;Weng Shi-Fu;Wu Jin-Guang.Structure and Luminescence Properties of Tb-doped Sibased Light-emitting[J]. Acta Phys. -Chim. Sin., 2001,17(01): 53-58
138. Yu Jia-Guo, Zhao Xiu-Jian, Zhao Qing-Nan.Preparation and Characterization of TiO2 Nnometer Thin Films by Sol-gel Process[J]. Acta Phys. -Chim. Sin., 2000,16(09): 792-797
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140. Bian Guo-Zhu, Han Bo, Fu Yi-Lu.Sol-gel Method Preparation and Characterization of NiMoO4 Ultrafine Particle Catalyst[J]. Acta Phys. -Chim. Sin., 1999,15(11): 1001-1004
141. Sun Yan-Hua, Shen Yue-Nian, Jia Mei-Lin, Hu Rui-Sheng.The Effects of Support on Loaded Combustion Catalyst of La0.8Sr0.2MnO3[J]. Acta Phys. -Chim. Sin., 1999,15(08): 721-725
142. Zhang Yu-Hong, Xiong Guo-Xing, Sheng Shi-Shan, Liu Sheng-Lin, Yang Wei-Shen.Interaction of NiO with γ-Al2O3 Supporter of NiO/γ-Al2O3 Catalysts[J]. Acta Phys. -Chim. Sin., 1999,15(08): 735-741
143. Chen Tong, Li Wen-Zhao, Yu Chun-Ying.Investigation of the Interaction between NiO and Support,γ-Al2O3,for Oxidative Dehydrogenation of Ethane[J]. Acta Phys. -Chim. Sin., 1999,15(07): 613-618
144. Gan Li-Hua, Li Guang-Ming, Yue Tian-Yi, Zhang Ming, Wu Jian-Wen, Chen Long-Wu.Preparation of Fe2O3-SiO2 Aerogels by Supercritical Drying Technique[J]. Acta Phys. -Chim. Sin., 1999,15(07): 588-592
145. Zeng Jian-Qing, Zhang Jing-Cheng, Zhong Bing.Monte Carlo Simulation of CO Oxidation Reaction on Fractal Surface[J]. Acta Phys. -Chim. Sin., 1999,15(06): 555-559
146. Liu Ying-Jun, Zhang Ji-Jun, Li Neng, Lin Bing-Xiong.The Effect of CO2 on Catalytic Activity of Cu-Ce-O Complex Oxides for CO Oxidation[J]. Acta Phys. -Chim. Sin., 1999,15(02): 97-100
147. Zhang Ji-Jun, Liu Ying-Jun, Li Neng, Lin Bing-Xiong.Synergistic Effect between CuO and CeO2 for CO Oxidation[J]. Acta Phys. -Chim. Sin., 1999,15(01): 15-21
148. Fu Jin-Kun, Liu Yue-Ying, Hu Rong-Zong, Zeng Jin-Long, Xu Pian-Pian, Lin Zhong-Yu, Yao Bing-Xin, Weng Cheng-Zhou.Preparation of Highly Dispersive Supported Gold Catalyst by Microbial Reduction Method[J]. Acta Phys. -Chim. Sin., 1998,14(09): 769-771
149. Ma Zhi, Qin Yong-Ning, Qi Xiao-Zhou, Liang Zhen-Cheng, He Fei.Studies on Prepartion and CO Oxidation Activity of LaSrBO4 Compound[J]. Acta Phys. -Chim. Sin., 1998,14(05): 453-457
150. Zhang Bin, Wan Hong, Zheng Yan-Ke, Ruan Qian, Wu Nian-Zu, Xie You-Chang, Tang You-Qi.Study of Dispersion of MoO3,NiO,ZnO onto Rutile with Low Surface Area[J]. Acta Phys. -Chim. Sin., 1998,14(05): 385-390
151. Zhang Bin, Wu Nian-Zu, Xie You-Chang, Tang You-Qi.Measurement of Dispersion Capacity of MoO3 on Low Specific Surface Support α-Al2O3[J]. Acta Phys. -Chim. Sin., 1998,14(04): 358-360
152. Zhou Ren-Xian, Chen Fang, Jiang Xiao-Yuan, Zheng Xiao-Ming.The Dispersed States of Manganese Species on Mn-O/ZrO2 Catalysts and its Influents on the Catalytic Performance[J]. Acta Phys. -Chim. Sin., 1998,14(02): 178-180
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154. Hou Xiang-Lin,Gao Yin-Ben,Chen Song-Ying.Temperature-Programmed Sulfiding Studies of Cu-based H2S Sorbents[J]. Acta Phys. -Chim. Sin., 1997,13(11): 1044-1048
155. Dai Chang-Hong,Liu Su-Lan,Zhang Xian-Peng.Microwave Synthesis of SiC Nanometer Whiskers[J]. Acta Phys. -Chim. Sin., 1997,13(04): 380-384
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158. Kuang Wen-Xing,Fan Yi-Ning,Chen Kai-Dong,Wang Jing-Lei,Chen Yi.Preparation of Fe2(MoO4)3 Ultrafine Particle Catalyst[J]. Acta Phys. -Chim. Sin., 1997,13(01): 86-88
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160. Zheng Hong-He,Zhang Qing-Zhi,Wang Jian-Ji,Wang Zheng-Yu,Mikio konno,Shozaburo Sa.Solvent Effects on Sol-gel Transition of Sodium Alginate Solutions[J]. Acta Phys. -Chim. Sin., 1996,12(07): 604-608
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162. Wang Wen-Tao,Zhong Bang-Ke.The Preparation and Characterization of Alumina Membranes Supported by Porous Titanium Plate[J]. Acta Phys. -Chim. Sin., 1996,12(01): 85-90
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168. Bao Ding-Hua; Wang Shi-Min; Gu Hao-Shuang; Zhao Jian-Hong; Huang Gui-Yu; Kuang An-Xiang.Highly-Oriented K(Ta,Nb)O3 Thin Film Derived by Sol-Gel Process[J]. Acta Phys. -Chim. Sin., 1993,9(04): 450-451
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