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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2007,Vol.23>> Issue(06)>> 835-840     doi: 10.3866/PKU.WHXB20070608         中文摘要
Glow Discharge Plasma Electrolysis of Methanol Solutions
YAN Zong-Cheng; CHEN Li; WANG Hong-Lin

Guangdong Provincial Laboratory of Green Chemical Technology, School of Chemical and Energy Engineering, South China University of Technology, Guangzhou 510640, P. R. China

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Non-faradic phenomena were found during the glow discharge plasma electrolysis of methanol solution, and the main products of the reactions induced by the glow discharge plasmas were hydrogen, formaldehyde, monoxide, methane, ethane, propane, sym-trioxane, and water. The chemical yields were affected by the polarity of the glow discharge plasma and supporting electrolytes of the solutions. The gas yield of the anodic glow discharge electrolysis of methanol was 55.90 mol/(mol electrons) when the discharge voltage across the circuit was 700 V and the conductivity of the solution was 11.40 mS·cm-1. The gas yield of the cathodic glow discharge was 707.90 mol/(mol electrons), 12.66 times of the anodic glow discharge gas yield, under the same conditions. The hydrogen concentration in the emission gas of the glow discharge electrolysis was higher than 86% (molar fraction). The decomposition of methanol molecules induced by the glow discharge plasmas around discharge electrode was similar to those induced by corona plasmas and dielectric discharge plasmas. Non-faradic phenomena of the glow discharge electrolysis of the methanol solutions were stirred up by the accelerated electrons within the gas sheath around the discharge electrode. Neutral species and electrons excited the methanol molecules on the plasma-electrolyte interface during cathodic glow discharge, while positive ions and neutral species played a more important role to excite the methanol molecules on the plasma-electrolyte interface during anodic glow discharge. The reactions in the liquid phase near the plasma-solution interface were affected by the supporting electrolytes of the solutions.



Keywords: Methanol   Glow discharge electrolysis   Plasma   Plasma chemical reaction  
Received: 2006-11-10 Accepted: 2006-12-29 Publication Date (Web): 2007-04-26
Corresponding Authors: YAN Zong-Cheng Email: nevill_yan@126.com


Cite this article: YAN Zong-Cheng; CHEN Li; WANG Hong-Lin. Glow Discharge Plasma Electrolysis of Methanol Solutions[J]. Acta Phys. -Chim. Sin., 2007,23 (06): 835-840.    doi: 10.3866/PKU.WHXB20070608
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91. WANG Jian-She, GUO Xun, SONG Cheng-Ying, WANG Liu-Cheng, ZHAO Jian-Hong, QIU Xin-Ping.Promoting Methanol Electro-Oxidation through Fabricating Pore Structure in Pt/CNTs Catalyst Layer by Dissolving Away Premixed La2O3 Particles[J]. Acta Phys. -Chim. Sin., 2009,25(04): 767-772
92. XU Lei; WU Shu-Jie; ZHANG Wen-Xiang; JIA Ming-Jun; LIU Gang.Vapour Phase ortho-Selective Alkylation of Phenol with Methanol over Fe-Zr Oxide Catalysts[J]. Acta Phys. -Chim. Sin., 2009,25(02): 242-246
93. LI Lai-Cai; WANG Yi-Wei; TIAN An-Min.Adsorption of Methanol on the Pt-Mo(111)/C Surface[J]. Acta Phys. -Chim. Sin., 2008,24(11): 2013-2018
94. YAO Hui-Jun; MO Dan; DUAN Jing-Lai; CHEN Yan-Feng; ZHANG Ling; LIU Jie; HOU Ming-Dong; SUN You-Mei.Preparation and Optical Properties of Gold Nanowire Arrays[J]. Acta Phys. -Chim. Sin., 2008,24(10): 1922-1926
95. CHANG Xiao-Tu, WANG Jian-Ming, SHAO Hai-Bo, WANG Jun-Bo, ZENG Xiao-Xu, ZHANG Jian-Qing, CAO Chu-Nan.Corrosion and Anodic Behaviors of Pure Aluminumin a Novel Alkaline Electrolyte[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1620-1624
96. ZHENG Bo; LI He-Xian; WANG Guo-Chang; LIU Kun; YUAN Wei; LI He; LIANG Bo.Supramolecular Complexation in Water-Methanol Mixtures[J]. Acta Phys. -Chim. Sin., 2008,24(08): 1503-1506
97. XU Hui-Yuan; CHU Wei; SHI Li-Min; ZHANG Hui; ZHOU Jun.Preparation of Copper-Cobalt Catalyst by Glow Discharge Plasma for Lower Alcohols Synthesis[J]. Acta Phys. -Chim. Sin., 2008,24(06): 1085-1089
98. ZHENG Gen-Wen; GONG Chun-Li; WEN Sheng; XIE Xiao-Lin.Preparation and Performances of Sulfonated Poly(ether imide) and Poly (ether sulfone) Blends for Proton Exchange Membrane[J]. Acta Phys. -Chim. Sin., 2008,24(05): 855-860
99. LIANG Ying; LIAO Dai-Wei.Effects of pH on the PtRu/C Catalyst Prepared by Microwave-assisted Ethylene Glycol Process[J]. Acta Phys. -Chim. Sin., 2008,24(02): 317-322
100. DENG Hui-Ning; WANG Yu-Xin.Preparation and Properties of Proton Conducting Composite Membranes from Sulfonated Poly(phthalazinone ether keton) and Phosphotungstic Acid[J]. Acta Phys. -Chim. Sin., 2007,23(08): 1235-1240
101. XU Hui-Yuan; CHU Wei; CI Zhi-Min.Effect of Glow Discharge Plasma on Copper-based Catalysts for Methanol Synthesis[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1042-1046
102. ZHENG Hai-Tao; LI Yong-Liang; LIANG Jian-Ying; SHEN Pei-Kang.Methanol Oxidation on Pd-based Electrocatalysts[J]. Acta Phys. -Chim. Sin., 2007,23(07): 993-996
103. LI Lan-Lan; WEI Zi-Dong; YAN Can; LUO Yi-Hui; YIN Guang-Zhi; SUN Cai-Xin.Methanol Oxidation on a Pt ElectrodeModified by Underpotential Deposition of Ru[J]. Acta Phys. -Chim. Sin., 2007,23(05): 723-727
104. ZHAO Wen-Xia; HU Man-Cheng; LI Shu-Ni; JIANG Yu-Cheng; ZHANG Xiao-Lei; HU Lei; CHEN Huai-Jun.The Solubility of Ternary SystemRbBr/CsBr-CH3OH/C2H5OH-H2O at Different Temperatures[J]. Acta Phys. -Chim. Sin., 2007,23(05): 695-700
105. WU Wei; CAO Jie-Ming; CHEN Yu; LU Tian-Hong.Preparation of High-alloying Pt-Ru/CMK-3 Catalysts in THF-H2O-EtOH Ternary Solution System[J]. Acta Phys. -Chim. Sin., 2007,23(04): 559-564
106. ZHANG Cheng-Gen;LI Wen-Zuo;HUANG Ming-Bao.Reaction of Methyl Alcohol with Thionyl Chloride in Solution[J]. Acta Phys. -Chim. Sin., 2007,23(03): 399-403
107. ZHANG Shu-Dong;ZHU Xiang-Jun;WANG Yan;KONG Xiang-He.Multiphoton Ionization Mass Spectrum of Methanol Clusters and Ab Initio Calculations[J]. Acta Phys. -Chim. Sin., 2007,23(03): 379-383
108. HU Xiao-Tu;WANG Yi;ZHU Tian-Le;JIANG Xue-Dong;LI Rui-Nian.Oxidation of Ammonium Sulfite in Aqueous Solutions with Streamer Plasmas[J]. Acta Phys. -Chim. Sin., 2007,23(03): 384-388
109. DENG Hui-Ning;WANG Yu-Xin .Sulfonated Poly(phthalazinones) Membranes For Direct Methanol Fuel Cell[J]. Acta Phys. -Chim. Sin., 2007,23(02): 187-191
110. HUANG Mian-Yan;CHEN Hua-Yan;GUO Jian-Zhao;WANG Zhi-Tao;XU Li;WANG Yu-Xin.Methanol Resistant Poly(Ether Sulfone)/Sulfonated Poly(Ether Ether Ketone) Blend Proton Exchange Membrane for DMFC[J]. Acta Phys. -Chim. Sin., 2007,23(01): 44-49
111. SHEN Pei-Kang;WANG Sheng-Long;HU Zhi-Yi;LI Yong-Liang;ZENG Rong;HUANG Yue-Qiang.Hydrogen Production by Alcohol Electrolysis[J]. Acta Phys. -Chim. Sin., 2007,23(01): 107-110
112. ZOU Ji-Jun;LIU Chang-Jun.Preparation of NiO/SrTiO3 with Cold Plasma Treatment for PhotocatalyticWater Splitting[J]. Acta Phys. -Chim. Sin., 2006,22(08): 926-931
113. ZHANG Xue-Hong;TANG Xing-Hua;CHENG Xin-Sun.Synthesis and Application of Ce-doped Mesoporous TiO2[J]. Acta Phys. -Chim. Sin., 2006,22(05): 532-537
114. CHEN Ling; WANG Xin-dong; GUO Min.The Effect of NdOx as Co-catalyst for the Electro-oxidation of Methanol on PtRu/C[J]. Acta Phys. -Chim. Sin., 2006,22(02): 141-145
115. CHEN Yu; TANG Ya-wen; Kong Ling-yong; LIU Chang-peng; XING Wei; LU Tianhong.Effect of Surface Modification Extent of Carbon Nanotubes on Electrocatalytic Performance of Carbon Nanotubes Supported Pt catalyst[J]. Acta Phys. -Chim. Sin., 2006,22(01): 119-123
116. LIU Jing;NIU Jin-Hai;XU Yong;ZHU Ai-Min;SUN Qi;NIE Long-Hui.Optical Emission Spectroscopy Diagnosis on Decomposition of NO in NO/N2 Mixtures in Dielectric Barrier Discharge Plasma[J]. Acta Phys. -Chim. Sin., 2005,21(12): 1352-1356
117. WANG Da-wang; MA Teng-cai; CUI Jin-hua.Methane Coupling in Atmospheric Pressure Glow Discharge Plasma with a Rotary Helix Electrode[J]. Acta Phys. -Chim. Sin., 2005,21(11): 1291-1294
118. WANG Zhen-bo; YIN Ge-ping; SHI Peng-fei.The Influence of Three Groups of Pt-Ru/C Catalyst’s Precursors on Its Performance for Direct Methanol Fuel Cell[J]. Acta Phys. -Chim. Sin., 2005,21(10): 1156-1160
119. WANG Sheng-gao; ZHAO Xiu-jian; HAN Jian-jun; WANG Jian-hua.Integration of Carbon Nanotubes Electrodes on Glass Substrate[J]. Acta Phys. -Chim. Sin., 2005,21(09): 1050-1054
120. ZHANG Wen-yu; DONG Qing-nian; ZHAO Ning; WEI Wei; SUN Yu-han.The Reaction Mechanism for the Synthesis of 1-methoxy-2-propanol on MgO Catalyst[J]. Acta Phys. -Chim. Sin., 2005,21(06): 653-657
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122. PEI Mei-Xiang; LIN He; SHANGGUAN Wen-Feng; HUANG Zhen.The Effects of Plasma on Simultaneously Catalytic Removal of NOx and Soot[J]. Acta Phys. -Chim. Sin., 2005,21(03): 255-260
123. JIA Yu-Xiang; GUO Xiang-Yun.Monte Carlo Simulation of Adsorption Process of CO and H2 in Supercritical Fluids[J]. Acta Phys. -Chim. Sin., 2005,21(03): 306-309
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127. Hu Ji-Ming;Zhang Jian-Qing;Zhang Jin-Tao;Cao Chu-Nan.Electrochemical Activities of IrO2 Electrodes in Small Organic Molecules Containing Aqueous Solutions[J]. Acta Phys. -Chim. Sin., 2004,20(07): 740-744
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129. Gao Li-Zhen;Zhang Xing-Tang;Dai Shu-Xi;Li Yun-Cai;Huang Ya-Bin;Du Zu-Liang;Li Tie-Jin.Preparation of PyDDP-modified Gold Nanoparticles and Mechanism for Red-shift in the Surface Plasma Resonance Absorption[J]. Acta Phys. -Chim. Sin., 2004,20(06): 647-650
130. Yun Hong;Chen Jian-Hua;Zhang Hui;Lin Jing-Dong;Chen Hong-Bo;Lin Chang-Jian.The Effects of ZrO2 on Cu-ZnO-ZrO2 Catalysts for Hydrogen Generation by Steam Reforming of Methanol[J]. Acta Phys. -Chim. Sin., 2004,20(05): 550-553
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137. Wang Sheng-Gao;Wang Jian-Hua;Wang Chuan-Xin;Ma Zhi-Bin;Man Wei-Dong.Self-bias Induced Aligned Growth of Carbon Nanotubes[J]. Acta Phys. -Chim. Sin., 2003,19(09): 864-866
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156. Deng Guo-Yang, Jes Henningsen.Quantitative Measurement of Adsorption of CH3OH on Commonly Used Mterials by Photoacoustic Method[J]. Acta Phys. -Chim. Sin., 1999,15(08): 764-768
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