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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2000,Vol.16>> Issue(03)>> 226-231     doi: 10.3866/PKU.WHXB20000307         中文摘要
Cu-Ni/V2O5-SiO2 Catalyst for the Direct Synthesis of Dimethyl Carbonate from Carbon Dioxide and Methanol
Zhong Shun-He, Li Han-Sehng, Wang Jian-Wei, Xiao Xiu-Fen
College of Chemical Engineering and Technology,Tianjin University,Tianjin 300072
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The surface complex support of V2O5-SiO2(VSiO) was prepared by the method of surface reaction modification. VSiO supported Cu-Ni bimetallic catalysts were made using isovolumic impregnation. Adsorption and reaction of CO2 and CH3OH on catalyst were characterized by IR, TPD, TPSR and micro-reactor techniques. The results show that three active sites exist on Cu-Ni/VSiO catalyst: metal site(Cu-Ni alloy, denoted M), Lewis acid site(Vn+)and Lewis basic site(V=O); horizontally adsorped CO2, formed by shearingly adsorbed CO2 on M in cooperation with the adjacent Vn+, can dissociate into M-CO and V=O at about 138 ℃and methanol dissociated into V-OCH3 and V-OH cooperated with Vn+ and adjacent V=O; the mainly reaction products of the reaction of CO2 and CH3OH on Cu-Ni/VSiO catalyst are DMC (with selectivity over 85%), CH2O, CO and H2O.



Keywords: Carbon dioxide   Methanol   Dimethyl carbonate   V2O5-SiO2 complex support   Binetallic catalyst   Surface reaction  
Received: 1999-06-24 Accepted: 1999-09-14 Publication Date (Web): 2000-03-15
Corresponding Authors: Zhong Shun-He Email:


Cite this article: Zhong Shun-He, Li Han-Sehng, Wang Jian-Wei, Xiao Xiu-Fen. Cu-Ni/V2O5-SiO2 Catalyst for the Direct Synthesis of Dimethyl Carbonate from Carbon Dioxide and Methanol[J]. Acta Phys. -Chim. Sin., 2000,16 (03): 226-231.    doi: 10.3866/PKU.WHXB20000307
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90. NI Zhe-Ming, MAO Jiang-Hong, PAN Guo-Xiang, XU Qian, LI Xiao-Nian.Mechanism of Palladium-Catalyzed Methanol Decomposition for Hydrogen Production[J]. Acta Phys. -Chim. Sin., 2009,25(05): 876-882
91. YANG Hong-Yan, GUO Pan-Pan, LI Wei-Shan.Electrodeposition Preparation and Activity of CO-Resistant Catalyst Pt-HxWO3 for Methanol Oxidation[J]. Acta Phys. -Chim. Sin., 2009,25(04): 719-723
92. WANG Jian-She, GUO Xun, SONG Cheng-Ying, WANG Liu-Cheng, ZHAO Jian-Hong, QIU Xin-Ping.Promoting Methanol Electro-Oxidation through Fabricating Pore Structure in Pt/CNTs Catalyst Layer by Dissolving Away Premixed La2O3 Particles[J]. Acta Phys. -Chim. Sin., 2009,25(04): 767-772
93. XU Lei; WU Shu-Jie; ZHANG Wen-Xiang; JIA Ming-Jun; LIU Gang.Vapour Phase ortho-Selective Alkylation of Phenol with Methanol over Fe-Zr Oxide Catalysts[J]. Acta Phys. -Chim. Sin., 2009,25(02): 242-246
94. LI Lai-Cai; WANG Yi-Wei; TIAN An-Min.Adsorption of Methanol on the Pt-Mo(111)/C Surface[J]. Acta Phys. -Chim. Sin., 2008,24(11): 2013-2018
95. CHANG Xiao-Tu, WANG Jian-Ming, SHAO Hai-Bo, WANG Jun-Bo, ZENG Xiao-Xu, ZHANG Jian-Qing, CAO Chu-Nan.Corrosion and Anodic Behaviors of Pure Aluminumin a Novel Alkaline Electrolyte[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1620-1624
96. DENG Wen-Ping, XU Gang, WAN Lei, LIU An-Wen, GAO Bo, DU Jun-He, HU Shui-Ming, CHEN Yang.Apparatus for High-Resolution Solid Hydrogen Matrix Isolation Spectroscopy and Its Application[J]. Acta Phys. -Chim. Sin., 2008,24(08): 1329-1334
97. ZHENG Bo; LI He-Xian; WANG Guo-Chang; LIU Kun; YUAN Wei; LI He; LIANG Bo.Supramolecular Complexation in Water-Methanol Mixtures[J]. Acta Phys. -Chim. Sin., 2008,24(08): 1503-1506
98. ZHENG Gen-Wen; GONG Chun-Li; WEN Sheng; XIE Xiao-Lin.Preparation and Performances of Sulfonated Poly(ether imide) and Poly (ether sulfone) Blends for Proton Exchange Membrane[J]. Acta Phys. -Chim. Sin., 2008,24(05): 855-860
99. LU Zhao-Ling; QIU Yu-Bing; GUO Xing-Peng.Effect of pH Value on the Adsorption Behavior and Inhibition Mechanism of Dodecylamine on Carbon Steel[J]. Acta Phys. -Chim. Sin., 2008,24(02): 243-249
100. LIANG Ying; LIAO Dai-Wei.Effects of pH on the PtRu/C Catalyst Prepared by Microwave-assisted Ethylene Glycol Process[J]. Acta Phys. -Chim. Sin., 2008,24(02): 317-322
101. DENG Hui-Ning; WANG Yu-Xin.Preparation and Properties of Proton Conducting Composite Membranes from Sulfonated Poly(phthalazinone ether keton) and Phosphotungstic Acid[J]. Acta Phys. -Chim. Sin., 2007,23(08): 1235-1240
102. XU Hui-Yuan; CHU Wei; CI Zhi-Min.Effect of Glow Discharge Plasma on Copper-based Catalysts for Methanol Synthesis[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1042-1046
103. ZHENG Hai-Tao; LI Yong-Liang; LIANG Jian-Ying; SHEN Pei-Kang.Methanol Oxidation on Pd-based Electrocatalysts[J]. Acta Phys. -Chim. Sin., 2007,23(07): 993-996
104. YUE Qiao-Hong; SHAO Xiao-Hong; CAO Da-Peng.Separation of Hydrogen and Carbon Dioxide in Activated Mesocarbon Microbeads with High Specific Surface[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1080-1084
105. YAN Zong-Cheng; CHEN Li; WANG Hong-Lin.Glow Discharge Plasma Electrolysis of Methanol Solutions[J]. Acta Phys. -Chim. Sin., 2007,23(06): 835-840
106. LI Lan-Lan; WEI Zi-Dong; YAN Can; LUO Yi-Hui; YIN Guang-Zhi; SUN Cai-Xin.Methanol Oxidation on a Pt ElectrodeModified by Underpotential Deposition of Ru[J]. Acta Phys. -Chim. Sin., 2007,23(05): 723-727
107. ZHAO Wen-Xia; HU Man-Cheng; LI Shu-Ni; JIANG Yu-Cheng; ZHANG Xiao-Lei; HU Lei; CHEN Huai-Jun.The Solubility of Ternary SystemRbBr/CsBr-CH3OH/C2H5OH-H2O at Different Temperatures[J]. Acta Phys. -Chim. Sin., 2007,23(05): 695-700
108. LIU De-Rong; XIONG Wei; YANG Chao-Fen; WANG Jin-Bo; CHEN Hua; LI RUI-Xiang; LI Xian-Jun.Asymmetric Hydrogenations of Acetophenone and Its Derivatives over RuRh/γ-Al2O3 Modified by (1S, 2S)-DPEN and PPh3[J]. Acta Phys. -Chim. Sin., 2007,23(04): 479-483
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