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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2000,Vol.16>> Issue(03)>> 207-213     doi: 10.3866/PKU.WHXB20000304         中文摘要
Crystal Structure and Photochemical Properties of r-1,c-2,t-3,t-4-1,3-bis(4-biphenyl)-2,4-di(4-pyridyl)cyclobutane
Zhang Wen-Qin, Zhang Zhi-Ming, Zheng Yan, Wang Shu-Li, Zhao Shu-Na
Department of Chemistry,Tianjin University,Tianjin 300072
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r-1,c-2, t-3, t-4-1,3-bis(4-biphenyl)-2,4-di(4-pyridyl)cyclobutane (II) was obtained in diluted sulfuric acid by photodimerization reaction. Its structure was determined by X-ray diffraction method. The crystal is monoclinic, space group is P21/n,with a=1.0038(2), b=1.8995(4), c=1.4647(3)nm, β=98.82(3)°, Z=4. The cyclobutane ring of II has puckered conformation. It was found that under short wave UV light II is easy to be photolyzed to reproduce its monomer trans-1-(4-biphenyl)-2-(4-pyridyl)ethene (E-I),and then the new formed E-I transforms to its cis-isomer(Z-I) through trans-cis isomerization. Finally, the equilibrium of isomerization establishes between E-I and Z-I. Photolysis of II or E-I will form the same isomerization mixture.



Keywords: Crystal strueture   Photodimerization   Trans-cis isomerization  
Received: 1999-06-03 Accepted: 1999-07-26 Publication Date (Web): 2000-03-15
Corresponding Authors: Zhang Wen-Qin Email:


Cite this article: Zhang Wen-Qin, Zhang Zhi-Ming, Zheng Yan, Wang Shu-Li, Zhao Shu-Na. Crystal Structure and Photochemical Properties of r-1,c-2,t-3,t-4-1,3-bis(4-biphenyl)-2,4-di(4-pyridyl)cyclobutane[J]. Acta Phys. -Chim. Sin., 2000,16 (03): 207-213.    doi: 10.3866/PKU.WHXB20000304
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