ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2002,Vol.18>> Issue(08)>> 754-758     doi: 10.3866/PKU.WHXB20020817         中文摘要
Study of SPS and XPS of Pd/ZnO and Ag/ZnO Composite Nanoparticles
Jing Li-Qiang;Sun Xiao-Jun;Cai Wei-Min;Zheng Da-Fang;Xu Yue;Xu Zhao-Peng;Xu Zi-Li;Du Yao-Guo
Department of Environmental Sciences and Engineering, Harbin Institute of Technology, Harbin 150001;Analysis Testing and Experimental Center;Department of Environmental Sciences and Engineering, Jilin University, Changchun 130021
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ZnO nanoparticles were prepared by calcining the precursor, zinc carbonate hydroxide,and Pd/ZnO and Ag/ZnO composite nanoparticles with the noble metal content of 0.5%(mass fraction) were obtained by photoreduction method. The as-prepared samples were also characterized by the XRD,TEM,XPS and SPS techniques, respectively. The results showed that the deposited noble metal of both Pd and Ag existed as the form of atomic clusters,and the possible reasons of forming the atomic clusters of noble metal on the surface of ZnO nanoparticles were primarily discussed. The intensity of SPS responses of ZnO nanoparticle remarkably decreased by depositing the appropriate noble metal on its surface. Moreover, Pd/ZnO and Ag/ZnO composite nanoparticles exhibited higher photocatalytic activity than ZnO nanoparticles in the experiment of photocatalytic oxidation of gas phase n-heptane. The essential reasons why the photocatalytic activity of ZnO nanoparticles improved by depositing noble metal Pd or Ag on its surface were also further discussed. In addition, the point was put forward that the photocatalytic activity of nanoparticle could be primarily evaluated by its SPS response, i.e., the weaker the SPS responseis, the higher the photoactivity.

Keywords: ZnO   Composite nanoparticles   SPS   XPS   Noble metal   Photocatalytic activity  
Received: 2001-12-28 Accepted: 2002-03-04 Publication Date (Web): 2002-08-15
Corresponding Authors: Jing Li-Qiang Email:

Cite this article: Jing Li-Qiang;Sun Xiao-Jun;Cai Wei-Min;Zheng Da-Fang;Xu Yue;Xu Zhao-Peng;Xu Zi-Li;Du Yao-Guo. Study of SPS and XPS of Pd/ZnO and Ag/ZnO Composite Nanoparticles[J]. Acta Phys. -Chim. Sin., 2002,18 (08): 754-758.    doi: 10.3866/PKU.WHXB20020817
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95. Zhang Qi;Li Xin-Jun;Li Fang-Bai;Chang Jie.Investigation on Visible -light Activity of WOx/TiO2 Photocatalyst[J]. Acta Phys. -Chim. Sin., 2004,20(05): 507-511
96. Li Ling-Xia;Wu Xia-Wan;Wang Hong-Ru;Zhang Zhi-Ping;Yu Hao-Ming.Analysis on Quantitative Relationship between Dielectric Properties and Phase Structure of High Frequency Dielectric System[J]. Acta Phys. -Chim. Sin., 2004,20(04): 396-399
97. Zhang Jin-Long;Zhao Wen-Juan;Chen Hai-Jun;Xu Hua-Sheng;Chen Ai-Ping;Anpo Masa-Kazu.Study of Loaded Photocatalysts by Precious Metals on the Photocatalytic Reactivity[J]. Acta Phys. -Chim. Sin., 2004,20(04): 424-427
98. Wu ShuXin;Ma Zhi;Qin Yong-Ning;Qi Xiao-Zhou;Liang Zhen-Cheng.Photocatalytic Redox Activity of Doped Nanocrystalline TiO2[J]. Acta Phys. -Chim. Sin., 2004,20(02): 138-143
99. Qiu Li-Mei;Jiang Yong;Liu Fen;Zhao Liang-Zhong.XPS Investigation of the Spherulite Surface for Poly(ε-caprolactone)/poly(vinyl chloride)[J]. Acta Phys. -Chim. Sin., 2004,20(01): 47-49
100. Zhao Li-Yan;Wang Xue-Kai;Guo Yu-Guo;Wu Nian-Zu;Xie You-Chang.Adsorption of Methylene Blue on the Muscovite[J]. Acta Phys. -Chim. Sin., 2003,19(10): 896-901
101. Wu Shu-Xin;Ma Zhi;Qin Yong-Ning;He Fei;Jia Li-Shan;Zhang Yan-Jun.XPS Study of Copper Doping TiO2 Photocatalyst[J]. Acta Phys. -Chim. Sin., 2003,19(10): 967-969
102. Guo Min;Diao Peng;Ren Yan-Jie;Wang Bin;Cai Sheng-Min.Preparation and Characterization of Highly Oriented ZnO Single Crystal Submicrorod Arrays[J]. Acta Phys. -Chim. Sin., 2003,19(05): 478-480
103. Wang Bin;Gao Fei;He Bin;Zhang Dong-Bai;Cheng Hu-Min;Ma Ji-Ming;Qi Li-Min.Optic Property of CdS/TiO2 Composite Nanoparticle Prepared in the Reversed Microemulsion[J]. Acta Phys. -Chim. Sin., 2003,19(01): 21-24
104. Qiu Li-Mei;Liu Fen;Zhao Liang-Zhong.Synthesis of K-Pb-Tl-O Complex Oxides and XPS Study on Their Electronic Structure[J]. Acta Phys. -Chim. Sin., 2002,18(07): 633-635
105. Gong Hai-Ning;Shen Hua;Huang Hui-Zhong;Wu Nian-Zu.Preliminary Exploration of Touggard′s Method Used for the Background[J]. Acta Phys. -Chim. Sin., 2002,18(04): 326-331
106. Yang Yong-Lai;Xu Heng-Yong;Li Wen-Zhao.Promotion Effects of CeO2 and Pd on Ni/γ-Al2O3 Catalyst[J]. Acta Phys. -Chim. Sin., 2002,18(04): 321-325
107. Xi Jing-Yu;Wang Zhi-Fei;Wang Wei-Ping;Lü Gong-Xuan.In-situ XPS Study for Reaction Mechanism of Methanol Decomposition over Cu-Ni/Zn Catalyst[J]. Acta Phys. -Chim. Sin., 2002,18(01): 82-86
108. Zhao Liang-Zhong;Liu Fen;Li Jian-Zhang;Xu Yong-Tong.XPS Study of Three Dimensional C/SiC Composites[J]. Acta Phys. -Chim. Sin., 2001,17(09): 802-805
109. Li Chun-Yi;Shan Hong-Hong;Zhao Bo-Yi;Yang Chao-He;Zhang Jian-Fang.USY/ZnO/Al2O3 Catalyst for Gasoline Desulfurization via Catalytic Cracking[J]. Acta Phys. -Chim. Sin., 2001,17(07): 641-644
110. Lin Zhong-Yu;Fu Jin-Kun;Wu Jian-Ming;Liu Yue-Ying;Cheng Hu.Preliminary Study on the Mechanism of Nonenzymatic Bioreduction of Precious Metal Ions[J]. Acta Phys. -Chim. Sin., 2001,17(05): 477-480
111. Yu Jia-Guo;Zhao Xiu-Jian;Chen Wen-Mei;Lin Li;Zhang Ai-Li.Photocatalytic Activity and Hydrophilic Property of TiO2/SiO2 Composite Nanometer Thin Films[J]. Acta Phys. -Chim. Sin., 2001,17(03): 261-264
112. Liu Jin-Cui;Mu Shao-Lin;Li Yong-Fang.Growth of Poly(methylene blue) Film and Properties of the Film[J]. Acta Phys. -Chim. Sin., 2001,17(03): 229-233
113. Xia Sheng-Qing;Chen Sheng-Pei;Sun Shi-Gang.The Preparation and Characterization of Platinum Based PbSb Surface Alloy Electrode[J]. Acta Phys. -Chim. Sin., 2001,17(02): 134-139
114. Ren Si-Li;Yang Sheng-Rong;Xue Qun-Ji.Perfluorodecanoic Acid Ultrathin Film on Single Crystal Silicon Substrate Coated with Polyethyleneimine[J]. Acta Phys. -Chim. Sin., 2001,17(02): 97-100
115. Zhang Yu-Zhi;Kuai Su-Lan;Huang Yin-Song;Wang Zhong-Chun;Hu Xing-Fang.X-ray Photoelectron Spectroscopic Study on Electrochromic Molybdenum Oxide Films[J]. Acta Phys. -Chim. Sin., 2001,17(01): 79-82
116. Li Wei-Hua, Hao Yan-Zhong, Qiao Xue-Bin, Zhang Li, Yang Mai-Zhi, Cai Sheng-Min.Photoelectrochemical Studies on the Nanostructured ZnO/Dye/PPy Electrode[J]. Acta Phys. -Chim. Sin., 1999,15(10): 905-910
117. Xu Bin, Cheng Hu-Min, Wang Yan-Qin, Ma Ji-Ming.Preparation and Properties of Nanosized Composite Particle SnO2/CdS[J]. Acta Phys. -Chim. Sin., 1999,15(10): 925-929
118. Deng Zong-Wu, Guo Wei-Min, Liu Huan-Ming, Cao Li-Li.Band Bending of Cleaved GaAs(100) Surface[J]. Acta Phys. -Chim. Sin., 1999,15(06): 528-532
119. Zhao Liang-Zhong, Wang Rui-Lan, Xu Hong-Yu, Li Hong-Cheng, Liu Shi-Hong.XPS Studies of Superconducting Gd-Ba-Cu-O Films[J]. Acta Phys. -Chim. Sin., 1999,15(05): 398-402
120. Deng Zong-Wu, Guo Wei-Min, Liu Huan-Ming, Cao Li-Li.Band Bending of Cleaved InP(110) Surface[J]. Acta Phys. -Chim. Sin., 1999,15(04): 303-307
121. Yang Ru, Hu Tian-Dou, Liu Tao, Xiang Hong-Wei, Zhong Bing, Xu Yao, Wu Dong.Characterization of CuO-BaO/SiO2 Catalysts Structure[J]. Acta Phys. -Chim. Sin., 1998,14(07): 590-596
122. Zhang Bin, Wan Hong, Zheng Yan-Ke, Ruan Qian, Wu Nian-Zu, Xie You-Chang, Tang You-Qi.Study of Dispersion of MoO3,NiO,ZnO onto Rutile with Low Surface Area[J]. Acta Phys. -Chim. Sin., 1998,14(05): 385-390
123. Ouyang Jian-Ming, Tai Zi-Hou, Tang Wen-Xia.XPS Study of LB Films of Amphiphilic Ligand on Surface of the Subphase Containing Metal Ions[J]. Acta Phys. -Chim. Sin., 1998,14(01): 84-87
124. Xiao Zhong-Dang, Huang Dan, Gu Jian-Hua, Lu Zu-Hong.X-ray Photoelectron Spectroscopy Study of the Deposition of TiO2 Thin Films on Self-assembly Monolayer[J]. Acta Phys. -Chim. Sin., 1998,14(01): 57-62
125. Lv Xin,Xu Xin,Wang Nan-Qin,Liao Meng-Sheng,Zhang Qian-Er.Cluster Modelling of CO Chemisorption on Cu/ZnO[J]. Acta Phys. -Chim. Sin., 1997,13(11): 1005-1009
126. Tan Hai-Shu,Chen Li-Chun,Yang Xiao-Hui,Wang Xiang-Jun,Xie Hong-Quan,Gao Guang-Hu.Thin Film Light-emitting Diodes with Organic/Inorganic Heterostructure[J]. Acta Phys. -Chim. Sin., 1997,13(10): 942-945
127. Zhang Guo-Qing,Liu Bing,Yao Su-Wei,Guo He-Tong,He Fei,Gong Zheng-Lie.XPS Evidence for the Diffusion and Formation of Metal Silicide at Atmospheric Temperature on the Interface of NiPd/Si[J]. Acta Phys. -Chim. Sin., 1997,13(02): 164-168
128. Li Xing-Lin,She Yi-Min,Guo Jun,Jiang Da-Zhen.XPS Study of the Interaction between Layers and Pillars of Layered Double Hydroxides Pillared with Heteroplyanion(II)[J]. Acta Phys. -Chim. Sin., 1996,12(10): 929-932
129. Wu Zheng-Hua,Qiu Si-Chou,Huang Han-Yao,He Hua-Hui.Study on the Characteristics and Mechanism of Electrochromism of NiOxHy Thin Film[J]. Acta Phys. -Chim. Sin., 1996,12(07): 615-620
130. Zhang Han-Chang,Zuo Xiao-Bing,Ji Ming-Rong,Wu Shou-Guo.Properties of Anodically Oxidative Glass Carbon Electrodes(GCE) in Strong Alkaline solutions[J]. Acta Phys. -Chim. Sin., 1996,12(07): 649-653
131. Luo Sheng-Cheng,Gui Lin-Lin,Tang You-Qi.The Characterisation of the Adsorption of H2S on MoO3/TiO2-Al2O3 by XPS[J]. Acta Phys. -Chim. Sin., 1996,12(04): 341-345
132. Fu Xian-Zhi,Huang Hui-Zhong,Zhu Lin,Luo Sheng-Cheng,Gui Lin-Lin.Investigation of Sulfidation Processes for Hydrotreating Catalysts by[J]. Acta Phys. -Chim. Sin., 1995,11(12): 1071-1076
133. Zhang Da-Heng.Adsorption and Desorption of Oxygen on the Surface of Polycrystalline ZnO Films Deposited by r.f.Sputtering[J]. Acta Phys. -Chim. Sin., 1995,11(09): 791-795
134. Yang Xiang-Guang,Liu She-Tian,Ye Xing-Kai,Wu Yue,Sheng Shi-Shan,Xiong Guo-Xing.X-Ray Photoelectron Spectroscopy Study of LaMn1-xFexO3(x=0-1) Oxides[J]. Acta Phys. -Chim. Sin., 1995,11(08): 681-687
135. Yu Bao-Long,Zhang Gui-Lan,Tang Guo-Qing,Wu Xiao-Chun,Chen Wen-Ju.Electronic Spin Resonance Properties of ZnO Nanocrystallite[J]. Acta Phys. -Chim. Sin., 1995,11(07): 587-589
136. Chen Si-Hai,Ren Xin-Min.The Prepartion of ZnO-Ag Core-shell Nanoparticle:Absorption and Fluorescence Spectrs[J]. Acta Phys. -Chim. Sin., 1995,11(04): 365-368
137. Xiong Guo-Xing, Xia Xin-Rui, Chen Heng-Rong, Guo Xie-Xian.Synergetic Effect between NaCl and B2O3 in Modified FeOχ Catalysts[J]. Acta Phys. -Chim. Sin., 1994,10(11): 971-977
138. Chen Xue-An, Chen De-Jun, Xu Cui-Ying, Zhang Jin-Biao, Zhu Dao-Ben, Yang De-Liang.The Effect of Cu2S Addition on the Superconductivity of Bi-Pb-Sr-Ca-Cu-O System[J]. Acta Phys. -Chim. Sin., 1994,10(08): 704-709
139. Zhang Rui-Feng, Li Xing-Lin, Liu She-Tian, Yu Zuo-Long, Wu Yue.XPS Study of the Oxygen State in LaMnyCo1-yO3 Catalysts[J]. Acta Phys. -Chim. Sin., 1994,10(08): 720-723
140. Zhai Run-Sheng, Cai Mao-Sheng, D.M.Kolb.XPS Evidence of Sulfate Anion Adsorption on Emersed Pt(111) in H2SO4 Solution[J]. Acta Phys. -Chim. Sin., 1994,10(08): 741-743
141. Yan Jian-Hua; Liu Ying-Jun; Gui Lin-Lin; Tang You-Qi.The Surface Structure of WO3/Titania-alumina System[J]. Acta Phys. -Chim. Sin., 1993,9(01): 13-20
142. Wu Hui-Huang; Wu Bao-Zhang; Zhou Shao-Min.Electrochemistry and XPS of Palladium Oxides[J]. Acta Phys. -Chim. Sin., 1992,8(04): 519-522
143. Zhao Liang-Zhong; Guo Zhong-Cheng; Liang Zhen-Hua; Hu Yu-Xiu; Liu Han-Fan.Variations in the Elemental Concentration in Surface Region of the YBCO Films and Interactions of the Films with Substrate in Heating Process Studied by Angular Deprndent XPS[J]. Acta Phys. -Chim. Sin., 1991,7(03): 305-310
144. Zhu Wen-Xiang; Zhao Ji-Zhou; Yang Rui-Na; Huang Hui-Zhong.Investigation on XPS of Lanthanide Complexes of Crown Ethers[J]. Acta Phys. -Chim. Sin., 1991,7(03): 371-374
145. Wang Dian-Xun; Li Er-Cheng; Xu Guang-Zhi; Zhang Lun.Studies of XPS Satellite Peaks and its Valence Band Spectra of the Pyridoygen Complexes of Rare Earth Decahydro-Decaborate[J]. Acta Phys. -Chim. Sin., 1991,7(02): 234-237
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