Acta Phys. -Chim. Sin. ›› 1992, Vol. 8 ›› Issue (02): 266-269.doi: 10.3866/PKU.WHXB19920225

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In-Situ Raman Spectroscopic Investigation of the SO2Cl2 Electroreduction Using Micro-Raman Electrolytic Cell

Zhong Fa-Ping; Yang Han-Xi; Xu Zhi-San; Zha Quan-Xing   

  1. Department of Chemistry, Wuhan University, Wuhan 430072
  • Received:1990-11-02 Revised:1991-05-06 Published:1992-04-15
  • Contact: Yang Han-Xi

Abstract: A micro-Raman electrochemical cell was designed for in-situ study of the elec-troreduction of SO_2Cl_2. This type of microcell has advantages of low sample volume, easy manipulation and experimental safety. Therefore, it can be used conveniently for in-situ spectroscopic investigation of strongly oxidative and hazardous Li-liquid cathode electrochemical systems.

Key words: Sulfuryl chloride, Electroreduction, Micro-Raman electrolytic cell, In-situ Raman spectroscopic investigation