Please wait a minute...
Acta Physico-Chimica Sinica  2006, Vol. 22 Issue (10): 1212-1216    DOI: 10.3866/PKU.WHXB20061008
Synthesis of Fe3+-modified SnO2 Nanoparticles by Hydrothermal Method
FANG Li-Mei;LI Zhi-Jie;LIU Chun-Ming;ZU Xiao-Tao
Department of Applied Physics, University of Electronic Science and Technology of China, Chengdu 610054, P. R. China
Download:   PDF(458KB) Export: BibTeX | EndNote (RIS)      

Abstract  Fe3+-modified SnO2 nanoparticles were directly prepared by hydrothermal method, and were characterized by X-ray diffraction (XRD), transmission electron microscope (TEM), Fourier transform infrared (FT-IR) spectroscopy, and UV-Vis diffuse reflectance spectra (DRS). It was found that rutile phase was directly synthesized without calcination. The Fe3+-modified SnO2 nanoparticles were well dispersed with narrow size distribution. The crystalline size of SnO2 decreased from 6.0 to 3.8 nm when the Fe3+ content increased from 0 to 20%. The specific surface area of pure SnO2 was 206.1 m2•g−1, and it increased to 259.8 m2•g−1 when Fe content was 15%. A considerable red shift in the absorbing band edge was observed as increase of Fe3+ content. XRD and DRS proved that Fe3+ and SnO2 formed solid solution nanoparticles.

Key wordsSnO2      Nanoparticles      Hydrothermal      Modified     
Received: 04 April 2006      Published: 11 October 2006
Corresponding Authors: ZU Xiao-Tao     E-mail:
Cite this article:

FANG Li-Mei;LI Zhi-Jie;LIU Chun-Ming;ZU Xiao-Tao. Synthesis of Fe3+-modified SnO2 Nanoparticles by Hydrothermal Method. Acta Physico-Chimica Sinica, 2006, 22(10): 1212-1216.

URL:     OR

[1] LIU Changjiang, MA Hongwen, ZHANG Pan. Thermodynamics of the Hydrothermal Decomposition Reaction of Potassic Syenite with Zeolite Formation[J]. Acta Physico-Chimica Sinica, 2018, 34(2): 168-176.
[2] LEI Gang, HE Yan. Applications of Single Plasmonic Nanoparticles in Biochemical Analysis and Bioimaging[J]. Acta Physico-Chimica Sinica, 2018, 34(1): 11-21.
[3] QIAN Hui-Hui, HAN Xiao, ZHAO Yan, SU Yu-Qin. Flexible Pd@PANI/rGO Paper Anode for Methanol Fuel Cells[J]. Acta Physico-Chimica Sinica, 2017, 33(9): 1822-1827.
[4] JU Guang-Kai, TAO Zhan-Liang, CHEN Jun. Controllable Preparation and Electrochemical Performance of Self-assembled Microspheres of α-MnO2 Nanotubes[J]. Acta Physico-Chimica Sinica, 2017, 33(7): 1421-1428.
[5] CHEN Fan, WANG Zhong-Yue, ZHANG Yan-Yan, YU Ke-Han, WENG Li-Xing, WEI Wei. Synthesis of Poly(acrylic acid)-Functionalized La1-xEuxF3 Nanocrystals with High Photoluminescence for Cellular Imaging[J]. Acta Physico-Chimica Sinica, 2017, 33(7): 1446-1452.
[6] HUANG Yu-Fen, ZHANG Hai-Long, YANG Zheng-Zheng, ZHAO Ming, HUANG Mu-Lan, LIANG Yan-Li, WANG Jian-Li, CHEN Yao-Qiang. Effects of CeO2 Addition on Improved NO Oxidation Activities of Pt/SiO2-Al2O3 Diesel Oxidation Catalysts[J]. Acta Physico-Chimica Sinica, 2017, 33(6): 1242-1252.
[7] ZHANG Xiao-Ru, XU Yue-Feng, SHEN Shou-Yu, CHEN Yuan, HUANG Ling, LI Jun-Tao, SUN Shi-Gang. Reduced Graphene Oxide-LaFeO3 Composite Nanomaterials as Bifunctional Catalyst for Rechargeable Lithium-Oxygen Batteries[J]. Acta Physico-Chimica Sinica, 2017, 33(11): 2237-2244.
[8] LIU Zhao-Xin, LI Wei-Bin. Catalytic Activity and Deactivation of Toluene Combustion on Rod-Like Copper-Manganese Mixed Oxides[J]. Acta Physico-Chimica Sinica, 2016, 32(7): 1795-1800.
[9] SUN Meng-Ting, HUANG Bi-Chun, MA Jie-Wen, LI Shi-Hui, DONG Li-Fu. Morphological Effects of Manganese Dioxide on Catalytic Reactions for Low-Temperature NH3-SCR[J]. Acta Physico-Chimica Sinica, 2016, 32(6): 1501-1510.
[10] ZHANG Ling, WANG Hai-Yan, JIANG Zhong-Xiang, WANG Yu-Jia. Synthesis and Catalytic Activity of Core-Shell MFI/CHA Zeolites[J]. Acta Physico-Chimica Sinica, 2016, 32(3): 745-752.
[11] HU Hai-Feng, HE Tao. Controllable Modulation of Morphology and Photocatalytic Performance of ZnO Nanomaterials via pH Adjustment[J]. Acta Physico-Chimica Sinica, 2016, 32(2): 543-550.
[12] ZHUANG Jian-Dong, TIAN Qin-Fen, LIU Ping. Bi2Sn2O7 Visible-Light Photocatalysts: Different Hydrothermal Preparation Methods and Their Photocatalytic Performance for As(Ⅲ) Removal[J]. Acta Physico-Chimica Sinica, 2016, 32(2): 551-557.
[13] ZHAO Jia, LIU Li-Feng, ZHANG Ying. Synthesis of Silver Nanoparticles Loaded onto a Structural Support and Their Catalytic Activity[J]. Acta Physico-Chimica Sinica, 2015, 31(8): 1549-1558.
[14] HU Hai-Feng, HE Tao. Controlled Aspect Ratio Modulation of ZnO Nanorods via Indium Doping[J]. Acta Physico-Chimica Sinica, 2015, 31(7): 1421-1429.
[15] CHEN Yang, ZHANG Zi-Lan, SUI Zhi-Jun, LIU Zhi-Ting, ZHOU Jing-Hong, ZHOU Xing-Gui. Preparation and Electrochemical Performance of Ni(OH)2 Nanowires/ Three-Dimensional Graphene Composite Materials[J]. Acta Physico-Chimica Sinica, 2015, 31(6): 1105-1112.