ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2006,Vol.22>> Issue(10)>> 1212-1216     doi: 10.3866/PKU.WHXB20061008         中文摘要
Synthesis of Fe3+-modified SnO2 Nanoparticles by Hydrothermal Method
FANG Li-Mei;LI Zhi-Jie;LIU Chun-Ming;ZU Xiao-Tao
Department of Applied Physics, University of Electronic Science and Technology of China, Chengdu 610054, P. R. China
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Fe3+-modified SnO2 nanoparticles were directly prepared by hydrothermal method, and were characterized by X-ray diffraction (XRD), transmission electron microscope (TEM), Fourier transform infrared (FT-IR) spectroscopy, and UV-Vis diffuse reflectance spectra (DRS). It was found that rutile phase was directly synthesized without calcination. The Fe3+-modified SnO2 nanoparticles were well dispersed with narrow size distribution. The crystalline size of SnO2 decreased from 6.0 to 3.8 nm when the Fe3+ content increased from 0 to 20%. The specific surface area of pure SnO2 was 206.1 m2•g−1, and it increased to 259.8 m2•g−1 when Fe content was 15%. A considerable red shift in the absorbing band edge was observed as increase of Fe3+ content. XRD and DRS proved that Fe3+ and SnO2 formed solid solution nanoparticles.

Keywords: SnO2   Nanoparticles   Hydrothermal   Modified  
Received: 2006-04-04 Accepted: 2006-05-12 Publication Date (Web): 2006-10-11
Corresponding Authors: ZU Xiao-Tao Email:

Cite this article: FANG Li-Mei;LI Zhi-Jie;LIU Chun-Ming;ZU Xiao-Tao. Synthesis of Fe3+-modified SnO2 Nanoparticles by Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2006,22 (10): 1212-1216.    doi: 10.3866/PKU.WHXB20061008
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89. CHEN Shi-Yu, WANG Zhao-Xiang, FANG Xiang-Peng, ZHAO Hai-Lei, LIU Xiao-Jiang, CHEN Li-Quan.Characterization of TiS2 as an Anode Material for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2011,27(01): 97-102
90. HAN Rong-Cheng1 YU Min1 SHA Yin-Lin.Interaction between CdSeS Quantum Dots and Gold Nanoparticles in Solution[J]. Acta Phys. -Chim. Sin., 2011,27(01): 255-261
91. ZHANG Fang, YUAN Chang-Zhou, ZHANG Xiao-Gang, ZHANG Luo-Jiang, XU Ke.5-Sulfosalicylic Acid-Assisted Hydrothermal Synthesis and Supercapacitive Properties of Co-Ni Layered Double Hydroxides[J]. Acta Phys. -Chim. Sin., 2010,26(12): 3175-3180
92. WU Xiao-Qin, ZONG Rui-Long, MU Hao-Jie, ZHU Yong-Fa.Cataluminescence Performance on Catalysts of Graphene Supported Platinum[J]. Acta Phys. -Chim. Sin., 2010,26(11): 3002-3008
93. WU Tao, TAO Jie, DENG Jie, TANG Yu-Xin, ZHU Hong, GAO Peng.Preparation and Characterization of One-Dimensional TiO2 Nanowire Films on a Flexible Stainless Steel Substrate[J]. Acta Phys. -Chim. Sin., 2010,26(11): 3087-3094
94. ZONG Hua, WANG Lei, FANG Hong-Bo, MAO Lei-Ting, WANG Yu-Hui, ZHANG Lu, ZHAO Sui, YU Jia-Yong.Effect of Hydrophobically Modified Polyacrylamide on Interfacial Dilational Rheological Properties of Crude Oil Components[J]. Acta Phys. -Chim. Sin., 2010,26(11): 2982-2988
95. LI Zhao-Hu, ZHANG Zhi-Kun, GUO Deng-Zhu.Fabrication of Al2O3 Nanoparticles by Cathodic Plasma Electrolysis[J]. Acta Phys. -Chim. Sin., 2010,26(11): 3106-3112
96. LUO Yong-Chun, ZHANG Tie-Jun, WANG Duo, KANG Long.Influence of Ball-Milling on Hydrogen Storage and Electrochemical Properties of (Ti Cr)0.497V0.42Fe0.083/30%(w) (LaRMg)(NiCoAl)3.5 Alloy Electrodes[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2397-2404
97. ZHU Yan-Feng, DU Rong-Gui, LI Jing, QI Hai-Qing, LIN Chang-Jian.Photogenerated Cathodic Protection Properties of a TiO2 Nanowire FilmPrepared by a Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2349-2353
98. MAO Dong-Sen, GUO Qiang-Sheng, MENG Tao.Effect of Magnesium Oxide Modification on the Catalytic Performance of Nanoscale HZSM-5 Zeolite for the Conversion of Methanol to Propylene[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2242-2248
99. WANG Zheng-Ke, HU Qiao-Ling.Chitosan Rods Reinforced by N-Carboxyl Propionyl Chitosan Sodium[J]. Acta Phys. -Chim. Sin., 2010,26(07): 2053-2056
100. WU Jian, WANG Yu, HUANG Feng, YANG Yang, MENG Chang-Gong.Thermal Diffusion Synthesis and Characterization of SnO2 Clusters within ZSM-5 Crystals[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1705-1710
101. ZHANG Hui-Juan, SONG Huai-He, ZHOU Ji-Sheng, ZHANG Hong-Kun, CHEN Xiao-Hong.Preparation and Electrochemical Properties of SnO2/Onion-Like Hollow Carbon Nanoparticle Composites as Anode Materials for Lithium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1259-1263
102. HE Yue, DONG Mei, LI Jun-Fen, WANG Jian-Guo, FAN Wei-Bin.Synthesis and Catalytic Properties of MeAPO-5 Molecular Sieves for Selective Oxidation of Cinnamyl Alcohol[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1305-1310
103. ZHANG Shu-Cui, JIANG Dong, TANG Tao, LI Jun-Hua, XU Yao.Synthesis and Photocatalytic Activity of Highly Dispersed TiO2/SBA-15[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1330-1336
104. AN Xiao-Sha, CHEN De-Jun, ZHOU Zhi-You, WANG Qiang, FAN You-Jun, SUN Shi-Gang.Rare Earth Eu Doped PtRu/C Catalysts and Their Properties for Methanol Electrooxidation[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1207-1213
105. ZHANG Ai-Ping, ZHANG Jin-Zhi.Syntheses and Activities of Visible-Light-Driven Cu/BiVO4 Composite Photocatalysts[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1337-1342
106. ZHANG Ye-Xin, SU Qing-Yun, WANG Zhong-Peng, GAO Xi-Yan, ZHANG Zhao-Liang.Surface Modification of Mg-Al Hydrotalcite Mixed Oxides with Potassium[J]. Acta Phys. -Chim. Sin., 2010,26(04): 921-926
107. YAN Dong-Xia, WANG Hua, LI Kong-Zhai, WEI Yong-Gang, ZHU Xing, CHENG Xian-Ming.Structure and Catalytic Property of Ce1-xFexO2 Mixed Oxide Catalysts for Low Temperature Soot Combustion[J]. Acta Phys. -Chim. Sin., 2010,26(02): 331-337
108. XU Xin, WANG Xiao-Jing, HU Zhong-Hua, LIU Ya-Fei, WANG Chen-Chen, ZHAO Guo-Hua.Influence of Sol-Gel and Dip-Hydrothermal Preparation Methods on Structure and Performance of TiO2/AC Photocatalysts[J]. Acta Phys. -Chim. Sin., 2010,26(01): 79-86
109. PANG Xu, MA Zheng-Qing, ZUO Lie.Sn Doped MnO2 Electrode Material for Supercapacitors[J]. Acta Phys. -Chim. Sin., 2009,25(12): 2433-2437
110. YANG Xin-Wei, ZHANG Gui-Rong, LI Yong-Xiu, XU Bo-Qing.Size-Control of Monodispersing Gold Nanoparticles via Stepwise Seed-Mediated Growth[J]. Acta Phys. -Chim. Sin., 2009,25(12): 2565-2569
111. LV Cun-Qin, LING Kai-Cheng, WANG Gui-Chang.Decomposition of Methylamine on the Clean and P Modified Mo(100) Surfaces[J]. Acta Phys. -Chim. Sin., 2009,25(11): 2336-2342
112. XU Jiang, ZHUO Cheng-Zhi, JIANG Shu-Yun.Effect of Nanoparticles on the Erosion-Corrosion Resistance Property of a Ni-Based Alloying Layer[J]. Acta Phys. -Chim. Sin., 2009,25(10): 1958-1966
113. WANG Run-Han, JIANG Ji-Sen, HU Ming.Controlled Syntheses of FeNi3 Alloy Nanostructures via Reverse Microemulsion-Directed Hydrothermal Motheds[J]. Acta Phys. -Chim. Sin., 2009,25(10): 2167-2172
114. LI Gui-An, ZHU Ting-Liang, YE Lu-Yuan, DENG Zhong-Xun, ZHANG Ya-Juan, JIAO Fei, ZHENG Hai-Rong.Hydrophobic Silica Aerogel Prepared In-situ by Ambient Pressure Drying and Its Thermal Stability[J]. Acta Phys. -Chim. Sin., 2009,25(09): 1811-1815
115. DONG Xiang, TAO Jie, LI Ying-Ying, WANG Tao, ZHU Hong.Photoelectrochemical Properties of Three-Dimensional Network TiO2 Nanowire Film Prepared by Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2009,25(09): 1874-1882
116. LV Yong, LU Wen-Cong, ZHANG Liang-Miao, YUE Bao-Hua, SHANG Xing-Fu, NI Ji-Peng.Synthesis, Characterization and Growth Mechanism of Core/Shell AlOOH Microspheres[J]. Acta Phys. -Chim. Sin., 2009,25(07): 1391-1396
117. CHEN Qi-Feng, JIANG Dong, XU Yao, WU Dong, SUN Yu-Han.Visible Region Photocatalysis of Ce-Si/TiO2 Synthesized Using Sol-Gel-Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2009,25(04): 617-623
118. MA Ruo-Biao, FU Yan-Bao, MA Xiao-Hua.Preparation and Electrochemical Performance of Tin-Dioxide Filled Multi-Walled Carbon Nanotubes[J]. Acta Phys. -Chim. Sin., 2009,25(03): 441-445
119. GAO Qiang; LIU Ya-Fei; HU Zhong-Hua; ZHENG Xiang-Wei; WEN Zu-Biao.Electrochemical Properties of Manganese Oxide Surface-Modified Activated Carbon Electrode Materials[J]. Acta Phys. -Chim. Sin., 2009,25(02): 229-236
120. ZHAO Li-Na; ZHAO Xu; REN Su-Xia; LIU Ying; WANG Zi-Chen.In Situ Synthesis and Surface Modification of Calcium Carbonate[J]. Acta Phys. -Chim. Sin., 2009,25(01): 47-52
121. ZHAO Rui-Hua, DONG Mei, QIN Zhang-Feng, DING Jian-Fei, GUO Xing-Cui, WANG Jian-Guo.Synthesis and Characterization of CoAPO-5 with different Cobalt Contents and Their Catalytic Performance for Cyclohexane Oxidation[J]. Acta Phys. -Chim. Sin., 2008,24(12): 2304-2308
122. JIANG Cai-Yun, WENG Xiao-Lei, QIAN Wei-Ping.Preparation and Thermoresponsive Properties of AuNPs/PNIPAM Composite Particles[J]. Acta Phys. -Chim. Sin., 2008,24(12): 2159-2164
123. DONG Yong-Chun; DU Fang; HAN Zhen-Bang.Coordination Structure between Modified PAN Fiber and Fe(III) Ion and Its Catalytic Function on Degradation of Azo Dyes[J]. Acta Phys. -Chim. Sin., 2008,24(11): 2114-2121
124. YANG Zhen; YANG Xiao-Ning; XU Zhi-Jun.Molecular Dynamics Simulation of Structure and Dynamics Properties of Water Near an Au Nanoparticle[J]. Acta Phys. -Chim. Sin., 2008,24(11): 2047-2052
125. CHANG Guo-Qing, ZHENG Xi, CHEN Ri-Yao, CHEN Xiao, CHEN Li-Qin, CHEN Zhen.Silver Nanoparticles Filling in TiO2 Hollow Nanofibers by Coaxial Electrospinning[J]. Acta Phys. -Chim. Sin., 2008,24(10): 1790-1796
126. ZHENG Yi-Xiong; YAO Shi-Bing; ZHOU Shao-Min.Electrooxidation of Ethanol at Ni-B Amorphous Alloy Electrode and Measurements of Kinetic Parameters[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1643-1649
127. LV Cun-Qin; LING Kai-Cheng; SHANG Zhen-Feng; WANG Gui-Chang.Adsorption of Methyl, Amido and Methylamine Species on the Clean and C(N, O) Modified Mo(100) Surfaces[J]. Acta Phys. -Chim. Sin., 2008,24(08): 1366-1370
128. JIN Zheng-Wei; WANG Xiao-Dong.Mechanism of Acidity-Induced Mesostructure Transformation for Highly Ordered Mesoporous Silica Materials and Their Functionalizations[J]. Acta Phys. -Chim. Sin., 2008,24(08): 1519-1523
129. LI Hai-Long; LUO Wu-Lin; CHEN Tao; TIAN Wen-Yu; SUN Mao; LI Chun; ZHU Di; LIU Ran-Ran; ZHAO Yu-Liang; LIU Chun-Li.Preparation and Photocatalytic Performance of Titania Nanotubes Loaded with Ag Nanoparticles[J]. Acta Phys. -Chim. Sin., 2008,24(08): 1383-1386
130. ZHANG Hui; ZHU Li-Qun; LI Wei-Ping; LIU Hui-Cong.Sonochemical Fabrication and Electrochemical Performance of Electrode Materials Containing Rare Earth Yttrium[J]. Acta Phys. -Chim. Sin., 2008,24(08): 1425-1431
131. LIU Ya-Fei; HU Zhong-Hua; XU Kun; ZHENG Xiang-Wei; GAO Qiang.Surface Modification and Performance of Activated Carbon Electrode Material[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1143-1148
132. WANG Bai-Qi; XIA Chun-Hui; FU Qiang; WANG Peng-Wei; SHAN Xu-Dong; YU Da-Peng.Hydrothermal Preparation and Photoluminescence Property of Co-Doped ZnO Nanorods[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1165-1168
133. FAN Jie; XU Xiu-Feng; NIU Xian-Jun.Decomposition of CF4 over Al2O3-Based Metal Oxides[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1271-1276
134. HAO Li-Juan; LI Shuang-Yan; HAN Lei; HUANG Jie; CHANG Jin.Preparation and Characterization of a Novel Magnetic Nano-Gene Vector[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1857-1863
135. CAO Ji-Lin; XING Dong-Qiang; LIU Xiu-Wu; TAN Zhao-Yang.Synthesis of Magnetic 4A Zeolite at Ultrasonic Condition[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1893-1898
136. WANG Xiao-Dong; YI Gui-Yun; DONG Peng; CHEN Sheng-Li.Mechanism of Floating Self-assembly of Binary Colloidal Particles at Water-Air Interface of Suspension[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1707-1713
137. PENG Lin; YU Ning-Ya; TANG Qun-Li; QIU Hua-Yu; YIN Du-Lin; YIN Dong-Hong.Effect of Hydrophobic Modification on Sustained-Release Properties of Alachlor/MCM-41[J]. Acta Phys. -Chim. Sin., 2007,23(10): 1572-1576
138. FU Xiao-Feng; ZOU Hua-Min; HAN Jun-Bo.Photo Oxidation of Ag/Titanium Oxide Nanoparticle Film Induced by Ultrafast Laser[J]. Acta Phys. -Chim. Sin., 2007,23(06): 940-944
139. ZHAO Hai-Jun; HOU Hai-Tao; CAO Jie-Ming ZHENG Ming-Bo; LIU Jing-Song; ZHANG Fang.Solvothermal Synthesis of Mesoporous SnO2 with Spongy Structure[J]. Acta Phys. -Chim. Sin., 2007,23(06): 959-963
140. HE Yong-Jun; YU Xiang-Yang; ZHAO Xiao-Ling.Surface Modification and Assembly of Cu2(OH)2CO3 Microspheres[J]. Acta Phys. -Chim. Sin., 2007,23(05): 774-778
141. TANG Yan-Jun; LI You-Ming; SONG Jing; PAN Zhi-Dong.Structural Characterization and Thermal Decomposition Behavior of Microsized and Nanosized CaCO3[J]. Acta Phys. -Chim. Sin., 2007,23(05): 717-722
142. ZENG Wei; ZHOU Hai-Hui; YING Xiao-Fang; ZENG Qing-Liang; HU Wei-Ya; KUANG Ya-Fei.Electrodeposition of Gold Nanoparticles Coatings from Electrode/ReverseMicroemulsion System[J]. Acta Phys. -Chim. Sin., 2007,23(05): 769-773
143. GUO Wen-Jing;SUN Lei;ZHANG Ping-Yu;WU Zhi-Shen;ZHANG Zhi-Jun.Preparation and Antiwear Property of Monodisperse Silver Nanoparticles in Microemulsion[J]. Acta Phys. -Chim. Sin., 2007,23(03): 367-372
144. SONG Xu-Chun;ZHENG Yi-Fan;LIN Shen;WANG Yun.A Simple Method to Synthesize α-MnO2 and β-MnO2 Single-crystalline Nanorods[J]. Acta Phys. -Chim. Sin., 2007,23(02): 258-261
145. ZHOU Hong-Wei;LI Huai-Xiang;JIANG Zheng-Wei;ZUO Xiang-Qing.Treatment of ZnS:Mn Phosphors by Partial Sublimation of SnO2:Sb Xerogel[J]. Acta Phys. -Chim. Sin., 2007,23(01): 88-91
146. SHI Qiu-Jie;LEI Jing-Xin;ZHANG Ning.Modification of Ni-B/TiO2-Al2O3(S) Amorphous Alloy Catalyst by Mo for Liquid-phase Furfural Hydrogenation[J]. Acta Phys. -Chim. Sin., 2007,23(01): 98-102
147. ZHANG Yue-Wei;SHEN Mei-Qing;WU Xiao-Dong;WENG Duan;ZHANG Zhi-Hua;TIAN Ran;CHI Ke-Bin.Modification of the Structure and Properties of SAPO-11 Using Rare Earths[J]. Acta Phys. -Chim. Sin., 2006,22(12): 1495-1500
148. LI De-Bao;QI Hui-Jie;LI Wen-Huai;SUN Yu-Han;ZHONG Bing.Surficial Structure and Charge Effects of Ni Promoted K2CO3/MoS2 Catalysts for Higher Alcohols Synthesis[J]. Acta Phys. -Chim. Sin., 2006,22(09): 1132-1136
149. YU Zhi- Hui;TIAN Mi;JIAO Qing-Ying;XIA Ding- Guo.Self-assembling Nanobimetallic Particles of Au-Pt on Glassy Carbon Electrode[J]. Acta Phys. -Chim. Sin., 2006,22(08): 1015-1020
150. WANG Xiao-Dong;DONG Peng;CHEN Sheng-Li.Preparation of Macroporous Al2O3 by Template Method[J]. Acta Phys. -Chim. Sin., 2006,22(07): 831-835
151. LIU Hui-Yu;CHEN Dong;TANG Fang-Qiong;LING Hui;REN Xiang-Ling.Fabrication of Silver Nanoshells on Modified Polystyrene Microspheres through Electroless Plating Approach[J]. Acta Phys. -Chim. Sin., 2006,22(05): 644-648
152. YANG Li-Ping;TU Wei-Xia.Studies on Au Colloidal Nanoparticles Synthesized by Microwave Irradiation[J]. Acta Phys. -Chim. Sin., 2006,22(04): 513-516
153. HAO Yan-Zhong; HAN Wen-Tao.Preparation and Photoelectrochemical Properties of Titanate Nanotubes[J]. Acta Phys. -Chim. Sin., 2006,22(02): 221-225
154. LIN Wei; ZHANG Yong-fan; LI Yi; CHEN Yong; LI Jun-qian.First Principle Studies on the Geometry and Electronic Structures of the SnO2(110) Surface[J]. Acta Phys. -Chim. Sin., 2006,22(01): 76-81
155. SONG Xu-chun; ZHENG Yi-fan; YIN Hao-yong; CAO Guang-sheng.Synthesis and Characterization of Transition Element Substituted Titanate Nanotubes[J]. Acta Phys. -Chim. Sin., 2005,21(10): 1076-1080
156. WANG Chang-song; FENG Xin; LU Xiao-hua.Surface Modification of Potassium Titanate Whiskers with n-octadecyltrichlorosilane[J]. Acta Phys. -Chim. Sin., 2005,21(06): 586-590
157. TAO Xiao-Jun; LI Zhi-Wei; CHEN Hong-Jie; ZHANG Ping-Yu; ZHANG Zhi-Jun; WU Zhi-Shen; DANG Hong-Xin.A New Approach to Synthesize Nickel Nanoparticles[J]. Acta Phys. -Chim. Sin., 2005,21(05): 569-572
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162. Chen Wei-Ping;Feng Xin;Wang Chang-Song;Sun Sheng-Hua;Lu Xiao-Hua.The Interface Properties of Potassium Titanate Whiskers[J]. Acta Phys. -Chim. Sin., 2004,20(08): 868-870
163. Cai Wei-Quan;Li Hui-Quan;Zhang Yi.Hydrothrmal Crystal Growth of Very Light Boehmite products[J]. Acta Phys. -Chim. Sin., 2004,20(07): 717-721
164. Deng Mei-Gen;Zhang Zhi-An;Hu Yong-Da;Wang Bin-Hua;Yang Bang-Chao.Effect of Activation and Surface Modification on the Properties of Carbon Nanotubes Supercapacitors[J]. Acta Phys. -Chim. Sin., 2004,20(04): 432-435
165. Chen Hong;Han Li-Juan;Xu Peng;Luo Ping-Ya.The Thickening Mechanism Study of Hydrophobically Modified Polyacrylamide[J]. Acta Phys. -Chim. Sin., 2003,19(11): 1020-1024
166. Ji Hong-Bing;Qian Yu.Influence of Cu Additive on the Structure of Ru-modified Spinel Catalyst and Its Oxidative Performance[J]. Acta Phys. -Chim. Sin., 2003,19(09): 824-828
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171. Zhang Xin-Rong;Shi Peng-Fei.Catalytic Production of Hydrogen from Steam Reforming of Methanol on CeO2 Promoted Cu/Al2O3 Catalysts[J]. Acta Phys. -Chim. Sin., 2003,19(01): 85-89
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