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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2004,Vol.20>> Issue(06)>> 582-586     doi: 10.3866/PKU.WHXB20040606         中文摘要
Effect on the Electrochemical Performance of Lithium Iron Phosphate by Cr3+ Ion Doping
Ni Jiang-Feng;Zhou Heng-Hui;Chen Ji-Tao;Su Guang-Yao
College of Chemistry and Molecular Engineering, Peking University, Beijing 100871;College of Chemistry, Xiangtan University, Xiangtan 411105
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Two different methods(mechanical ball-milling and co-precipitation)were applied to prepare lithium iron phosphate(LiFePO4) containing low concentration(1%, mole fraction) Cr3+ ion dopant. The samples were characterized by X-ray diffraction and scanning electron microscope, and their electrochemical performances were investigated including cycling behavior and large current discharging. The results indicate that the Cr3+ ion dopant does not affect the structure of the material but considerably improves its kinetics in terms of capacity delivery and cycle performance. At a low discharging rate (0.1 C), LiFePO4 samples doping via mechanical ball-milling and co-precipitation are capable of delivering reversible specific capacities of 144 mAh•g-1 and 158 mAh•g-1 respectively, with fairly stable cycleability. Even at a 2 C discharging rate, they can show capacities of 110 mAh•g-1 and 130 mAh•g-1 respectively, too. The results also confirm that doping via co-precipitation with Fe sources is an effective method to improve the ion doping effect.

Keywords: Lithium iron phosphate   Co-precipitation   Ion doping   Electronic conductivity   Lithium intercalation capacity   Positive electrode material  
Received: 2003-12-10 Accepted: 2004-02-05 Publication Date (Web): 2004-06-15
Corresponding Authors: Zhou Heng-Hui Email: hhzhou@chem.pku.edu.cn


Cite this article: Ni Jiang-Feng;Zhou Heng-Hui;Chen Ji-Tao;Su Guang-Yao. Effect on the Electrochemical Performance of Lithium Iron Phosphate by Cr3+ Ion Doping[J]. Acta Phys. -Chim. Sin., 2004,20 (06): 582-586.    doi: 10.3866/PKU.WHXB20040606
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