Register
ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2004,Vol.20>> Issue(06)>> 598-601     doi: 10.3866/PKU.WHXB20040609         中文摘要
Preparation and Characterization of Fe3O4/PVDF Magnetic Composite Membrane
Du Jun;Wu Ling;Tao Chang-Yuan;Sun Cai-Xin
College of Chemistry and Chemical Engineering, Chongqing University, Chongqing 400044; College of Electrical Engineering, Chongqing University, Chongqing 400044
Full text: PDF (1947KB) Export: BibTeX | EndNote (RIS)
Fe3O4 nanoparticles were introduced into microporous poly(vinylidene fluoride) (PVDF)membrane by in-situ membrane phase permeating method and a magnetic composite Fe3O4/PVDF membrane was prepared. Optimum preparation conditions were studied. FT-IR and DSC study indicates that the introducing of Fe3O4 did not affect the PVDF structure and the composite membranes show good thermo-stability. Fe3O4 particle size calculated from XRD result is about 68 nm. The susceptibility of the resulting composite membrane reached 0.044 cm3•g-1 and changed with reaction conditions. The variations of pore size of the composite membrane were investigated by gas permeating method. The maximum and average pore size, as well as pore size distribution, of the composite membranes are different from those of PVDF host membrane, and changed obviously with preparing conditions.

Keywords: Fe3O4   PVDF   Magnetic composite membrane   In-situ reaction    Nanostructure materials  
Received: 2003-12-11 Accepted: 2004-02-23 Publication Date (Web): 2004-06-15
Corresponding Authors: Tao Chang-Yuan Email: taocy@cqu.edu.cn


Cite this article: Du Jun;Wu Ling;Tao Chang-Yuan;Sun Cai-Xin. Preparation and Characterization of Fe3O4/PVDF Magnetic Composite Membrane[J]. Acta Phys. -Chim. Sin., 2004,20 (06): 598-601.    doi: 10.3866/PKU.WHXB20040609
1. LIU Shan-Shan, XU Zheng, ZHAO Su-Ling, LIANG Zhi-Qin, ZHU Wei.Effects of F- Concentration on the Morphologies and Fluorescent Lifetimes of Ln3+-Doped Up-Conversion Nanocrystals[J]. Acta Phys. -Chim. Sin., 2016,32(8): 2108-2112
2. SUN Meng-Ting, HUANG Bi-Chun, MA Jie-Wen, LI Shi-Hui, DONG Li-Fu.Morphological Effects of Manganese Dioxide on Catalytic Reactions for Low-Temperature NH3-SCR[J]. Acta Phys. -Chim. Sin., 2016,32(6): 1501-1510
3. FENG Lei, HAO Jing-Cheng.Preparation and Property of Gold Nanoparticles from Muliple Self- Assembled Structures as Templates in LA/C14DMAO/H2O System[J]. Acta Phys. -Chim. Sin., 2016,32(1): 380-390
4. LIU Jian-Hua, LIU Bin-Hong, LI Zhou-Peng.Fe3O4/Graphene Composites with a Porous 3D Network Structure Synthesized through Self-Assembly under Electrostatic Interactions as Anode Materials of High-Performance Li-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2014,30(9): 1650-1658
5. LI Ya-Jing, SUN Xiao-Feng, YE Qing, LIU Bai-Chen, WU Yao-Guo.Preparation and Properties of a Novel Hemicellulose-Based Magnetic Hydrogel[J]. Acta Phys. -Chim. Sin., 2014,30(1): 111-120
6. PANG Rui-Zhi, LI Xin, LI Jian-Sheng, LU Zhuang-Yu, HUANG Cheng, SUN Xiu-Yun, WANG Lian-Jun.In situ Preparation and Antifouling Performance of ZrO2/PVDF Hybrid Membrane[J]. Acta Phys. -Chim. Sin., 2013,29(12): 2592-2598
7. HONG Zhou-Qin, LI Jin-Xia, ZHANG Fang, ZHOU Li-Hui.Synthesis of Magnetically Graphitic Mesoporous Carbon from Hard Templates and Its Application in the Adsorption Treatment of Traditional Chinese Medicine Wastewater[J]. Acta Phys. -Chim. Sin., 2013,29(03): 590-596
8. DING Peng, XU You-Long, SUN Xiao-Fei.Synthesis and Performance of Nano MnO as an Anode Material for Lithium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2013,29(02): 293-297
9. WEN Wen, GAO Xiao-Ya, SONG Zhi-Ying, HAN Dong, WANG Juan, ZHU Mei-Xia, ZHANG Ai-Ping.Preparation of Magnetic Targeted Fe3O4-TiO2Nanoparticles and Their Photocatalytic Killing Effect on Hepatoma Carcinoma Cells[J]. Acta Phys. -Chim. Sin., 2012,28(09): 2221-2230
10. ZHANG Hua, HU Yao-Juan, WU Ping, ZHANG Hui, CAI Chen-Xin.Preparation of an Ultrahigh Aspect Ratio Anodic Aluminum Oxide Template for the Fabrication of Ni Nanowire Arrays[J]. Acta Phys. -Chim. Sin., 2012,28(06): 1545-1550
11. ZHANG Xiao, YANG Rong, WANG Chen, HENG Cheng-Lin.Cell Biocompatibility of Functionalized Graphene Oxide[J]. Acta Phys. -Chim. Sin., 2012,28(06): 1520-1524
12. CHEN Peng-Peng, WANG Jing, YAO Peng-Jun, DU Hai-Ying, LI Xiao-Gan.Synthesis and Gas Sensitivity of In2O3/CdO Composite[J]. Acta Phys. -Chim. Sin., 2012,28(06): 1539-1544
13. GUO Xue-Yi, YI Peng-Fei, WANG Wei-Jia, YANG Ying.Electrochemical Properties of an Agarose-Based Magnetic Polymer Electrolyte in Dye-Sensitized Solar Cells[J]. Acta Phys. -Chim. Sin., 2012,28(03): 585-590
14. LI Xue-Fei, ZHAO Yun, JIAO Qing-Ze, LI Han-Sheng, WU Hong-Yu, LIU Hong-Bo, CUI Wen-Jia.Preparation of One-Dimensional Titanate Nanomaterials Using Different Titania Sources[J]. Acta Phys. -Chim. Sin., 2011,27(08): 1996-2000
15. MAI Li-Qiang, YANG Shuang, HAN Chun-Hua, XU Lin, XU Xu, PI Yu-Qiang.Chemical Lithiation and Electroactivity of Nanomaterials[J]. Acta Phys. -Chim. Sin., 2011,27(07): 1551-1559
16. SUN Du, YIN Peng-Gang, GUO Lin.Synthesis and Raman Property of Porous Jujube-Like Cu2O Hierarchy Structure[J]. Acta Phys. -Chim. Sin., 2011,27(06): 1543-1550
17. XIANG Mei, HE Chang-Cheng, WANG Hui-Liang.Magnetic Polyacrylamide/Fe3O4 Nanocomposite Hydrogel with High Mechanical Strength[J]. Acta Phys. -Chim. Sin., 2011,27(05): 1267-1272
18. ZHANG Yi, CHEN Biao, YANG Zu-Pei, ZHANG Zhi-Jun.Controlled Synthesis and Characterization of the Structure and Property of Fe3O4 Nanoparticle-Graphene Oxide Composites[J]. Acta Phys. -Chim. Sin., 2011,27(05): 1261-1266
19. YAN Gong-Qin, WANG Wei, SUN Zhi-Gang, GUAN Jian-Guo.Magnetite Sub-Microspheres with Controlled Diameter and Magnetic Properties Synthesized by the Citrate-Assisted Polyol Process[J]. Acta Phys. -Chim. Sin., 2010,26(11): 3120-3126
20. ZHAO Chuan-Xi, WU Ping, ZHANG Dan-Li, CHEN Rong, CHI Ling-Fei, XIAO Tan.Synthesis and Photoluminescence of Zn2SnO4 Nanomaterials[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1343-1348
21. FENG Hua-Jun; CHEN Yuan;DAI Ke-Hua; SONG Zhao-Shuang; MA Jian-Wei; QI Lu.Preparation and Characterization of a Novel Kind of Polymer Electrolyte Composite Membrane for Lithium-Ion Battery[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1922-1926
22. XU Can; ZHANG Xiao-Fang; CHEN Liang; ZHU Li-Fang; ZHANG Rong-Jun.Theoretical Study on the Even-Odd Oscillation of the Vibration Modes of the Silica Nanowire[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1733-1737
23. SHE Shi-Xiong; SU Bi-Tao; YANG Yan; MIN Shi-Xiong; LEI Zi-Qiang.Preparation of Functional Polymer Nanomaterial and Its Catalytic Property[J]. Acta Phys. -Chim. Sin., 2007,23(06): 900-904
24. CHAI Yong-Cun;CHEN Xiao;SUI Zhen-Ming;ZHUANG Wen-Chang.Electrochemical Deposition of Bunchy Nanostructured Platinum from Lyotropic Liquid Crystal Template[J]. Acta Phys. -Chim. Sin., 2006,22(12): 1506-1510
25. WANG Zhong;TIAN Wen-Huai;LI Xing-Guo.Synthesis and Electrochemical Properties of Sn-Sb Alloy Prepared by Hydrogen Plasma-metal Reaction[J]. Acta Phys. -Chim. Sin., 2006,22(06): 752-755
26. CAO Jie-ming; WANG Jun; FANG Bao-qing; ZHENG Ming-bo; LU Hong-xia; CHANG Xin; WANG Hai-yan.Synthesis and Characterization of ZnO Nanomaterials with Different Morphologies in Ionic Liquids[J]. Acta Phys. -Chim. Sin., 2005,21(06): 668-672
27. JIANG Wei;LI Feng-Sheng;CHEN Ling-Yun;YANG Yi;CHU Jian-Jun.Preparation and Properties of Novel Magnetic Fe3O4/EDTA Nano-composite Particles[J]. Acta Phys. -Chim. Sin., 2005,21(02): 182-186
28. Chen Feng; Zhu Yi-Ping; Ma Hong-Liao; Bo Zi-Long; Zhang Jin-Long.Preparation and Characterization of TiO2--CdS-MCM-41 Nano-composite[J]. Acta Phys. -Chim. Sin., 2004,20(11): 1292-1296
29. Li Di;Li Jing-Hong.Electrochemistry of Monolayer Protected Nanoclusters[J]. Acta Phys. -Chim. Sin., 2004,20(08S): 982-988
30. Sun Shi-Gang.Enhanced IR Absorption and Abnormal IR Effects of Low-dimensional Nanomaterials[J]. Acta Phys. -Chim. Sin., 2004,20(08S): 1017-1023
31. Qiu Jie-Shan;An Yu-Liang;Li Qi-Xiu;Zhou Ying;Yang Qing.Preparation of Carbon Encapsulated Metal (Mn,Co) Nanomaterials with Apoferrintin as the Constrained Nano-sized Reactor[J]. Acta Phys. -Chim. Sin., 2004,20(03): 260-264
32. Wang Hui;Zhang Xiu-Juan;Zhang Xiao-Hong;Wu Shi-Kang.The Preparation of Nano-sized Silica Gel Suspension and the Recognition of Transition Metal Cations[J]. Acta Phys. -Chim. Sin., 2004,20(03): 313-317
33. Dong Xiang-Ting;He Ying;Yan Jing-Hui;Xue Bo-Fei;Feng Xiu-Li;Hong Guang-Yan.Preparation and Characterization of Nanosized AgBr/PMMA Photochromic Hybrid Material[J]. Acta Phys. -Chim. Sin., 2003,19(12): 1159-1162
34. Xu Jin-Xia;Huang Xin-Min;Qian Li-Hua.Structure and Properties of Ni-Al2O3 Nanochannel Array System by Direct Current Electro-deposition[J]. Acta Phys. -Chim. Sin., 2003,19(03): 265-267
35. Wei Jian-Hong;Guan Jian-Guo;Chen Wen-Yi;Yuan Run-Zhang.Preparation and Characteristics of Polyaniline - Barium Titanate Nanocomposite Particles[J]. Acta Phys. -Chim. Sin., 2002,18(07): 653-656
36. Zhao Li-Li;Wang Rong-Shu;Niu Wen-Tai;Li Xiang.Synthesis of γ-MnO2 Nano Powder Used for SieveMembrane Reactor[J]. Acta Phys. -Chim. Sin., 2002,18(03): 197-200
37. Cao Da-Peng;Wang Wen-Chuan;Shen Zhi-Gang;Chen Jian-Feng.Determination of Optimum Pressure for Supercritical Methane Adsorbed in Nano-material[J]. Acta Phys. -Chim. Sin., 2001,17(10): 940-943
38. Shi Wei-Xian;Yang Jun;Wang Ting-Jie;Jin Yong.Surface Organic Modification of Magnetic Iron Oxide Black Particles[J]. Acta Phys. -Chim. Sin., 2001,17(06): 507-510
39. Mou Chun-Bo,He Tian-Jing,Wang Xiu-Yan,Liu Fan-Zhen,Jiang Ji-Sen,Chen Long-Wu.Surface Enhanced Raman Scattering(SERS) from H2TSPP and Ag(II)TSPP Adsorbed on Uniform Fe3O4 Colloids[J]. Acta Phys. -Chim. Sin., 1996,12(09): 841-844
40. HOU Jing-Fei, YANG Yan-Lian, WANG Chen.Molecular Mechanisms of Interface Interactions between Nanomaterials and Proteins[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
Copyright © 2006-2016 Editorial office of Acta Physico-Chimica Sinica
Address: College of Chemistry and Molecular Engineering, Peking University, Beijing 100871, P.R.China
Service Tel: +8610-62751724 Fax: +8610-62756388 Email:whxb@pku.edu.cn
^ Top