ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2001,Vol.17>> Issue(02)>> 177-180     doi: 10.3866/PKU.WHXB20010218         中文摘要
Preparation of TiO2 Nanoparticles by Hydrothermal Method and its Application for Photoelectrochemical Cell
Gao En-Qin;Zhang Li;Yang Mai-Zhi;Cai Sheng-Min
College of Chemistry and Molecular Engineering,Peking University,Beijing 100871;Suzhou Teacher′s College,Su Zhou 234000
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By varying the hydrolysis and hydrothermal processing parameters in preparing TiO2 nanoparticles different sizes of TiO2 nanoparticles are obtained.(1) At higher autoclaving temperature,lower pH and longer autoclaving period,larger sizes of TiO2 nanoparticles are prepared.(2) The nanoporous electrodes made from sintering smaller TiO2 nanoparticles show relatively poor IPCE and low absorption in UVVis spectrum,(3) Higher IPCE can be achieved with TiO2 nanoporous electrodes made from sintering larger TiO2 nanoparticles.These electrodes are suitable for studying behavior of the photoelectrochemistry of dye sensitized nanoporous electrodes.

Keywords: Hydrothermal method   TiO2 nanoparticle   Dye sensitization    Photoelectrochemistry  
Received: 2000-05-01 Accepted: 2000-09-14 Publication Date (Web): 2001-02-15
Corresponding Authors: Cai Sheng-Min Email:

Cite this article: Gao En-Qin;Zhang Li;Yang Mai-Zhi;Cai Sheng-Min. Preparation of TiO2 Nanoparticles by Hydrothermal Method and its Application for Photoelectrochemical Cell[J]. Acta Phys. -Chim. Sin., 2001,17 (02): 177-180.    doi: 10.3866/PKU.WHXB20010218
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90. ZHANG Qiao-Bao, FENG Zeng-Fang, HAN Nan-Nan, LIN Ling-Ling, ZHOU Jian-Zhang, LIN Zhong-Hua.Preparation and Photoeletrochemical Performance of CdS Quantum Dot Sensitized ZnO Nanorod Array Electrodes[J]. Acta Phys. -Chim. Sin., 2010,26(11): 2927-2934
91. QIAN Di-Feng, ZHANG Qing-Hong, WAN Jun, LI Yao-Gang, WANG Hong-Zhi.Enhancing the Photovoltaic Performance of Dye Sensitized Solar Cells with the TiO2 Sol Infiltrated Nanocrystalline Electrode[J]. Acta Phys. -Chim. Sin., 2010,26(10): 2745-2751
92. LI Wen-Zhang, LI Jie, WANG Xuan, ZHANG Shu-Juan, CHEN Qi-Yuan.Photoelectrochemical Properties of Cubic Tungsten Trioxide Films Obtained by the Polymeric Precursor Method[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2343-2348
93. ZHU Yan-Feng, DU Rong-Gui, LI Jing, QI Hai-Qing, LIN Chang-Jian.Photogenerated Cathodic Protection Properties of a TiO2 Nanowire FilmPrepared by a Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2349-2353
94. WANG Wen-Li, LIN Hong, ZHANG Luo-Zheng, LI Xin, CUI Bai, LI Jian-Bao.Electrochemical Impedance Spectroscopy Analysis of an Electrophoretic Titania Nanotube/Nanoparticle Composite Film[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1249-1253
95. HE Yue, DONG Mei, LI Jun-Fen, WANG Jian-Guo, FAN Wei-Bin.Synthesis and Catalytic Properties of MeAPO-5 Molecular Sieves for Selective Oxidation of Cinnamyl Alcohol[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1305-1310
96. ZHAN Wei-Shen, PAN Shi, LI Yuan-Zuo, CHEN Mao-Du.Molecular Design of D5 Analogues for Dye-Sensitized Solar Cells[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1408-1416
97. ZHANG Ai-Ping, ZHANG Jin-Zhi.Syntheses and Activities of Visible-Light-Driven Cu/BiVO4 Composite Photocatalysts[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1337-1342
98. TAO Li, YANG Yan-Zhen, SHI Cheng-Wu, WU Yu-Cheng, WU Xiao-Yan.Improved Preparation of Benzothiazolium Iodides and Their Application in Dye Sensitized Solar Cells[J]. Acta Phys. -Chim. Sin., 2010,26(03): 578-582
99. YAN Dong-Xia, WANG Hua, LI Kong-Zhai, WEI Yong-Gang, ZHU Xing, CHENG Xian-Ming.Structure and Catalytic Property of Ce1-xFexO2 Mixed Oxide Catalysts for Low Temperature Soot Combustion[J]. Acta Phys. -Chim. Sin., 2010,26(02): 331-337
100. JIANG Lei, HUANG Hui, WANG Chun-Tao, ZHANG Wen-Kui, GAN Yong-Ping, TAO Xin-Yong.Photoelectrochromic Properties of TiO2-xNx/NiO Bilayer Thin Films[J]. Acta Phys. -Chim. Sin., 2010,26(02): 299-303
101. XU Xin, WANG Xiao-Jing, HU Zhong-Hua, LIU Ya-Fei, WANG Chen-Chen, ZHAO Guo-Hua.Influence of Sol-Gel and Dip-Hydrothermal Preparation Methods on Structure and Performance of TiO2/AC Photocatalysts[J]. Acta Phys. -Chim. Sin., 2010,26(01): 79-86
102. LI Wen, LENG Wen-Hua, NIU Zhen-Jiang, LI Xiang, FEI Hui, ZHANG Jian-Qing, CAO Chu-Nan.Enhanced Photoelectrochemical Performance of WO3 Film Electrode under Visible Light by Electrochemical Etching Fluorination in Aqueous Solutions Containing Fluorine[J]. Acta Phys. -Chim. Sin., 2009,25(12): 2427-2432
103. ZHAN Wei-Shen, PAN Shi, LI Yuan-Zuo, CHEN Mao-Du.A Comparison of Indoline Dyes as Photosensitizers in Dye-Sensitized Solar Cells[J]. Acta Phys. -Chim. Sin., 2009,25(10): 2087-2092
104. WANG Run-Han, JIANG Ji-Sen, HU Ming.Controlled Syntheses of FeNi3 Alloy Nanostructures via Reverse Microemulsion-Directed Hydrothermal Motheds[J]. Acta Phys. -Chim. Sin., 2009,25(10): 2167-2172
105. DONG Xiang, TAO Jie, LI Ying-Ying, WANG Tao, ZHU Hong.Photoelectrochemical Properties of Three-Dimensional Network TiO2 Nanowire Film Prepared by Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2009,25(09): 1874-1882
106. LV Yong, LU Wen-Cong, ZHANG Liang-Miao, YUE Bao-Hua, SHANG Xing-Fu, NI Ji-Peng.Synthesis, Characterization and Growth Mechanism of Core/Shell AlOOH Microspheres[J]. Acta Phys. -Chim. Sin., 2009,25(07): 1391-1396
107. YANG Shu-Ming, KOU Hui-Zhi, WANG Ling, WANG Hong-Jun, FU Wen-Hong.Photoelectrochemical Properties of N3 Sensitized Ho3+ Modified TiO2 Nanocrystalline Electrodes[J]. Acta Phys. -Chim. Sin., 2009,25(06): 1219-1224
108. CHEN Qi-Feng, JIANG Dong, XU Yao, WU Dong, SUN Yu-Han.Visible Region Photocatalysis of Ce-Si/TiO2 Synthesized Using Sol-Gel-Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2009,25(04): 617-623
109. ZHANG Cai-Rong; WU You-Zhi; CHEN Yu-Hong; CHEN Hong-Shan.Geometries, Electronic Structures and Related Properties of Organic Dye Sensitizers JK16 and JK17[J]. Acta Phys. -Chim. Sin., 2009,25(01): 53-60
110. YU Zhi-Yong; ZHANG Wei; MA Ming; CUI Xiao-Li.Visible Light Photoelectrochemical Response of Nitrogen-Doped TiO2 Thin Films Prepared by Anodic Oxidation of Titanium Nitride Films[J]. Acta Phys. -Chim. Sin., 2009,25(01): 35-40
111. SHI Cheng-Wu, GE Qian, LI Bing, TAO Li, LIU Qing-An.Influence of Additives on the Performance of Electrolytes in Dye-Sensitized Solar Cells[J]. Acta Phys. -Chim. Sin., 2008,24(12): 2327-2330
112. ZHAO Rui-Hua, DONG Mei, QIN Zhang-Feng, DING Jian-Fei, GUO Xing-Cui, WANG Jian-Guo.Synthesis and Characterization of CoAPO-5 with different Cobalt Contents and Their Catalytic Performance for Cyclohexane Oxidation[J]. Acta Phys. -Chim. Sin., 2008,24(12): 2304-2308
113. ZHANG Wei; CUI Xiao-Li; JIANG Zhi-Yu.Effect of Composite Modes on Photoelectrochemical Properties of MWCNTs/TiO2 Nanocomposite Films[J]. Acta Phys. -Chim. Sin., 2008,24(11): 1975-1980
114. LI Hai-Long; LUO Wu-Lin; CHEN Tao; TIAN Wen-Yu; SUN Mao; LI Chun; ZHU Di; LIU Ran-Ran; ZHAO Yu-Liang; LIU Chun-Li.Preparation and Photocatalytic Performance of Titania Nanotubes Loaded with Ag Nanoparticles[J]. Acta Phys. -Chim. Sin., 2008,24(08): 1383-1386
115. WANG Bai-Qi; XIA Chun-Hui; FU Qiang; WANG Peng-Wei; SHAN Xu-Dong; YU Da-Peng.Hydrothermal Preparation and Photoluminescence Property of Co-Doped ZnO Nanorods[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1165-1168
116. CHEN Qiao-Lin; ZHOU Jian-Zhang; LIANG Jin-Ling; LIN Ling-Ling; LIN Zhong-Hua.Spectroscopic and Photoelectrochemical Properties of DNA/CdS Nanoparticle Composites[J]. Acta Phys. -Chim. Sin., 2008,24(05): 749-754
117. ZHU Lv-Jun; XU Qun-Jie; CAO Wei-Min; WAN Zong-Yue; ZHOU Guo-Ding; LIN Chang-Jian.Photoelectrochemical Study on the Complex of PASP and Tungstate as Inhibitors of Cupronickel B10’s Corrosion[J]. Acta Phys. -Chim. Sin., 2008,24(05): 805-809
118. CAO Ji-Lin; XING Dong-Qiang; LIU Xiu-Wu; TAN Zhao-Yang.Synthesis of Magnetic 4A Zeolite at Ultrasonic Condition[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1893-1898
119. MAN Yi; ZONG Rui-Long; ZHU Yong-Fa.Preparation and Photoelectrochemical Properties of Bi2MoO6 Films[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1671-1676
120. ZHU Lei; CUI Xiao-Li; SHEN Jie; YANG Xi-Liang; ZHANG Zhuang-Jian.Visible Light Photoelectrochemical Response of Carbon-doped TiO2 Thin Films Prepared by DC Reactive Magnetron Sputtering[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1662-1666
121. SHI Cheng-Wu; GE Qian; QIU Zhi-Guo; LI Bing; HAN Shi-Kui.Synthesis of 3-hexyl-1-methylimidazolium Iodide and Its Application in Dye-Sensitized Solar Cells[J]. Acta Phys. -Chim. Sin., 2007,23(09): 1473-1477
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130. PAN Xu; DAI Song-yuan; WANG Kong-jia; SHI Cheng-wu; GUO Li.Development and Application of Electrolyte based on Ionic Liquid in Dye-sensitized Solar Cells[J]. Acta Phys. -Chim. Sin., 2005,21(06): 697-702
131. SHI Cheng-Wu; DAI Song-Yuan; WANG Kong-Jia; GUO Li; PAN Xu; KONG Fan-Tai; HU Lin-Hua.Optimization of 1,2-dimethyl-3-propylimidazolium Iodide Concentration in Dye-sensitized Solar Cells[J]. Acta Phys. -Chim. Sin., 2005,21(05): 534-538
132. Guo Jia-Hao;He Xiao-Ying;Guo Min;Cai Sheng-Min;Chen Xiu-Ying;Peng Xiao-Jun.Photoelectrochemical Studies of the TiO2 Nanocrystalline Electrode Sensitized by Novel Cyanine Dye[J]. Acta Phys. -Chim. Sin., 2004,20(08): 849-853
133. Cai Wei-Quan;Li Hui-Quan;Zhang Yi.Hydrothrmal Crystal Growth of Very Light Boehmite products[J]. Acta Phys. -Chim. Sin., 2004,20(07): 717-721
134. Guo Min;Diao Peng;Ren Yan-Jie;Wang Bin;Cai Sheng-Min.Preparation and Characterization of Highly Oriented ZnO Single Crystal Submicrorod Arrays[J]. Acta Phys. -Chim. Sin., 2003,19(05): 478-480
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