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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2005,Vol.21>> Issue(03)>> 300-305     doi: 10.3866/PKU.WHXB20050315         中文摘要
Study of the Microstructure of TEOS-MTES Based Sol by SAXS
XU Hua; XU Yao; LI Zhi-Hong
Taiyuan Institute of Plastic, Taiyuan 030024; State Key Laboratory of Coal Conversion, Institute of Coal Chemistry, Chinese Academy of Sciences, Taiyuan 030001; Laboratory of Synchrotron Radiation, Institute of High Energy Physics, Chinese Academy of Sciences, Beijing 100039
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Polymer-modified silica sols were synthesized by the ammonia-catalyzed hydrolysis of tetraethoxysilane with polyvinylpyrrolidone (PVP) as polymer modifier in methyl alcohol. By small angle X-ray scattering (SAXS), the microstructure was studied with the assistance of dynamic light scattering (DLS). The dependence of the particle size distribution, fractal characteristics, and the rheology of PVP-modified silica sols on the PVP content, ammonia content and water content in sols was analyzed. It is easy to form hydrogen bonds between the surface hydroxyls of silica particles and the negatively charged oxygen atoms of inner amide in PVP molecules, and this holds back the further growth of silica particles. Thus the gelation was retarded and the rheology of the sol was largely modified by PVP.

Keywords: Sol   Silica   Small angle X-ray scattering   Rheology  
Received: 2004-07-20 Accepted: 2004-10-25 Publication Date (Web): 2005-03-15
Corresponding Authors: XU Yao Email: xuyaoc@yahoo.com.cn


Cite this article: XU Hua; XU Yao; LI Zhi-Hong. Study of the Microstructure of TEOS-MTES Based Sol by SAXS[J]. Acta Phys. -Chim. Sin., 2005,21 (03): 300-305.    doi: 10.3866/PKU.WHXB20050315
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90. ZHANG Liang-Miao; FENG Yong-Li; LU Wen-Cong; CHEN Nian-Yi.Synthesis of Nano-Alumina Hydroxide Sol Using Sol-gel Method[J]. Acta Phys. -Chim. Sin., 2007,23(05): 728-732
91. WANG Huan-Ping; ZHANG Qi-Long; YANG Hui; SUN Hui-Ping.Synthesis and Microwave Dielectric Properties of (Ca1-xMgx)SiO3 Ceramic by Sol-Gel Process[J]. Acta Phys. -Chim. Sin., 2007,23(04): 609-613
92. HAO Zhi-Xian;LIU Hui;GUO Bin;LI Hong;ZHANG Jia-Wei;GAN Li-Hua;XU Zi-Jie;CHEN Long-Wu.Sol-Gel Synthesis of Alumina Using Inorganic Salt Precursor[J]. Acta Phys. -Chim. Sin., 2007,23(03): 289-294
93. ZOU Xing-Quan;WU Ping;LI Qiang;XIAO Tan
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94. ZHOU Hong-Wei;LI Huai-Xiang;JIANG Zheng-Wei;ZUO Xiang-Qing.Treatment of ZnS:Mn Phosphors by Partial Sublimation of SnO2:Sb Xerogel[J]. Acta Phys. -Chim. Sin., 2007,23(01): 88-91
95. ZHU Lu-Ping;HUANG Wen-Ya;MA Li-Li;FU Shao-Yun;YU Ying;JIA Zhi-Jie.Synthesis and Characteristics of ZnO-CNTs Nanocomposites[J]. Acta Phys. -Chim. Sin., 2006,22(10): 1175-1180
96. ZHAO Chun-Xia;CHEN Wen;LIU Qi;TIAN Gao.Influence of HCl on the Mesostructure and Morphology of the Ordered Mesoporous Silica[J]. Acta Phys. -Chim. Sin., 2006,22(10): 1201-1205
97. QIAO Bin;TANG Zi-Long;ZHANG Zhong-Tai;CHEN Lei.Photoluminescent and Electroluminescent Characteristics of ZnGa2O4:Cr3+ Red Phosphor[J]. Acta Phys. -Chim. Sin., 2006,22(10): 1291-1295
98. WU Qiu-Mei;RUAN Jian-Ming;HUANG Bai-Yun;ZHOU Zhong-Cheng;ZOU Jian-Peng.Viscoelastic Behavior and the Ability of Dissipating Energy of SiO2 Dispersions under Stress Shear[J]. Acta Phys. -Chim. Sin., 2006,22(09): 1075-1078
99. FENG Chun-Bo;DU Zhi-Ping;Zhao Yong-Hong;TAI Xiu-Mei;LI Qiu-Xiao .Photocatalytic Activity of Au Modified Nano-TiO2 for NPE-10 Degradation[J]. Acta Phys. -Chim. Sin., 2006,22(08): 953-957
100. ZHANG Zhi-Qiang;QU Yi-Xin;REN Hui.Density Functional Theory Studies on Ethanol Physisorption on Ultrafine Silica[J]. Acta Phys. -Chim. Sin., 2006,22(07): 820-825
101. WANG Xiao-Dong;DONG Peng;CHEN Sheng-Li.Preparation of Macroporous Al2O3 by Template Method[J]. Acta Phys. -Chim. Sin., 2006,22(07): 831-835
102. LIU Yi-An;XUE Cheng-Shan;ZHUANG Hui-Zhao;ZHANG Xiao-Kai;TIAN De-Heng;WU Yu-Xin;SUN Li-Li;AI Yu-Jie;WANG Fu-Xue.Structure and Synthesis of GaN Powder by Sol-Gel Method[J]. Acta Phys. -Chim. Sin., 2006,22(06): 657-660
103. ZHANG Ai-Ping;FANG Yan.The Effect of Anions on Silver Colloids Aggregation[J]. Acta Phys. -Chim. Sin., 2006,22(06): 756-760
104. SUI Zhen-Ming;CHEN Xiao;WANG Lu-Yan;XU Li-Mei;YANG Chun-Jie.Study on the Doping and Interactions of Metal Nanoparticles in the Lyotropic Liquid Crystals[J]. Acta Phys. -Chim. Sin., 2006,22(06): 737-743
105. HUANG Ming-Qiang;HAO Li-Qing;ZHOU Liu-Zhou;GU Xue-Jun;WANG Zhen-Ya;FANG Li;ZHANG Wei-Jun.Chemical Composition and Reaction Mechanisms for Secondary Organic Aerosol from Photooxidation of Ethylbenzene[J]. Acta Phys. -Chim. Sin., 2006,22(05): 596-601
106. WANG Zhou-Cheng;HUANG Long-Men;TANG Yi;NI Yong-Jin;LIN Chang-Jian.Preparation of Co-YSZ/HAp Nano-composite Coating on Ti Substrate by Electrochemical Method[J]. Acta Phys. -Chim. Sin., 2006,22(05): 590-595
107. YE Qing; XU Bo-Qing.Textural and Structure Characterizations of Ce1-xMnxO2Prepared by Citric Acid Sol-Gel Method[J]. Acta Phys. -Chim. Sin., 2006,22(03): 345-349
108. WU Qiu-mei; RUAN Jian-ming; ZHOU Zhong-cheng; HUANG Bai-yun.Study on the Rheological Properties of Silica /Polyethylene Glycol Non-Newtonian Flow[J]. Acta Phys. -Chim. Sin., 2006,22(01): 48-52
109. YE Qing; WANG Rui-pu; XU Bo-qing.Structure and Oxygen Mobility of Ce1-xZrxO2 Prepared by Citric Acid Sol-gel Method[J]. Acta Phys. -Chim. Sin., 2006,22(01): 33-37
110. WANG Hong-Xia;ZHANG Gao-Yong;LIU Dian-Sheng;ZHANG Xin-Wei;XIAO Yong-Hong.Small Amplitude Oscillation Frequency Sweep of Lamellar Liquid Crystal[J]. Acta Phys. -Chim. Sin., 2005,21(12): 1411-1414
111. ZHUANG Wen-chang; CHEN Xiao; YANG Chun-jie; WANG Lu-yan; CHAI Yong-cun.Study of Ordering for AOT/Water Lamellar Lyotropic Liquid Crystal: Small-angle X-ray Scattering Experiments[J]. Acta Phys. -Chim. Sin., 2005,21(09): 1055-1058
112. LIU Rui-quan; XIE Ya-hong; LI Zhi-jie; WANG Ji-de; SUN Yi-gang.Application of Proton Conductors (Ce0.8La0.2)1-xCaxO2-δ in Synthesis of Ammonia[J]. Acta Phys. -Chim. Sin., 2005,21(09): 967-970
113. PENG Feng; CHEN Shui-hui; ZHANG Lei; WANG Hong-juan; XIE Zhi-yong.Preparation of Visible-light Response Nano-sized ZnO Film and Its Photocatalytic Degradation to Methyl Orange[J]. Acta Phys. -Chim. Sin., 2005,21(08): 944-948
114. LI Li-chun; GUAN Jian-guo; CHENG Hai-bin; TAO Jian-qing.Preparation of Poly(ethylene glycol)-coated Carbonyl Iron Particles for Aqueous Magnetorheological Suspension[J]. Acta Phys. -Chim. Sin., 2005,21(07): 817-821
115. HE Jian; HUANG Yun-hua; ZHANG Yue; GU You-song; JI Zhen; ZHOU Cheng.Synthesis, Growth Mechanism and Microstructure of ZnO Nanocables[J]. Acta Phys. -Chim. Sin., 2005,21(06): 637-640
116. JING Li-Qiang; FU Hong-Gang; WANG De-Jun; WEI Xiao; SUN Jia-Zhong.Surface Photoinduced Charge Separation and Photocatalytic Activity of Sn Doped TiO2 Nanoparticles[J]. Acta Phys. -Chim. Sin., 2005,21(04): 378-382
117. LI Zhi-Jie; HOU Bo; XU Yao; WU Dong; SUN Yu-Han.Preparation and Characterization of Silica-modified Titanium Dioxide Nanoparticles by Co-precipitation Method[J]. Acta Phys. -Chim. Sin., 2005,21(03): 229-233
118. YANG Xiao-Guang;DONG Peng;ZHOU Ya-Song;LIU Tao;ZHANG Jing;XIEYa-Ning;HU Tian-Dou.The Local Structure of Titania-Silica Composite Oxides[J]. Acta Phys. -Chim. Sin., 2005,21(01): 33-37
119. WU Yu-Cheng;YANG Ye;LI Yong;CUI Ping.Effect of Addition of Alumina Sol on γαPhase Transformation of Ultrafined Alumina[J]. Acta Phys. -Chim. Sin., 2005,21(01): 79-83
120. GE Xiu-Tao;FANG Da-Ru;LIU Xing-Qin.The Preparation and Gas-sensing Properties of Ga2O3-NiO Complex Oxide by Sol-gel Method[J]. Acta Phys. -Chim. Sin., 2005,21(01): 10-15
121. Zhou Xing-Fu; Zhao Jun-Feng; He Hui; Chu Dao-Bao.Electrochemical Dissolution of Tin in Ethylene Glycol Monomethyl Ether and Direct Hydrolysis of the Electrolyte for Preparation of Nano-sized SnO2[J]. Acta Phys. -Chim. Sin., 2004,20(12): 1472-1475
122. Wang Juan; Zhang Chang-Rui; Feng Jian.Modification of Nanoporous Silica Film by Trimethylchlorosilane[J]. Acta Phys. -Chim. Sin., 2004,20(12): 1399-1403
123. Li Yu;Zhang Xiao-Bin;Tao Xin-Yong;Wang You-Wen;Liu Fu;Xu Guo-Liang.Ni-Mo Bi-Metallic Oxide Catalyst for Large-scale Synthesis of Bundled Multi-walled Carbon Nanotubes by CVD[J]. Acta Phys. -Chim. Sin., 2004,20(10): 1233-1238
124. Zhang Shi-Cheng;Li Chun-He;Li Xing-Guo.Size Control and Characterization of ZnO Nanoparticles[J]. Acta Phys. -Chim. Sin., 2004,20(08S): 902-905
125. Liu Ying-Xin;Wei Zuo-Jun;Chen Ji-Xiang;Zhang Ji-Yan;Li Xin-Xue;Wei Xiong-Hui.Sol-gel Preparation,Characterization and Hydrogenation Property of Silica Supported Ni Catalyst[J]. Acta Phys. -Chim. Sin., 2004,20(07): 780-784
126. Ouyang Jian-Hua;Wu Nian-Zu;Zhao Xin-Sheng.The Role of Sulfite in the Wetting Etching of Silicon and Silica[J]. Acta Phys. -Chim. Sin., 2004,20(06): 612-615
127. Wang Hui;Zhang Xiu-Juan;Zhang Xiao-Hong;Wu Shi-Kang.The Preparation of Nano-sized Silica Gel Suspension and the Recognition of Transition Metal Cations[J]. Acta Phys. -Chim. Sin., 2004,20(03): 313-317
128. Zhou Jian-Fang;Zhang Li-Ming;Peter S. Hui.Rheological Characteristics of Aqueous Solutions of an Amphoteric Guar Gum Derivative[J]. Acta Phys. -Chim. Sin., 2003,19(11): 1081-1084
129. He Chong-Heng;Wang Ren.The Properties of Pd Catalysts Prepared by Sol-gel Method[J]. Acta Phys. -Chim. Sin., 2003,19(10): 952-956
130. Ren Da-Sen;Cui Xiao-Li;Zhang Qun;Wo Song-Tao;Yang Xi-Liang;Zhang Zhuang-Jian;Lu Ming.Characteristics of SiO2-TiO2 Complex Thin Films Prepared by Sol Method[J]. Acta Phys. -Chim. Sin., 2003,19(09): 829-833
131. Wei Jian-Hong;Shi Jing;Guan Jian-Guo;Yuan Run-Zhang.Surface Modification of PAn Particles[J]. Acta Phys. -Chim. Sin., 2003,19(07): 657-660
132. Yang Tong-Zai;Chen Yin-Liang;Xiong Wang;Yang Yan-Qiu;Ma Jun;Ye Shi-You;Liu Yi-Nong;Yu Zhong-Jin;Song Tao.Experimental Measurements of Distribution of Retention Time for Aerosol Particles through Packed Column[J]. Acta Phys. -Chim. Sin., 2003,19(07): 605-609
133. Gan Li-Hua;Chen Long-Wu;Zhang Yu-Xing.Preparation of Silica Aerogels by Nonsupercritical Drying[J]. Acta Phys. -Chim. Sin., 2003,19(06): 504-508
134. Zhao Yong-Xiang;Qin Xiao-Qin;Hou Xi-Cai;Xu Xian-Lun;Liu Dian-Sheng.Preparation,Characterization and Properties of Selective Hydrogenation on Ni-based Catalysts[J]. Acta Phys. -Chim. Sin., 2003,19(05): 450-454
135. Hou Ji-Rui;Liu Zhong-Chun;Zhang Shu-Fen;Yue Xiang-An;Yang Jin-Zong.Effect of Alkali on Molecular Configuration of Polymer and Its Rheologic Behavior[J]. Acta Phys. -Chim. Sin., 2003,19(03): 256-259
136. Ruan Sheng-Ping;Dong Wei;Wu Feng-Qing;Wang Yong-Wei;Yu Tao;Peng Zeng-Hui;Xuan Li.Dielectric Properties of Nanocrystalline BaTiO3[J]. Acta Phys. -Chim. Sin., 2003,19(01): 17-20
137. Qin Cao;Wang Ting-Jie;Jin Yong.The Coating Process of Nano-scale Hydrous Silica Film on TiO2 Particles by Chemical Deposition in Aqueous Solution[J]. Acta Phys. -Chim. Sin., 2002,18(10): 884-889
138. Xu Yao;Li Zhi-Hong;Wang Jun;Fan Wen-Hao;Wu Dong;Dong Bao-Zhong;Sun Yu-Han.Study of the Microstructure of TEOS-MTES Based Sol by SAXS[J]. Acta Phys. -Chim. Sin., 2002,18(09): 781-785
139. Zhou Xing-Fu;Han Ai-Jie;Chu Dao-Bao;Lin Chang-Jian;Tian Zhong-Qun.Preparation of Nanocrystalline NiO by Electrochemical Dissolution of Nickel[J]. Acta Phys. -Chim. Sin., 2002,18(07): 613-616
140. Zhao Zhuan-Qing;Yao Su-Wei;Zhang Wei-Guo;Gong Zheng-Lie.Preparation and Photoelectrochemical Performance of Photoelectrode of TiO2 Film on Nickel[J]. Acta Phys. -Chim. Sin., 2002,18(05): 473-476
141. Zhang Ye;Wu Dong;Sun Yu-Han;Peng Shao-Yi.Synthesis and Properties of Hydrophobic & Antireflective Silica Coating[J]. Acta Phys. -Chim. Sin., 2002,18(04): 355-358
142. Ma Jian-Hua;Wu Guang-Ming;Cheng Yin-Bing;Sun Qi;Wang Jun-Ling;Shen Jun;Wang Jue.Preparation of Hydrophobic Optical Silica Thin Film with Sol-gel Method[J]. Acta Phys. -Chim. Sin., 2001,17(12): 1112-1116
143. Yu Hai-Hu;Wu Hong-Biao;Li Xiao-Fu;Zhu Yun-Zhou;Jiang De-Sheng.Self-assembly and Optical Properties of Silica Nanoparticulate Thin Films[J]. Acta Phys. -Chim. Sin., 2001,17(12): 1057-1061
144. Zou Ling;Wu Xue-Dong;Chen Hai-Gang;Wang Da-Pu.Structural Characterization and Formation Mechanism of SurfaceModified Titanium Dioxide Nanoparticles[J]. Acta Phys. -Chim. Sin., 2001,17(04): 305-309
145. Yu Jia-Guo;Zhao Xiu-Jian;Chen Wen-Mei;Lin Li;Zhang Ai-Li.Photocatalytic Activity and Hydrophilic Property of TiO2/SiO2 Composite Nanometer Thin Films[J]. Acta Phys. -Chim. Sin., 2001,17(03): 261-264
146. Shui Miao;Yue Lin-Hai;Xu Zhe-De.Photocatalytic Activity of Iron Doping TiO2 Prepared by Several Methods[J]. Acta Phys. -Chim. Sin., 2001,17(03): 282-285
147. Zhang Yu-Hong;Xiong Guo-Xing;Yang Wei-Shen;Fu Xian-Zhi.Preparation of MxOy-TiO2 Photocatalysts by Sol-gel Method[J]. Acta Phys. -Chim. Sin., 2001,17(03): 273-277
148. Wang Tong-Wen;Dai Le-Rong.Synthesis of Hexagonal Mesostructured Titaniumcontaining Silica by Mixed Supramolecular Templating[J]. Acta Phys. -Chim. Sin., 2001,17(01): 10-14
149. Yan Xiu-Ru;Li Xiao-Hong;Huo Ming-Liang;Guo Wei-Wei;Gong Yong-Jin.Preparation and Photocatalytic Properties of Nanometer SnO2@TiO2[J]. Acta Phys. -Chim. Sin., 2001,17(01): 23-27
150. Wu Hong-Ying;Wang Xi-Gui;Xie Da-Tao;Weng Shi-Fu;Wu Jin-Guang.Structure and Luminescence Properties of Tb-doped Sibased Light-emitting[J]. Acta Phys. -Chim. Sin., 2001,17(01): 53-58
151. Yu Jia-Guo, Zhao Xiu-Jian, Zhao Qing-Nan.Preparation and Characterization of TiO2 Nnometer Thin Films by Sol-gel Process[J]. Acta Phys. -Chim. Sin., 2000,16(09): 792-797
152. Wang Tong-Wen, Chen Jing-Lei, Dai Le-Rong.Synthesis of Cubic Mesoporous Titanium-containing Silica by Mixed Surfactant Templating[J]. Acta Phys. -Chim. Sin., 2000,16(05): 385-388
153. Li Qing-Lian, Chen Shou-Tian, Yao Pu, Wei Guo, Qu Yong-He.Thermal Decomposation Mecharism of the Nano-BaTiO2 Formation[J]. Acta Phys. -Chim. Sin., 2000,16(02): 170-174
154. Zhu Zi-Hua, Zhu, Z. H., Zhu Tao, Liu Zhong-Fan.Prepartion of Gold Sols of Large Size Particles[J]. Acta Phys. -Chim. Sin., 1999,15(11): 966-970
155. Bian Guo-Zhu, Han Bo, Fu Yi-Lu.Sol-gel Method Preparation and Characterization of NiMoO4 Ultrafine Particle Catalyst[J]. Acta Phys. -Chim. Sin., 1999,15(11): 1001-1004
156. Zhu Yong-Fa, Zhang Li, Gao Chong, Yao Wen-Qing, Cao Li-Li.The Preparation of Nanosized Anatase TiO2 Powder by Using TiCl4 a Precursor[J]. Acta Phys. -Chim. Sin., 1999,15(09): 784-788
157. Zhang Yu-Hong, Xiong Guo-Xing, Sheng Shi-Shan, Liu Sheng-Lin, Yang Wei-Shen.Interaction of NiO with γ-Al2O3 Supporter of NiO/γ-Al2O3 Catalysts[J]. Acta Phys. -Chim. Sin., 1999,15(08): 735-741
158. Gan Li-Hua, Li Guang-Ming, Yue Tian-Yi, Zhang Ming, Wu Jian-Wen, Chen Long-Wu.Preparation of Fe2O3-SiO2 Aerogels by Supercritical Drying Technique[J]. Acta Phys. -Chim. Sin., 1999,15(07): 588-592
159. Chen Hong-Shan, Ji Sheng-Fu, Niu Jian-Zhong, Xie Bao-Han, Li Shu-Ben.Vibration Spectroscopy on Transformation of Amorphous Silica to α-cristobalite[J]. Acta Phys. -Chim. Sin., 1999,15(05): 454-457
160. Wang Cheng, Liu Lei, Li Yu-Fen.Energies and Structures of (SiO2)n Clusters[J]. Acta Phys. -Chim. Sin., 1999,15(02): 143-149
161. Yang Li-Qun, Xie Zhi-Ming, Li Zhuo-Mei.Coordination-crosslinking of Acrylate Copolymer Soap-free Hydrosol with Metal lon[J]. Acta Phys. -Chim. Sin., 1999,15(01): 28-34
162. Hu Bo-Lu, Hang Hu, Sun Yong, Chen Zong-Qi.Flocculation of Silica Suspensions[J]. Acta Phys. -Chim. Sin., 1999,15(01): 87-90
163. Yang Ru, Hu Tian-Dou, Liu Tao, Xiang Hong-Wei, Zhong Bing, Xu Yao, Wu Dong.Characterization of CuO-BaO/SiO2 Catalysts Structure[J]. Acta Phys. -Chim. Sin., 1998,14(07): 590-596
164. Dong Peng.Preparation of Monodisperse Silica Spheres by Growth of Silica Sol Particles[J]. Acta Phys. -Chim. Sin., 1998,14(02): 109-114
165. Huang Jian-Bin, Dai Qing-Hong, Gui Lin-Lin.The Preparation of Quantum-dot CdS Doped Silica Glass by the Improved Sol-gel Process[J]. Acta Phys. -Chim. Sin., 1998,14(01): 13-20
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169. Wang Jian,Zhu Tao,Liu Zhong-Fan.Fabricating SERS-Active Substrate by Assembling of Au Nanoparticles[J]. Acta Phys. -Chim. Sin., 1996,12(11): 961-964
170. Hou Wen-Hua,Wang Nan-Ping,Yan Qi-Hao.Preparation of Layered Ferrititanate Pillared by Silica[J]. Acta Phys. -Chim. Sin., 1996,12(10): 933-936
171. Yuan Xun-Dao,Zeng Guang-Fu,Xi Shi-Quan.Study on the Films Forming Process of Nanosized SnO2 Colloid Particles at the Gas-Liquid Interface[J]. Acta Phys. -Chim. Sin., 1996,12(10): 916-920
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174. Zhou Qing-Ye,Li Han,Zhang Bang-Hua,Song Mou-Dao,He Bing-Lin.Synthesis and Rheology of Polyurethane Latex[J]. Acta Phys. -Chim. Sin., 1996,12(08): 751-754
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177. Peng Ding-Kun,Wan Chuan-Hao,Yang Ping-Hua,Liu Jin,Meng Guang-Yao.Physical Chemistry of Controlled-Hydrolysis of Propanol Zirconia Doped with Yttrium Nitrite[J]. Acta Phys. -Chim. Sin., 1996,12(06): 547-550
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179. Wang Wen-Tao,Zhong Bang-Ke.The Preparation and Characterization of Alumina Membranes Supported by Porous Titanium Plate[J]. Acta Phys. -Chim. Sin., 1996,12(01): 85-90
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183. Wang Guang-Xin, Chen Zong-Qi, Wei Jian.Studies on Rheological Behaviours of Aluminum Stearate Benzene Gels[J]. Acta Phys. -Chim. Sin., 1994,10(01): 69-72
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