Acta Phys. -Chim. Sin. ›› 1996, Vol. 12 ›› Issue (12): 1110-1113.doi: 10.3866/PKU.WHXB19961213

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Arc-discharge Synthesis of Endohedral Metallofullerenes Er@ C2n

Sun Da-Yong,Liu Zi-Yang,Guo Xin-Hua,Xu Wen-Guo,Ji Yi-Ping,Liu Shu-Ying   

  1. The Key Laboratory of Applied Spectroscopy,Changchun Institute of Applied Chemistry,Chinese Academy of Sciences,Changchun 130022
  • Received:1996-06-24 Revised:1996-08-10 Published:1996-12-15
  • Contact: Liu Shu-Ying

Abstract:

Endohedral metallofullerenes Er@ C2n were synthesized using the carbonarc discharge method of activating the Er2O3- containing graphite anode in situ and bask-burning technique. A toluene soxhlet and pyridine high-temperature high-pressure extraction technique were employed for the effective extraction of Er@ C2n. The formation of Er@ C2n was confirmed by LD-TOF and DEIMS characterization.

Key words: Fullerenes, Er@ C2n, Arc-discharge synthesis, High-temperature and high-pressure extraction