Article
Visible Region Photocatalysis of Ce-Si/TiO2 Synthesized Using Sol-Gel-Hydrothermal Method
CHEN Qi-Feng, JIANG Dong, XU Yao, WU Dong, SUN Yu-Han
State Key Laboratory of Coal Conversion, Institute of Coal Chemistry, Chinese Academy of Sciences, Taiyuan 030001, P. R. China; Graduate University of the Chinese Academy of Sciences, Beijing 100049, P. R. China
State Key Laboratory of Coal Conversion, Institute of Coal Chemistry, Chinese Academy of Sciences, Taiyuan 030001, P. R. China; Graduate University of the Chinese Academy of Sciences, Beijing 100049, P. R. China
Cerium and silica co-doped nanoscale TiO2 particles were synthesized froma complex compound system of tetrabutyl titanate (TBT), tetraethyl orthosilicate (TEOS) and cerium nitrate hexahydrate (CNH) at 140 ℃. The reaction was carried out in a Teflon-lined steel autoclave with water as the solvent using a sol-gel-hydrothermal method. The obtained materials were characterized by X-ray diffraction, nitrogen adsorption, transmission electron microscopy, UV-visible diffuse reflectance spectroscopy, Fourier transform infrared spectroscopy as well as X-ray photoelectron spectroscopy. We found that all materials were in the anatase phase, even those calcined at 600 ℃, and that the samples possessed large surface areas. Furthermore, Si and Ce were successfully doped into the bulk TiO2. The photocatalytic activity of the doped material was determined by the degradation of Rhodamine B (RB) using visible light irradiation. Results showed that both Ce-doped TiO2 and Ce-Si co-doped TiO2 had better visible photoactivity than pure TiO2. These particles were all prepared using the same conditions. The highest photocatalytic activity for these samples was obtained using Ce/Ti and Si/Ti molar ratios of 0.010 and 0.10, respectively. These ratios are then considered to be the optimal doping dosages.
Keywords: Titania Ce-Si co-doped Sol-gel-hydrothermal method Visible-photocatalysis Rhodamine B
Received: 2008-11-19 Accepted: 2008-12-17 Publication Date (Web): 2009-02-16
Corresponding Authors: XU Yao, XUN Zhu-Han Email: xuyao@sxicc.ac.cn;yhsun@sxicc.ac.cn
Cite this article: CHEN Qi-Feng, JIANG Dong, XU Yao, WU Dong, SUN Yu-Han. Visible Region Photocatalysis of Ce-Si/TiO2 Synthesized Using Sol-Gel-Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2009,25 (04): 617-623. doi: 10.3866/PKU.WHXB20090412
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94． Li Wei-Hua, Hao Yan-Zhong, Qiao Xue-Bin, Wang Yan-Qin, Yang Mai-Zhi, Cheng Hu-Min, Cai Sheng-Min.A Photoelectrochemistry Study of the Photosensitization of Composite Sulfides and Ru(II) Complex for TiO2 Nanoporous Film Electrode[J]. Acta Phys. -Chim. Sin., 1998,14(09): 841-845
95． Zhang Bin, Wan Hong, Zheng Yan-Ke, Ruan Qian, Wu Nian-Zu, Xie You-Chang, Tang You-Qi.Study of Dispersion of MoO3,NiO,ZnO onto Rutile with Low Surface Area[J]. Acta Phys. -Chim. Sin., 1998,14(05): 385-390
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97． Ji Chun-Xin, Wei Zhao-Xin, Xin Qin.Study of WO3 Supported on Different Carrier by TPS[J]. Acta Phys. -Chim. Sin., 1994,10(10): 874-881
98． Wei Zhao-Bin, Xin Qin.Studies of Titania-Alumina as Support for Molybdenum Catalysts[J]. Acta Phys. -Chim. Sin., 1994,10(10): 931-935
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2． HU Long-Xing, XU Dan-Dan, ZOU Lian-Pei, YUAN Hang, HU Xing.Heterogeneous Fenton Oxidation of Refractory Dye Rhodamine B in Aqueous Solution with Mesoporous Fe/SBA-15[J]. Acta Phys. -Chim. Sin., 2015,31(4): 771-782
3． CHEN Ai-Min, BO Ying-Ying, SHAO Chen-Yi, WANG Jing, HU Jun.Synthesis of Single-Crystalline Cu3B2O6/CuB2O4 and Their Photocatalytic Degradation of Methylene Blue under Visible-Light Irradiation[J]. Acta Phys. -Chim. Sin., 2014,30(9): 1713-1719
4． WANG Jing-Sheng, WANG En-Jun, YU Yan-Long, GUO Li-Mei, CAO Ya-An.Visible Light Photocatalytic Activity of an In-Doped TiO2 Thin Film with a Three-Dimensional Ordered Structure[J]. Acta Phys. -Chim. Sin., 2014,30(3): 513-519
5． GU Yong-Qin, WANG Bo, GU Xiu-Quan, ZHAO Yu-Long, QIANG Ying-Huai, ZHANG Shuang, ZHU Lei.Preparation and Characterization of Co3(PO4)2/Ag3PO4 Nanocomposites for Visible-Light Photocatalysis[J]. Acta Phys. -Chim. Sin., 2014,30(10): 1909-1915
6． WANG Xiao-Xia, XU Hua-Long, SHEN Wei, RUHLMANN Laurent, QIN Feng, SORGUES Sébastien, COLBEAU-JUSTIN Christophe.Synthesis of Ternary Hybrid TiO2-SiO2-POM Catalysts and Its Application in Degrading Rhodamine B under Visible Light Illumination[J]. Acta Phys. -Chim. Sin., 2013,29(09): 1837-1841
7． JI Ping-Li, WANG Jin-Gang, ZHU Xiao-Li, KONG Xiang-Zheng.Preparation of Silver Doped TiO2 Hollow Nanoparticles and Characterization of Their Structures and Photocatalytic Properties[J]. Acta Phys. -Chim. Sin., 2012,28(09): 2155-2161
8． ZHAO Peng-Jun, WU Rong, HOU Juan, CHANG Ai-min, GUAN Fang, ZHANG Bo.One-Step Hydrothermal Synthesis and Visible-Light Photocatalytic Activity of Ultrafine Cu-Nanodot-Modified TiO2 Nanotubes[J]. Acta Phys. -Chim. Sin., 2012,28(08): 1971-1977
9． WU Qi, SU Yu-Feng, SUN Lan, WANG Meng-Ye, WANG Ying-Ying, LIN Chang-Jian.Preparation and Visible Light Photocatalytic Activity of Fe-N Codoped TiO2 Nanotube Arrays[J]. Acta Phys. -Chim. Sin., 2012,28(03): 635-640
10． CHEN Shu-Hai, XU Yao, LÜ Bao-Liang, WU Dong.Microwave-Assisted Hydrothermal Synthesis of Ag-Loaded Titania Nanotubes and Their Photocatalytic Performance[J]. Acta Phys. -Chim. Sin., 2011,27(12): 2933-2938
11． CHEN Jin-Yi, LI Nian, LI Jing, ZHU Liang, PENG Chang-Jun.Synthesis and Visible Light Photocatalytic Activity of Cross-Linked Sodium Rectorite/Cu2O Nanocomposites[J]. Acta Phys. -Chim. Sin., 2011,27(04): 932-938
12． LI Guo-Xian, WANG Tao, HE Jian-Ping, ZHOU Jian-Hua, XUE Hai-Rong, MAYi-Ou, HU Yuan-Yuan.Synthesis and Infrared Emissivity of Ordered Mesoporous C-Al2O3-TiO2 Nanocomposites with a Dual Pore System[J]. Acta Phys. -Chim. Sin., 2011,27(01): 248-254
13． HU Yan-Fei, JIANG Gang, MENG Da-Qiao, KONG Fan-Jie.Phase Transition and Thermodynamic Properties of TiO2[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1664-1668
14． ZHAI Xiao-Hui, ZHAO Jun-Yan, CHAO Hui, CAO Ya-An.Light Induced Interfacial Electron Transfer in Rup2P Surface-Sensitized TiO2-Based Films[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1617-1622
15． LI Li, LU Dan, JI Yuan, ZHAO Yue-Hong.Preparation of Nanocomposite Ag/TiO2-ZrO2 and the Microwave Enhanced Photocatalytic Degradation of Methyl Orange[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1323-1329
16． YANG Chang-Hu, MA Zhong-Quan, LI Feng, HE Bo, YUAN Jian-Hui, ZHANG Zhen-Hua.Spectrum Analysis on Phase Transformations in TiO2 Thin Films[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1349-1354
17． ZHANG Shu-Cui, JIANG Dong, TANG Tao, LI Jun-Hua, XU Yao.Synthesis and Photocatalytic Activity of Highly Dispersed TiO2/SBA-15[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1330-1336
18． XU Ling, TANG Chao-Qun, HUANG Zong-Bin.Light Absorption Properties of V-Doped Anatase TiO2[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1401-1407
19． DEDG Pei-Chang, HU Jie-Zhen, WANG Hai-Zeng, SUN Bao-Wei.Hydrothermal Preparation and Photocatalytic Activity of Chlorine Doped Titanium Dioxide Supported on SiO2[J]. Acta Phys. -Chim. Sin., 2010,26(04): 915-920
20． ZHAI Xiao-Hui, LONG Hui-Jin, DONG Jiang-Zhou, CAO Ya-An.Doping Mechanism of N-TiO2/ZnO Composite Nanotube Arrays and Their Photocatalytic Activity[J]. Acta Phys. -Chim. Sin., 2010,26(03): 663-668
21． LIANG Shan, XUE Qun-Ji, CUI Yu-Hong, ZHAO Zhan-Fen.Patterning of TiO2 Thin Films Prepared from Aqueous Solutions[J]. Acta Phys. -Chim. Sin., 2010,26(02): 502-506
22． LI Kui-Ying, LIU Tong, ZHOU Bing-Jing, WEI Sai-Ling, YANG Wei-Yong.Transient Photovoltaic and Surface Photoacoustic Characteristics of Mesoporous Crystalline La-doped TiO2 Nanoparticles[J]. Acta Phys. -Chim. Sin., 2010,26(02): 403-408
23． JIANG Lei, HUANG Hui, WANG Chun-Tao, ZHANG Wen-Kui, GAN Yong-Ping, TAO Xin-Yong.Photoelectrochromic Properties of TiO2-xNx/NiO Bilayer Thin Films[J]. Acta Phys. -Chim. Sin., 2010,26(02): 299-303
24． XU Xin, WANG Xiao-Jing, HU Zhong-Hua, LIU Ya-Fei, WANG Chen-Chen, ZHAO Guo-Hua.Influence of Sol-Gel and Dip-Hydrothermal Preparation Methods on Structure and Performance of TiO2/AC Photocatalysts[J]. Acta Phys. -Chim. Sin., 2010,26(01): 79-86
25． WANG Meng-Ye, WANG Cheng-Lin, XIE Kun-Peng, SUN Lan, LIN Chang-Jian.Fabrication of a Spongelike Nanostructured TiO2 Filmand Its Photocatalytic Activity[J]. Acta Phys. -Chim. Sin., 2009,25(12): 2475-2480
26． CHEN Xun, GENG Qiang, LIU Jun-Feng, DING Zheng-Xin, DAI Wen-Xin, WANG Xu-Xu.Influence of Conducting Substrates on the Photoinduced Hydrophilicity of TiO2 Films[J]. Acta Phys. -Chim. Sin., 2009,25(11): 2237-2242
27． ZHANG Mei-Yi, HE Guang-Zhi, DING Cheng-Cheng, CHEN Hao, PAN Gang.Mechanism of Arsenate (V) Adsorption on TiO2 Surfaces[J]. Acta Phys. -Chim. Sin., 2009,25(10): 2034-2038
28． YANG Qiu-Yun, ZHU Yuan, TIAN Li, PEI Yan, QIAO Ming-Hua, FAN Kang-Nian.Influence of Au/TiO2 Catalyst Preparation Parameters on the Selective Hydrogenation of Crotonaldehyde[J]. Acta Phys. -Chim. Sin., 2009,25(09): 1853-1860
29． SU Bi-Tao, SUN Jia-Xing, HU Chang-Lin, ZHANG Xiao-Hong, FEI Peng, LEI Zi-Qiang.Preparation and Characterization of Fe3+-Doped TiO2 Photocatalytic Fiber Materials[J]. Acta Phys. -Chim. Sin., 2009,25(08): 1561-1566
30． HU Mei-Long, XU Sheng-Ming, BAI Chen-Guang, XU Gang, LV Xue-Wei.Preparation of Spherical TiO2 and Kinetics of Its Hydrolysis Process[J]. Acta Phys. -Chim. Sin., 2009,25(08): 1511-1516
31． LI Li, MA Yu, CAO Yan-Zhen, JI Yuan, GUO Yi-Hang.Preparation of Periodic Mesoporous H6P2W18O62/TiO2(Brij-76) Composite and Microwave Enhanced Photocatalytic Degradation of Monochlorobenzene[J]. Acta Phys. -Chim. Sin., 2009,25(07): 1461-1466
32． CHU Dao-Bao, HE Jian-Guo, HOU Yuan-Yuan, XU Mai, WANG Shu-Xi, WANG Jian, ZHA Long-Wu, ZHANG Xue-Jiao.Electrocatalytic Oxidation of Glyoxal on Ti/NanoTiO2-Pt Modified Electrode[J]. Acta Phys. -Chim. Sin., 2009,25(07): 1434-1438
33． FENG Li-Li, ZHAO Wei, LIU Yang, JIAO Liang, LI Xing-Guo.Photocatalytic Degradation of Rhodamine B by Nanocrystalline TiO2 Loaded into MCM-41 Molecular Sieves[J]. Acta Phys. -Chim. Sin., 2009,25(07): 1347-1351
34． MIN Shi-Xiong, WANG Fang, ZHANG Zhen-Min, HAN Yu-Qi, FENG Lei.Preparation and Photocatalytic Activity of PANI/AMTES-TiO2 Nanocomposite Materials[J]. Acta Phys. -Chim. Sin., 2009,25(07): 1303-1310
35． YANG Shu-Ming, KOU Hui-Zhi, WANG Ling, WANG Hong-Jun, FU Wen-Hong.Photoelectrochemical Properties of N3 Sensitized Ho3+ Modified TiO2 Nanocrystalline Electrodes[J]. Acta Phys. -Chim. Sin., 2009,25(06): 1219-1224
36． TIAN Xi-Lin, TAO Jie, TAO Hai-Jun, BAO Zu-Guo, LI Zhuan-Li, ZHANG Yan-Yan, TANG Yu-Xin.Effect of Quenching on Properties of TiO2 Nanotube Arrays[J]. Acta Phys. -Chim. Sin., 2009,25(06): 1111-1116
37． CAO Yong-Qiang, LONG Hui-Jin, CHEN Yong-Mei, CAO Ya-An.Photocatalytic Activity of TiO2 Films with Rutile/Anatase Mixed Crystal Structures[J]. Acta Phys. -Chim. Sin., 2009,25(06): 1088-1092
38． SHEN Jing-Jing, LIU Chang, ZHU Yu-Dan, LI Wei, FENG Xin, LU Xiao-Hua.Photocatalytic Properties of Mesoporous TiO2 Prepared by Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2009,25(05): 1013-1018
39． SU Rong, XUE Wei-Dong, FENG Yong, WANG Jian-Hua, YI Dan.Sensitization Mechanism of Tris(8-hydroxyquinoline)iron (III) on TiO2 Anatase (101) Surface[J]. Acta Phys. -Chim. Sin., 2009,25(05): 947-952
40． CHEN Qi-Li, TANG Chao-Qun.First-Principles Calculations on Electronic Structures of N/F-Doped and N-F-Codoped TiO2 Anatase (101) Surfaces[J]. Acta Phys. -Chim. Sin., 2009,25(05): 915-920
41． WU Feng, WANG Meng, SU Yue-Feng, CHEN Shi.Surface Modification of LiCo1/3Ni1/3Mn1/3O2 by TiO2-Coating[J]. Acta Phys. -Chim. Sin., 2009,25(04): 629-634
42． HU Mei-Long, BAI Chen-Guang, XU Sheng-Ming, XU Gang, LIANG Dong.Preparation of the Size-Controlled TiO2 with Spherical Morphology[J]. Acta Phys. -Chim. Sin., 2008,24(12): 2287-2292
43． TANG Yu-Xin, TAO Jie, ZHANG Yan-Yan, WU Tao, TAO Hai-Jun, BAO Zu-Guo.Preparation and Characterization of TiO2 Nanotube Arrays via Anodization of Titanium Films Deposited on FTO Conducting Glass at Room Temperature[J]. Acta Phys. -Chim. Sin., 2008,24(12): 2191-2197
44． LI Kui-Ying; GUO Jing; LIU Tong; ZHOU Bing-Jing; LI Yue.Electron Structure and Energy Transformation Mechanism of the Surface of Porous Nanocrystalline TiO2 Doped with La[J]. Acta Phys. -Chim. Sin., 2008,24(11): 2096-2101
45． LI Xiao-Hui, LIU Shou-Xin.Characterization of Visible Light Response N-F Codoped TiO2 Photocatalyst Prepared by Acid Catalyzed Hydrolysis[J]. Acta Phys. -Chim. Sin., 2008,24(11): 2019-2024
46． ZHANG Wei; CUI Xiao-Li; JIANG Zhi-Yu.Effect of Composite Modes on Photoelectrochemical Properties of MWCNTs/TiO2 Nanocomposite Films[J]. Acta Phys. -Chim. Sin., 2008,24(11): 1975-1980
47． ZHAO Feng-Ming; SHEN Hai-Ping; CHEN Zhao-Yang; MA Chun-An.Electrocatalytic Reduction of Maleic Acid at Bundles of TiO2 Anodization Film[J]. Acta Phys. -Chim. Sin., 2008,24(11): 2139-2142
48． YIN Yu-Xin; JIN Zheng-Guo; TAN Xin; HOU Feng; ZHAO Lin.Effect of Anions on the Electrochemical Formation of TiO2 Nanotube Arrays in a Glycerol Based Electrolyte[J]. Acta Phys. -Chim. Sin., 2008,24(11): 2133-2138
49． WANG Wei-Cheng, LI Shuo, WEN Yi-Yun, GONG Mao-Chu, ZHANG Lei, YAO Yan-Ling, CHEN Yao-Qiang.Synthesis and Characterization of TiO2/YFeO3 and Its Photocatalytic Oxidation of Gaseous Benzene[J]. Acta Phys. -Chim. Sin., 2008,24(10): 1761-1766
50． YU Jun, WU Gui-Sheng, MAO Dong-Sen, LU Guan-Zhong.Effect of La2O3 on Catalytic Performance of Au/TiO2 for CO Oxidation[J]. Acta Phys. -Chim. Sin., 2008,24(10): 1751-1755
51． CHEN Yu-Juan; HU Zhong-Hua; WANG Xiao-Jing; ZHAO Guo-Hua; LIU Ya-Fei; LIU Wei.Influence of Pore Size and Surface Area of Activated Carbon on the Performance of TiO2/AC Photocatalyst[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1589-1596
52． SUN Yi; XU Juan; CAI Wen-Bin; JIANG Zhi-Yu.Mechanism of Photokilling LoVo Cells by Nano TiO2 Photocatalytic Oxidation Combined with Immunity and Electroporation Method[J]. Acta Phys. -Chim. Sin., 2008,24(08): 1359-1365
53． LIN Tao; ZHANG Qiu-Lin; LI Wei; GONG Mao-Chu; XING Yi-Xun; CHEN Yao-Qiang.Monolith Manganese-Based Catalyst Supported on ZrO2-TiO2 for NH3-SCR Reaction at Low Temperature[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1127-1131
54． TANG Yu-Xin; TAO Jie; TAO Hai-Jun; WU Tao; WANG Ling; ZHANG Yan-Yan; LI Zhuan-Li; TIAN Xi-Lin.Fabrication and Characterization for Transparent Electrodes of TiO2 Nanotube Arrays on Fluorine-Doped Tin Oxide-Coated Glass[J]. Acta Phys. -Chim. Sin., 2008,24(06): 1120-1126
55． WANG Ting; JIANG Xin; WU Yan-Xiang.Crystallization of Nano TiO2 Prepared by Adsorption Phase Reaction Technique and Photo-degradation of Gaseous Toluene[J]. Acta Phys. -Chim. Sin., 2008,24(05): 817-822
56． LU Han-Feng; ZHOU Ying; XU Bo-Qing; CHEN Yin-Fei; LIU Hua-Zhang.Effect of Gold Doping on the Photocatalytic Activity of the Anatase TiO2[J]. Acta Phys. -Chim. Sin., 2008,24(03): 459-464
57． LIU Shou-Xin; CHEN Xiao-Yun.Effect of Pore Structure of Activated Carbon on the Photocatalytic Activity of TiO2/AC Composite Photocatalyst[J]. Acta Phys. -Chim. Sin., 2008,24(03): 533-538
58． LIN Tao; LI Wei; GONG Mao-Chu; YU Yao; DU Bo; CHEN Yao-Qiang.Prepareration of ZrO2-TiO2-CeO2 and Its Application in the Selective Catalytic Reduction of NO with NH3[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1851-1856
59． YIN Yu-Xin; JIN Zheng-Guo; HOU Feng.Fabrication and Properties of TiO2 Nanotube Arrays Using Glycerol-DMSO-H2O Electrolyte[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1797-1802
60． ZHANG Tian-Yong; FAN Qiao-Fang; ZENG Miao; WANG Zheng; XIA Wen-Juan; CHI Li-Feng.Photocatalytic Degradation of Light Fast Scarlet BBN and Surfactant Bicomponents[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1803-1807
61． ZHANG Wei; WANG Shu-Liang; MA Yun-Qing; WANG Cui-Ping; LIU Xing-Jun.Influence of Interface Diffusion between Al Substrate and TiO2 Filmon Photocatalytic Activity[J]. Acta Phys. -Chim. Sin., 2007,23(09): 1347-1352
62． WANG Ting; JIANG Xin; LI Xi.Preparation of TiO2 Nanoparticles on Surface of Different Supports by Adsorption Phase Reaction Technique[J]. Acta Phys. -Chim. Sin., 2007,23(09): 1375-1380
63． WU Liang-Zhuan; ZHI Jin-Fang.One-step Synthesis of Anatase-Crystalline Titania Hollow Spheres in Aqueous Solution[J]. Acta Phys. -Chim. Sin., 2007,23(08): 1173-1177
64． LI Jing-Yi; MA Jun-Hua; BAI Tu-Ya; SUYOU Le-Ma.Effect of Fluoride Ion on the Photocatalytic Degradation of Sulforhodamine B on TiO2/Bentonite[J]. Acta Phys. -Chim. Sin., 2007,23(08): 1213-1218
65． TIAN Bao-Zhu; TONG Tian-Zhong; CHEN Feng; ZHANG Jin-Long.Effect of Water Washing Treatment on the Photocatalytic Activity of Au/TiO2 Catalysts[J]. Acta Phys. -Chim. Sin., 2007,23(07): 978-982
66． ZHAO Meng; WANG Jin-Xing; FENG Cai-Hui; ZOU Bo; CHEN Cheng; WANG Zhu-Yi; WU Feng-Qing; ZOU Le-Hui.Preparation and Gas Sensing Properties to Formaldehyde of TiO2/Ag2O Nanocrystalline[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1003-1006
67． ZHANG Xia; ZHAO Yan; ZHANG Cai-Bei; MENG Hao.Synthesis and Characterization of TiO2 Nano-crystalline with Different Morphologies by Low-temperature Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2007,23(06): 856-860
68． TAI Hui-Ling; JIANG Ya-Dong; XIE Guang-Zhong; DU Xiao-Song; CHEN Xuan.Preparation and Gas Sensitive Properties of Polyaniline/Titanium Oxide Composite Thin Films[J]. Acta Phys. -Chim. Sin., 2007,23(06): 883-888
69． LI Wei; PAN Gang; CHEN Hao; ZHANG Mei-Yi; HE Guang-Zhi; LI Jin; YANG Yu-Huan.Temperature Effects on Adsorption-Desorption Irreversibility of Zn(II) onto Anatase[J]. Acta Phys. -Chim. Sin., 2007,23(06): 807-812
70． WU Lun-Peng; ZHAO Lian-Hua; ZHANG Hai-Ming; ZHAO Qing-Nan.Effects of the Adsorption of Oxygen on the Photocatalytic Activity of TiO2 Films Using PhotocurrentMethod[J]. Acta Phys. -Chim. Sin., 2007,23(05): 765-768
71． CHEN Xiao-Yun; LIU Shou-Xin.Preparation and Characterization of S-doped Ti1-xSyO2 Photocatalyst withWide Range Light Response[J]. Acta Phys. -Chim. Sin., 2007,23(05): 701-708
72． YAN Shan-Shan;WU Lian-Di;CHEN Feng;ZHANG Jin-Long.Low-temperature Preparation and Characterization of TiO2 Thin Films with a Bicrystalline Framework[J]. Acta Phys. -Chim. Sin., 2007,23(03): 414-418
73． LI Jing-Yi;SIQIN Gao-Wa;LIU Li-Na.Photocatalytic Degradation of Organic Pollutants on TiO2/Bentonite[J]. Acta Phys. -Chim. Sin., 2007,23(01): 16-20
74． SHI Qiu-Jie;LEI Jing-Xin;ZHANG Ning.Modification of Ni-B/TiO2-Al2O3(S) Amorphous Alloy Catalyst by Mo for Liquid-phase Furfural Hydrogenation[J]. Acta Phys. -Chim. Sin., 2007,23(01): 98-102
75． CHU Dao-Bao;YIN Xiao-Juan;FENG De-Xiang;LIN Hua-Shui;TIAN Zhao-Wu.Electrocatalytic Oxidation of Ethanol on Pt/nanoTiO2-CNT Complex Catalysts[J]. Acta Phys. -Chim. Sin., 2006,22(10): 1238-1242
76． HAN Cheng-Hui;LIU Bing-Hua;ZHANG Hui-Liang;SHEN Jian-Yi .Characterization of TiO2–ZrO2and Isopropanol Catalysis Conversion[J]. Acta Phys. -Chim. Sin., 2006,22(08): 993-998
77． FENG Chun-Bo;DU Zhi-Ping;Zhao Yong-Hong;TAI Xiu-Mei;LI Qiu-Xiao .Photocatalytic Activity of Au Modified Nano-TiO2 for NPE-10 Degradation[J]. Acta Phys. -Chim. Sin., 2006,22(08): 953-957
78． YANG Ying;GONG Chu-Qing;XIAO Si;GONG Hong-Mei;WANG Qu-Quan;ZHONG Jia-Cheng.Influences of Titania Concentration on the Structure and the Three-order Nonlinear Optical Properties of Core-shell Ag/TiO2 Nanocomposites[J]. Acta Phys. -Chim. Sin., 2006,22(07): 791-796
79． ZHOU Li-Jun;YAN Shan-Shan;TIAN Bao-Zhu;CHEN Feng;ZHANG Jin-Long;HUANG Jia-Zhen.Preparation and Characterization of Anatase-Brookite TiO2 Film on the PET Surface[J]. Acta Phys. -Chim. Sin., 2006,22(05): 569-573
80． CHEN Xiao-Yun;LIU Shou-Xin;CHEN Xi;SUN Cheng-Lin.Characterization and Activity of TiO2 /wAC Composite Photocatalyst Prepared by Acid Catalyzed Hydrolysis Method[J]. Acta Phys. -Chim. Sin., 2006,22(05): 517-522
81． LI Hui-Juan;JIANG Xiao-Yuan;ZHENG Xiao-Ming.Synthesis of TiO2/[[gamma]]r-Al2O3 and Effect of CuO Loading on NO Reduction[J]. Acta Phys. -Chim. Sin., 2006,22(05): 584-589
82． CHU Dao-Bao; ZHANG Li-Yan; ZHANG Jin-Hua; ZHANG Xiu-Mei; YIN Xiao-Juan.Heterogeneous Electrocatalytic Reduction of Furfural on Nanocrystalline TiO2-CNT Complex Film Electrode in DMF Solution[J]. Acta Phys. -Chim. Sin., 2006,22(03): 373-377
83． HAO Yan-Zhong;CAI Chun-Li.A Photoelectrochemical Study of the Nanostructured TiO2 /P3HT Film Electrode[J]. Acta Phys. -Chim. Sin., 2005,21(12): 1395-1398
84． PANG Ying-Cong;GAN Li-Hua;HAO Zhi-Xian;XU Zi-Jie;CHEN Long-Wu.Preparation and Characterization of TiO2/SiO2 Aerogel Microspheres[J]. Acta Phys. -Chim. Sin., 2005,21(12): 1363-1367
85． Chen Feng; Zhu Yi-Ping; Ma Hong-Liao; Bo Zi-Long; Zhang Jin-Long.Preparation and Characterization of TiO2--CdS-MCM-41 Nano-composite[J]. Acta Phys. -Chim. Sin., 2004,20(11): 1292-1296
86． Zhu Shi-Guo;Tang Ke;Xiang Juan-Juan;Lü Hong-Bin;Li Xiao-Ling;Nie Xin-Min;Zhou Hou-De;Shen Shou-Rong;Li Gui-Yuan.Synthesis and Applications of Florescence-Doped Silica Nanoparticles[J]. Acta Phys. -Chim. Sin., 2003,19(04): 311-314
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