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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2009,Vol.25>> Issue(10)>> 2167-2172     doi: 10.3866/PKU.WHXB20091014         中文摘要
Controlled Syntheses of FeNi3 Alloy Nanostructures via Reverse Microemulsion-Directed Hydrothermal Motheds
WANG Run-Han, JIANG Ji-Sen, HU Ming
Center of Functional Nanomaterials and Devices, Department of Physics, East China Normal University, Shanghai 200062, P. R. China
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FeNi3 alloy nanostructures were synthesized by hydrothermal methods in the surfactant/n-octane/n-hexanol/water quaternary reverse microemulsion systems. The size and shape of the products could be controlled by changing the type and dosage of the surfactant. Spherical particles with a diameter of ca 75 nmwere prepared when polyethylene glycol 4000 (PEG4000) was used as the surfactant. Sea-urchin-like particle was obtained when cetyltrimethylammonium bromide (CTAB) was used as the surfactant. The single sea-urchin-like particles were composed of many nanorods with diameters of ca 42 nm and lengths of 0.4-1.2 μm. The as-synthesized products were characterized by powder X-ray diffraction (XRD), Mossbauer spectroscopy, scanning electronic microscopy (SEM), transmission electron microscopy (TEM), selected area electron diffraction (SAED), and multi-purpose magnetic variable field translation balance (MM VFTB). Both the spherical and sea-urchin-like FeNi3 samples exhibited typical ferromagnetic behavior at roomtemperature. Their saturation magnetization values (Ms) were 114.4 and 97.4 emu·g-1, respectively, while their coercivity values (Hc) were 94.0 and 329.0 Oe, respectively.



Keywords: Nanoparticles   FeNi3 alloy   Reverse microemulsion   Hydrothermal method   Morphology control  
Received: 2009-05-12 Accepted: 2009-07-22 Publication Date (Web): 2009-08-26
Corresponding Authors: JIANG Ji-Sen Email: jsjiang@phy.ecnu.edu.cn


Cite this article: WANG Run-Han, JIANG Ji-Sen, HU Ming. Controlled Syntheses of FeNi3 Alloy Nanostructures via Reverse Microemulsion-Directed Hydrothermal Motheds[J]. Acta Phys. -Chim. Sin., 2009,25 (10): 2167-2172.    doi: 10.3866/PKU.WHXB20091014
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114. Zhang Qing-Min;Li Yan;Huang Fu-Zhi;Gu Zhen-Nan.Synthesis of Silver Nanoparticles in Nonionic Surfactant System[J]. Acta Phys. -Chim. Sin., 2001,17(06): 537-541
115. Gao En-Qin;Zhang Li;Yang Mai-Zhi;Cai Sheng-Min.Preparation of TiO2 Nanoparticles by Hydrothermal Method and its Application for Photoelectrochemical Cell[J]. Acta Phys. -Chim. Sin., 2001,17(02): 177-180
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117. Zeng Hong-Xia, Li Zhi-Ping, Wang Han-Qing.Physical Chemistry Property of Water/TX-100/Hexanol/Octane Reverse Microemulsion[J]. Acta Phys. -Chim. Sin., 1999,15(06): 522-527
118. ZHAI Wei, WANG Jian-yuan.【Retracted】Stability of Au Nanocrystals in 2D Superlattice[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
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