Acta Phys. -Chim. Sin. ›› 2009, Vol. 25 ›› Issue (11): 2275-2278.doi: 10.3866/PKU.WHXB20091109

• ARTICLE • Previous Articles     Next Articles

Effect of Silica Source on the Hydrothermal Synthesis of ITQ-13 Zeolite

XU Chen, GUAN Jing-Qi, WU Shu-Jie, KAN Qiu-Bin   

  1. College of Chemistry, Jilin University, Changchun 130023, P. R. China
  • Received:2009-06-01 Revised:2009-07-27 Published:2009-10-28
  • Contact: KAN Qiu-Bin E-mail:qkan@mail.jlu.edu.cn

Abstract:

ITQ-13 zeolite was successfully synthesized using three silica sources, i.e., tetraethylorthosilicate (TEOS), colloidal silica, and fumed silica, and was characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), BET surface area, and acidity by the adsorption of d3-acetonitrile. Characterization results showed that the ITQ-13 samples synthesized using colloidal silica and fumed silica possessed better crystallinity and larger crystals than those synthesized by the TEOS route.

Key words: Crystallinity, Silica sources, ITQ-13 zeolite

MSC2000: 

  • O643