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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2010,Vol.26>> Issue(03)>> 654-662     doi: 10.3866/PKU.WHXB20100318         中文摘要
CATALYSIS AND SURFACE STRUCTURE
Intercalated Structure and Photocatalytic Properties of TiO2-Graphite Oxide Composite
ZHANG Qiong, HE Yun-Qiu, CHEN Xiao-Gang, HU Dong-Hu, LI Lin-Jiang, YIN Ting, JI Ling-Li
School of Material Science and Engineering, Tongji University, Shanghai 200092, P. R. China
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TiO2-graphite oxide (TiO2-GO) composites were successfully prepared at low temperature (80 ℃) using graphite oxide (GO) and titanium sulfate (Ti(SO4)2) as initial reactants. The photocatalytic properties of TiO2-GO under UV light irradiation were also studied. Results show that the degradation rate of methyl orange is 1.17 mg·min-1·g-1 (referring to the efficiency of the initial 15 min). Compared with Degussa P25 powders, this intercalation composite is far more efficiently. In addition, the crystalline structure, interface status and microscopic structure of TiO2-GO were characterized by X-ray diffraction (XRD), Fourier-transform infrared (FT-IR) spectroscopy, X-ray photoelectron spectroscopy (XPS) and field emission scanning electron microscopy (FESEM). Result showed that the TiO2 crystallites in the intercalated structure were composed of anatase and rutile phase with the former phase being enriched. The functional groups present in GO such as carboxyl (C=O) were mostly reduced in the intercalation composite. On the other hand, the synthesis mechanism and the main reasons responsible for the superior photocatalytic properties of TiO2-GO are also discussed.



Keywords: Titania   Graphite oxide   Intercalated structure   Composite material   Photocatalytic property  
Received: 2009-09-14 Accepted: 2009-11-12 Publication Date (Web): 2010-01-26
Corresponding Authors: HE Yun-Qiu Email: heyunqiu@mail.tongji.edu.cn


Cite this article: ZHANG Qiong, HE Yun-Qiu, CHEN Xiao-Gang, HU Dong-Hu, LI Lin-Jiang, YIN Ting, JI Ling-Li. Intercalated Structure and Photocatalytic Properties of TiO2-Graphite Oxide Composite[J]. Acta Phys. -Chim. Sin., 2010,26 (03): 654-662.    doi: 10.3866/PKU.WHXB20100318
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92. QIAN Di-Feng, ZHANG Qing-Hong, WAN Jun, LI Yao-Gang, WANG Hong-Zhi.Enhancing the Photovoltaic Performance of Dye Sensitized Solar Cells with the TiO2 Sol Infiltrated Nanocrystalline Electrode[J]. Acta Phys. -Chim. Sin., 2010,26(10): 2745-2751
93. LIU Yu-Liang, YOU Cui-Rong, LI Yang, HE Tao, ZHANG Xiang-Qin, SUO Zhang-Huai.Preparation of Au@TiO2 Catalyst Using Escherichia Coil as the Template and Its Oxidation Reaction Activity toward CO[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2455-2460
94. SONG Hua,GUO Yun-Tao, LI Feng ,YU Hong-Kun.Preparation, Hydrodesulfurization and Hydrodenitrogenation Performance of a Ni2P/TiO2-Al2O3 Catalyst[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2461-2467
95. XU Ping-Chang, LIU Yang, WEI Jian-Hong, XIONG Rui, PAN Chun-Xu, SHI Jing.Solvothermal Preparation of Ag/TiO2 Nanoparticles and Their Photocatalytic Activity[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2261-2266
96. WANG Zheng-Ke, HU Qiao-Ling.Chitosan Rods Reinforced by N-Carboxyl Propionyl Chitosan Sodium[J]. Acta Phys. -Chim. Sin., 2010,26(07): 2053-2056
97. CAO Yin-Di, DANG Li-Qin, BAI Dan, LEI Zhi-Bin, LIU Mei-Ying.Adsorption of Lysozymes on Fe/CMK-5 Composites Synthesized by Chemical Vapor Deposition[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1593-1598
98. WU Li-Na, HUANG Yu-Dong, WANG Zhi-Jiang, LIU Li.Preparation and Characterization of Monolithic Silica Fiber/Al2O3 Aerogel Composites by Non-Supercritical Drying[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1717-1721
99. YAO Guo-Xin, SHI Bin-Bin, LI Guo-Hua, ZHENG Yi-Fan.Preparation and Electrocatalytic Activity of Tungsten Carbide and Zeolite Nanocomposite[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1317-1322
100. ZHANG Ai-Qin, YAN Wei, SHI Li-Qun, SHI Li-Yi, FANG Jian-Hui, JIN Lu-Jiang.Synthesis of Polypropylene/Silica Hybrid Materials by Supercritical CO2 Impregnation Using a Co-Solvent[J]. Acta Phys. -Chim. Sin., 2010,26(03): 643-648
101. SUN Jian-Ping, WENG Jia-Bao, LIN Ting, MA Lin-Pu.Synthesis and Optical Effects of Poly(2-methoxy-5-butoxy)-p-phenylene Vinylene/Eu2O3 Nanocomposites[J]. Acta Phys. -Chim. Sin., 2009,25(11): 2385-2390
102. WANG Tao, ZHOU Jian-Hua, WANG Dao-Jun, SUN Dun, DI Zhi-Yong, HE Jian-Ping.Syntheses and Infrared Emissivities of Ordered Mesoporous C-Al2O3 Nanocomposites[J]. Acta Phys. -Chim. Sin., 2009,25(10): 2155-2160
103. ZHANG Xiao-Yan, CUI Xiao-Li.Preparation and Photocatalytic Hydrogen Evolution Performance of C-N Co-doped Nano TiO2 Photocatalysts[J]. Acta Phys. -Chim. Sin., 2009,25(09): 1829-1834
104. DONG Xiang, TAO Jie, LI Ying-Ying, WANG Tao, ZHU Hong.Photoelectrochemical Properties of Three-Dimensional Network TiO2 Nanowire Film Prepared by Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2009,25(09): 1874-1882
105. LI Chang-Yu, LIU Shou-Xin, MA Yue.Preparation of Visible-Light Response Cu-Cu2+1O Composites by a One-Step Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2009,25(08): 1555-1560
106. DU Wei-Ping, LI Zhen, LENG Wen-Hua, XU Yi-Ming.Photocatalytic Reduction of Silver Ions on Ferric Oxides and Ferric Hydroxides[J]. Acta Phys. -Chim. Sin., 2009,25(08): 1530-1534
107. ZHOU Jing-Hong, HAN Wei-Wei, SUI Zhi-Jun, GUO Rong, FANG Xiang-Chen, ZHOU Xing-Gui.Preparation and Characterization of Tri-Lobular Alumina/Carbon Nanofiber Composites[J]. Acta Phys. -Chim. Sin., 2009,25(07): 1455-1460
108. FENG Li-Li, ZHAO Wei, LIU Yang, JIAO Liang, LI Xing-Guo.Photocatalytic Degradation of Rhodamine B by Nanocrystalline TiO2 Loaded into MCM-41 Molecular Sieves[J]. Acta Phys. -Chim. Sin., 2009,25(07): 1347-1351
109. HUANG Zhi-Hai, DONG Yin-Sheng, LIN Ping-Hua.Depositing an Apatite Coating in/on Massive Chitosan Porous Scaffolds by an Alternate Soaking Method[J]. Acta Phys. -Chim. Sin., 2009,25(07): 1285-1289
110. DUAN Jun-Yuan, ZHANG Qiao-Xin, WANG Yi-Long, GUAN Jian-Guo.Facile Synthesis and Formation Mechanism of Silver Nanoplates with Edge Lengths of Several Micrometers[J]. Acta Phys. -Chim. Sin., 2009,25(07): 1405-1408
111. LEI Jian-Fei, LI Wei-Shan.Photoelectrocatalytic Performance of Arrayed Porous TiO2/Ti[J]. Acta Phys. -Chim. Sin., 2009,25(06): 1173-1178
112. MA Ruo-Biao, FU Yan-Bao, MA Xiao-Hua.Preparation and Electrochemical Performance of Tin-Dioxide Filled Multi-Walled Carbon Nanotubes[J]. Acta Phys. -Chim. Sin., 2009,25(03): 441-445
113. DU Bing, JIANG Qi, ZHAO Xiao-Feng, LIN Sun-Zhong, MU Pei-Shan, ZHAO Yong.Preparation of PPy/CNTs Composite Based on the Electrostatic Absorption Effect[J]. Acta Phys. -Chim. Sin., 2009,25(03): 513-518
114. YU Zhi-Yong; ZHANG Wei; MA Ming; CUI Xiao-Li.Visible Light Photoelectrochemical Response of Nitrogen-Doped TiO2 Thin Films Prepared by Anodic Oxidation of Titanium Nitride Films[J]. Acta Phys. -Chim. Sin., 2009,25(01): 35-40
115. CHEN Xi-Liang; MA Ming-Wang; YANG Xiao-Min; YANG Kang; JI Te; WU Sheng-Wei; ZHU Zhi-Yong.Electrical and Optical Properties of MWNTs/HDPE Composites in THz Region[J]. Acta Phys. -Chim. Sin., 2008,24(11): 1969-1974
116. CHANG Guo-Qing, ZHENG Xi, CHEN Ri-Yao, CHEN Xiao, CHEN Li-Qin, CHEN Zhen.Silver Nanoparticles Filling in TiO2 Hollow Nanofibers by Coaxial Electrospinning[J]. Acta Phys. -Chim. Sin., 2008,24(10): 1790-1796
117. LI Hai-Long; LUO Wu-Lin; CHEN Tao; TIAN Wen-Yu; SUN Mao; LI Chun; ZHU Di; LIU Ran-Ran; ZHAO Yu-Liang; LIU Chun-Li.Preparation and Photocatalytic Performance of Titania Nanotubes Loaded with Ag Nanoparticles[J]. Acta Phys. -Chim. Sin., 2008,24(08): 1383-1386
118. SHI Jian; LI Jun; CAI Yun-Fa.Fabrication of C, N-Codoped TiO2 Nanotube Photocatalysts with Visible Light Response[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1283-1286
119. LUO Da-Chao; ZHANG Lan-Lan; LONG Hui-Jin; CHEN Yong-Mei; CAO Ya-An.Effect of Surface Modification by Ni2+ on Photocatalysis Activity of TiO2[J]. Acta Phys. -Chim. Sin., 2008,24(06): 1095-1099
120. FENG Cai-Xia; WANG Yan; JIN Zhen-Sheng; ZHANG Shun-Li.Kinetic Behavior of Visible Light Photocatalytic Oxidation of Propylene for N-Doped Nano-TiO2[J]. Acta Phys. -Chim. Sin., 2008,24(04): 633-638
121. WU Hua-Tao; ZHANG Ying; NING Xiang-Li; LIANG Hong-Lian; FANG Yu.Preparation of P(AM-co-MAA)-W-Ag Composite Microspheres with Core-Shell Structures[J]. Acta Phys. -Chim. Sin., 2008,24(04): 646-652
122. WU Yu-Cheng; LIU Xiao-Lu; YE Min; XIE Ting; HUANG Xin-Min.Preparation and Properties of Carbon Nanotube-TiO2 Nanocomposites[J]. Acta Phys. -Chim. Sin., 2008,24(01): 97-102
123. ZHANG Jun-Jie; WU Min; QIN Yan-Tao; CHEN Rui; JIANG Yin-Hua; SUN Yue-Ming; YANG Zhao-Hui.Study on Zn(II) Tetracarboxy Phthalocyanine Doped TiO2 Electrode Using Electrochemical Impedance Spectrum[J]. Acta Phys. -Chim. Sin., 2008,24(01): 79-84
124. CHEN Qi-Yuan; TONG Hai-Xia; YIN Zhou-Lan; HU Hui-Ping; LI Jie; LIU Liang-Liang.Preparation, Characterization and Photo-catalytic Behavior of TiO2 Catalysts with Oxygen Vacancies[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1917-1921
125. WANG Yi; JIANG Wei; CHENG Zhi-Peng; ZHANG Xian-Feng; AN Chong-Wei; SONG Xiao-Lan; LI Feng-Sheng.Thermal Performance Investigation of Core-Shell Cu/Al Micron-Nano Composites with WO3[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1753-1759
126. ZHU Lei; CUI Xiao-Li; SHEN Jie; YANG Xi-Liang; ZHANG Zhuang-Jian.Visible Light Photoelectrochemical Response of Carbon-doped TiO2 Thin Films Prepared by DC Reactive Magnetron Sputtering[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1662-1666
127. LI Guo-Hua; TIAN Wei; TANG Jun-Yan; MA Chun-An.Preparation and Electrocatalytic Property for Methanol Oxidation of WC/CNT Nanocomposite[J]. Acta Phys. -Chim. Sin., 2007,23(09): 1370-1374
128. YANG Hui; SHEN Qian-Hong; GAO Ji-Wei.Morphology Control of Anatase TiO2 Films Prepared at Low Temperature Using 4,4’-isopropylidenediphenol[J]. Acta Phys. -Chim. Sin., 2007,23(08): 1269-1274
129. HUANG Dong-Sheng; ZENG Ren-Jie; CHEN Chao-Feng; LI Yu-Hua.Hydrophilicity of TiO2 Thin Films Codoped with Iron and Nitrogen[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1037-1041
130. YAN Zhi-Ying; WU Li-Yan; SUN Gui-Xiang; ZHANG Ning; ZHENG Wen-Jun.Structural Characterization of Nanocrystalline TiO2 fromIonic Liquid-Water Solvent Mixture and Its Photocatalytic Activity[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1032-1036
131. DING Ying-Ying; LI Kui-Ying.Photoacoustic and Surface Photovoltaic Characters of Nanocrystalline TiO2[J]. Acta Phys. -Chim. Sin., 2007,23(04): 569-574
132. SONG Yu-Feng;ZHU Zhi-Yong;JI Te;GE Min;CHEN Xi-Liang;LIU Qi .THz time-domain spectroscopic study of polyethylene-carbon black composites[J]. Acta Phys. -Chim. Sin., 2007,23(02): 177-180
133. ZHOU Yu-Ming1;ZHONG Ai-Min;HE Man;CUI Yi-Ping;ZHANG Tong .Preparation and Characterization of Novel PUT/SiO2 Nanocomposite Material[J]. Acta Phys. -Chim. Sin., 2007,23(02): 223-227
134. ZHU Lu-Ping;HUANG Wen-Ya;MA Li-Li;FU Shao-Yun;YU Ying;JIA Zhi-Jie.Synthesis and Characteristics of ZnO-CNTs Nanocomposites[J]. Acta Phys. -Chim. Sin., 2006,22(10): 1175-1180
135. BIAN Cheng-Xiang;XU Xue-Cheng;YU Wei;CHEN Yi-Wei;CHENG Rong-Ming;SHI Yan;LI Xiang-Mei;JIN Sheng-Song.Study on Conductive Mechanism of Composites―Sulfonated Polyphenylacetylene / Multiwalled Carbon Nanotubes[J]. Acta Phys. -Chim. Sin., 2006,22(10): 1185-1190
136. LEI Zhong-Li;FAN You-Hua .Preparation and Characterization of Silver Nanocomposites Based on Copolymers[J]. Acta Phys. -Chim. Sin., 2006,22(08): 1021-1024
137. GU Hong;XU Bo-Lian;ZHOU Jing;LI Yuan-Zhi;FAN Yi-Ning.Catalytic Properties of Supported Pd/TiO2 and Pd-Ag/TiO2 Catalysts for Selective Hydrogenation of Acetylene[J]. Acta Phys. -Chim. Sin., 2006,22(06): 712-715
138. ZHANG Xue-Hong;TANG Xing-Hua;CHENG Xin-Sun.Synthesis and Application of Ce-doped Mesoporous TiO2[J]. Acta Phys. -Chim. Sin., 2006,22(05): 532-537
139. WANG Peng; CHEN Dong; LIU Jian-Shu; TANG Fang-Qiong.Synthesis and Characterization of Monodisperse TiO2 Colloid Particles[J]. Acta Phys. -Chim. Sin., 2006,22(03): 365-368
140. LI Zhi; GONG Qian-Ming; LIANG Ji; HUANG Qi-Zhong; HUANG Bai-Yun.Study on Oxidation Properties of New ACNT/C Nanocomposites[J]. Acta Phys. -Chim. Sin., 2006,22(03): 316-321
141. LI Zhi-Jie; HOU Bo; XU Yao; WU Dong; SUN Yu-Han.Preparation and Characterization of Silica-modified Titanium Dioxide Nanoparticles by Co-precipitation Method[J]. Acta Phys. -Chim. Sin., 2005,21(03): 229-233
142. YAN Qing-Zhi;SU Xin-Tai;ZHOU Yan-Ping;GE Chang-Chun.Controlled Synthesis of TiO2 Nanometer Powders by Sol-gel Auto-igniting Process and Their Structural Property[J]. Acta Phys. -Chim. Sin., 2005,21(01): 57-62
143. Li Yue-Xiang; Wang Tian-Hui; Peng Shao-Qin1 Lü Gong-Xuan; Li Shu-Ben.Synergistic Effect of Eu3+ and Si4+ Co-doping on Photocatalytic Activity of Titanium Dioxide[J]. Acta Phys. -Chim. Sin., 2004,20(12): 1434-1439
144. Lin Li;Lin Wei;Wang Pei;Zhu Yue-Xiang;Zhao Bi-Yin;Xie You-Chang.Uniform Carbon-covered Alumina Synthesized by Pyrolysis of Sucrose/γ-Al2O3[J]. Acta Phys. -Chim. Sin., 2004,20(10): 1179-1181
145. Shen Jie;Wo Song-Tao;Cui Xiao-Li;Cai Zhen-Wei;Yang Xi-Liang;Zhang Zhuang-Jian.Photoelectrochemical Characteristics of Nano-Titanium Dioxide Thin Films Prepared by RF Magnetron Sputtering[J]. Acta Phys. -Chim. Sin., 2004,20(10): 1191-1195
146. Zhang Ying;Fang Yu;Lin Shu-Yu;Liu Jing;Yang Juan-Ling.Preparation of Spherical Nano-structured PMAA/CdS Composites by a Microgel Template Method[J]. Acta Phys. -Chim. Sin., 2004,20(08S): 897-901
147. Chen Ming-An;Zhang Xin-Ming;Xie Xuan.Interphase Analysis of Adhesion Bonded Aluminum Sheet/polypropylene and Maleic Anhydride Grafted Polypropylene by XPS[J]. Acta Phys. -Chim. Sin., 2004,20(08): 882-886
148. Zhang Qi;Li Xin-Jun;Li Fang-Bai;Chang Jie.Investigation on Visible -light Activity of WOx/TiO2 Photocatalyst[J]. Acta Phys. -Chim. Sin., 2004,20(05): 507-511
149. Liu Shou-Xin;Sun Cheng-Lin.Mechanism of Silver Modification for the Enhanced Photocatalytic Activity of Cr(VI) Reduction on TiO2 Photocatalyst[J]. Acta Phys. -Chim. Sin., 2004,20(04): 355-359
150. Zhang Jin-Long;Zhao Wen-Juan;Chen Hai-Jun;Xu Hua-Sheng;Chen Ai-Ping;Anpo Masa-Kazu.Study of Loaded Photocatalysts by Precious Metals on the Photocatalytic Reactivity[J]. Acta Phys. -Chim. Sin., 2004,20(04): 424-427
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152. Ding Zheng-Xin;Hou Yi-Dong;Li Dan-Zhen;Wang Xu-Xu;Fu Xian-Zhi;Liu Ping.Effect of Morphological Structure and Photoelectric Properties on Photocatalytic Performance of TiO2[J]. Acta Phys. -Chim. Sin., 2003,19(10): 978-981
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154. Ren Da-Sen;Cui Xiao-Li;Zhang Qun;Wo Song-Tao;Yang Xi-Liang;Zhang Zhuang-Jian;Lu Ming.Characteristics of SiO2-TiO2 Complex Thin Films Prepared by Sol Method[J]. Acta Phys. -Chim. Sin., 2003,19(09): 829-833
155. Wang Shan;Fang Yu;Zhang Ying;Wang MingZhen;Hu DaoDao;Liao YiKun.Preparation of Chitosan/CdS Composite Films and Their Sensing Properties to Pyridine[J]. Acta Phys. -Chim. Sin., 2003,19(06): 514-518
156. Zhang Guo-Lin;Pan Xian-Hua;Kan Jin-Qing;Zhang Jing-Hui;Li Yong-Fang.Studies on Conducting Composite MaterialGlucose Oxidase Biosensor[J]. Acta Phys. -Chim. Sin., 2003,19(06): 533-537
157. Ruan Sheng-Ping;Wu Feng-Qing;Wang Yong-Wei;Zhang Li;Wu Ri-Na;Xuan Li.Synthesis and Microwave Absorbing Properties of Nanocrystalline Barium Ferrite Composite Material[J]. Acta Phys. -Chim. Sin., 2003,19(03): 275-277
158. Zhang Sheng-Mao;Zhang Zhi-Jun;Dang Hong-Xin;Liu Wei-Min;Xue Qun-Ji.Preparation and Characterization of TiO2/Poly(butyl acrylate) Nanocomposite Film[J]. Acta Phys. -Chim. Sin., 2003,19(02): 171-173
159. Song Hui-Hua;Fang Zhen;Guo Hai-Qing.Synthesis and Characterization of CdSe/Poly (4-vinylpyridine) Quaternary Ammonium Nanocomposite[J]. Acta Phys. -Chim. Sin., 2003,19(01): 9-12
160. Qin Cao;Wang Ting-Jie;Jin Yong.The Coating Process of Nano-scale Hydrous Silica Film on TiO2 Particles by Chemical Deposition in Aqueous Solution[J]. Acta Phys. -Chim. Sin., 2002,18(10): 884-889
161. Li Dan-Zhen;Zheng Yi;Fu Xian-Zhi.Study on the Effect and Mechanism of the Coupling between Microwave and Photocatalysis[J]. Acta Phys. -Chim. Sin., 2002,18(04): 332-335
162. Zhao Liang-Zhong;Liu Fen;Li Jian-Zhang;Xu Yong-Tong.XPS Study of Three Dimensional C/SiC Composites[J]. Acta Phys. -Chim. Sin., 2001,17(09): 802-805
163. Chen Hong-Ling;Wang Yan-Ru;Shi Jun.Preparation of Monodispersed Superfine Titanium Dioxide Particles and Size Control[J]. Acta Phys. -Chim. Sin., 2001,17(08): 713-717
164. Zou Ling;Wu Xue-Dong;Chen Hai-Gang;Wang Da-Pu.Structural Characterization and Formation Mechanism of SurfaceModified Titanium Dioxide Nanoparticles[J]. Acta Phys. -Chim. Sin., 2001,17(04): 305-309
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