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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2010,Vol.26>> Issue(12)>> 3187-3192     doi: 10.3866/PKU.WHXB20101212         中文摘要
ELECTROCHEMISTRY
Synthesis and Electrochemical Properties of High-Rate Spinel Li4Ti5Ol2/TiN Anode Material for Lithium-Ion Batteries
ZHOU Xiao-Ling, HUANG Rui-An, WU Zhao-Cong, YANG Bin, DAI Yong-Nian
National Engineering Laboratory for Vacuum Metallurgy, Faculty of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093, P. R. China
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Spinel Li4Ti5Ol2/TiN was successfully prepared by sol-gel processing using acetylacetone (ACAC) as a chelating ligand and polyethylene glycol (PEG) as a dispersant. The effect of the TiN film on the electrochemical properties of spinel Li4Ti5Ol2 for lithium-ion batteries was studied. The Li4Ti5Ol2/TiN was analyzed by X-ray photoelectron spectroscopy (XPS). X-ray diffraction (XRD) patterns and scanning electron microscope (SEM) images showed that this anode material with the TiN film was pure spinel Li4Ti5Ol2 and was of sub-micron size. The initial specific discharge capacity of the Li4Ti5Ol2/TiN is 173.0 mAh·g-1. When tested at a rate of 0.2C, 1C, 2C, and 5C, it still retained a discharge capacity of 170.6, 147.6, 135.6, and 111.0 mAh·g-1, respectively, after 10 cycles, indicating that Li4Ti5Ol2/TiN had better high-rate performance than that without the TiN film. The positive effect of the TiN film on lithium-ion batteries was also demonstrated by cyclic voltammetry (CV) and electrochemical impedance spectroscopy (EIS).



Keywords: Lithium-ion battery   Spinel Li4Ti5Ol2   TiN film   Anode material   Sol-gel processing   Polyethylene glycol  
Received: 2010-06-25 Accepted: 2010-09-02 Publication Date (Web): 2010-11-02
Corresponding Authors: HUANG Rui-An Email: rahuang2009@gmail.com

Fund: The project was supported by the Natural Science Foundation of Yunnan Province, China (2009CD024).

Cite this article: ZHOU Xiao-Ling, HUANG Rui-An, WU Zhao-Cong, YANG Bin, DAI Yong-Nian. Synthesis and Electrochemical Properties of High-Rate Spinel Li4Ti5Ol2/TiN Anode Material for Lithium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2010,26 (12): 3187-3192.    doi: 10.3866/PKU.WHXB20101212

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71. NIE Ping, SHEN Lai-Fa, CHEN Lin, SU Xiao-Fei, ZHANG Xiao-Gang, LI Hong-Sen.Sol-Gel Synthesis and Electrochemical Performance of Porous LiMnPO4/MWCNT Composites[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2123-2128
72. CHU Dao-Bao, LI Yan, SONG Qi, ZHOU Ying.Synthesis and Properties of LiFePO4/C Cathode Material with a New Carbon Source[J]. Acta Phys. -Chim. Sin., 2011,27(08): 1863-1867
73. MAI Li-Qiang, YANG Shuang, HAN Chun-Hua, XU Lin, XU Xu, PI Yu-Qiang.Chemical Lithiation and Electroactivity of Nanomaterials[J]. Acta Phys. -Chim. Sin., 2011,27(07): 1551-1559
74. CHEN Lang, RAO Mu-Min, LI Wei-Shan, XU Meng-Qing, LIAO You-Hao, TAN Chun-Lin, YI Jin.Performance Improvement of Polyethylene-Supported PAMS Electrolyte Using Urea as Foaming Agent[J]. Acta Phys. -Chim. Sin., 2011,27(07): 1689-1694
75. ZHAO Xing, ZHUANG Quan-Chao, QIU Xiang-Yun, XU Shou-Dong, SHI Yue-Li, CUI Yong-Li.Electrochemical Performance of Cr2O3/TiO2 Composite Material for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2011,27(07): 1666-1672
76. CHENG Feng, HUANG Ke-Long, LIU Su-Qin, FANG Xue-Song, ZHANG Xin.Surfactant Carbonization to Synthesize a Fe3O4/C Composite and Its Electrochemical Performance[J]. Acta Phys. -Chim. Sin., 2011,27(06): 1439-1445
77. ZHANG Hui-Min, HU Rui-Sheng, HU Jia-Nan, ZHANG Yu-Long.Preparation and Catalytic Activities of La2CoAlO6 for Methane Combustion[J]. Acta Phys. -Chim. Sin., 2011,27(05): 1169-1175
78. Lü Rong-Guan, YANG Jun, WANG Jiu-Lin, NULI Yan-Na.Electrodeposition and Electrochemical Property of Porous Li-Si Film Anodes for Lithium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2011,27(04): 759-763
79. TANG Yan, ZHONG Ben-He, GUO Xiao-Dong, LIU Heng, ZHONG Yan-Jun, NIE Xiang, TANG Hong.Effects of Mixed Solvents on the High-Rate Performance of Li3V2(PO4)3/C Prepared by Sol-Gel Method[J]. Acta Phys. -Chim. Sin., 2011,27(04): 869-874
80. SU Chang, LU Guo-Qiang, XU Li-Huan, ZHANG Cheng, MA Chun-An.Synthesis and Properties of Spindle-Shaped LiFePO4 for the Cathode Material of Lithium Ion Battery[J]. Acta Phys. -Chim. Sin., 2011,27(03): 609-614
81. AN Ting, ZHAO Feng-Qi, YI Jian-Hua, FAN Xue-Zhong, GAO Hong-Xu, HAO Hai-Xia, WANG Xiao-Hong, HU Rong-Zu, PEI Qing.Preparation, Characterization, Decomposition Mechanism and Non-Isothermal Decomposition Reaction Kinetics of the Super Thermite Al/CuO Precursor[J]. Acta Phys. -Chim. Sin., 2011,27(02): 281-288
82. ZHANG Qiu-Mei, SHI Zhi-Cong, LI Yi-Xiao, GAO Dan, CHEN Guo-Hua, YANG Yong.Recent Advances in Fluorophosphate and Orthosilicate Cathode Materials for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2011,27(02): 267-274
83. WANG Xiao-Ya, CHENG Qian, HUANG Tao, YU Ai-Shui.Effect of Calcination Atmosphere on Li/Ni Disorder and Electrochemical Performance of Layered LiNi0.5Mn0.5O2[J]. Acta Phys. -Chim. Sin., 2011,27(02): 437-442
84. CUI Wen-Yu, AN Mao-Zhong, YANG Pei-Xia, ZHANG Jin-Qiu.Cathodic and Thermal Stabilities of the P(VdF-HFP)-Based Ionic Liquid Composite Polymer Electrolyte[J]. Acta Phys. -Chim. Sin., 2011,27(01): 78-84
85. CHEN Shi-Yu, WANG Zhao-Xiang, FANG Xiang-Peng, ZHAO Hai-Lei, LIU Xiao-Jiang, CHEN Li-Quan.Characterization of TiS2 as an Anode Material for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2011,27(01): 97-102
86. CHANG Zhao-Rong, DAI Dong-Mei, LI Bao, TANG Hong-Wei.Effect of Hydrazine on the Performance of LiNi0.5Mn1.5O4Cathode Materials[J]. Acta Phys. -Chim. Sin., 2010,26(10): 2633-2637
87. LI Ya-Juan, ZHAN Hui, LIU Su-Qin, HUANG Ke-Long, ZHOU Yun-Hong.Nanosized Flame Retarded HydroxideMagnesium/Poly(ethylene-oxide) Composite Polymer Electrolyte[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2387-2391
88. HUANG Yan, ZHANG Xing-Wang, LEI Le-Cheng.Preparation, Characterization and Catalytic Activity for ortho- Dichlorobenzene Ozonation of Fe-, Mn-Doped Xerogels[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2443-2448
89. DAI Ke-Hua, MAO Jing, ZHAI Yu-Chun.High Rate Capability of 5 V LiNi0.5Mn1.5O4 Cathode Materials Synthesized via a Gel-Combustion Method[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2130-2134
90. SHEN Bin, WANG Yong-An, WANG Zhi-Fei, ZHANG Ling.Catalytic Activity of an Oxime Carbapalladacycle Complex Grafted onto Superparamagnetically Mesoporous Nanoparticles for the Heck Reaction[J]. Acta Phys. -Chim. Sin., 2010,26(07): 1860-1866
91. QIU Xiang-Yun, ZHUANG Quan-Chao, WANG Hong-Ming, CUI Yong-Li, FANG Liang, SUN Shi-Gang.Influence of Electrolyte Composition on the Intercalation-Deintercalation Process of Lithium Ion in Spinel LiMn2O4[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1499-1506
92. QU Xiao-Hua, LIU Jie, WANG Zhao-Xiang, CAO Dian-Liang, FANG Xiang-Peng, ZHANG Ling, DUAN Jing-Lai, YAO Hui-Jun, CHEN Yan-Feng, SUN You-Mei, HOU Ming-Dong.Preparation of Microporous Membranes by Swift Heavy Ion Irradiation and Impedance Characterization[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1722-1726
93. ZHANG Xiao-Yu, JIANG Wei-Jun, ZHU Xiao-Pei, QI Lu.Characterization of LiNi1/3Mn1/3Co1/3O2 Synthesized by Wet-Chemical Method[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1507-1514
94. CUI Wen-Yu, AN Mao-Zhong, YANG Pei-Xia.Preparation of an Ionic Liquid Gel Polymer Electrolyte and Its Compatibility with a LiFePO4 Cathode[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1233-1238
95. ZHANG Hui-Juan, SONG Huai-He, ZHOU Ji-Sheng, ZHANG Hong-Kun, CHEN Xiao-Hong.Preparation and Electrochemical Properties of SnO2/Onion-Like Hollow Carbon Nanoparticle Composites as Anode Materials for Lithium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1259-1263
96. GUO Xiang-Yun, JIN Guo-Qiang, WANG Ying-Yong.Preparations and Catalytic Applications of High Surface Area Silicon Carbide[J]. Acta Phys. -Chim. Sin., 2010,26(04): 1143-1150
97. CHANG Yu-Qing, HUANG Ling, SUN Shi-Gang.Electrodeposition and Electrochemical Properties of Ternary Sn-Co-Zn Alloy Electrodes as Anodes for Lithium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2010,26(03): 561-566
98. XIONG Li-Zhi, HE Ze-Qiang.A New Rheological Phase Route to Synthesize Nano-LiVOPO4 Cathode Material for LithiumIon Batteries[J]. Acta Phys. -Chim. Sin., 2010,26(03): 573-577
99. CHANG Zhao-Rong, YU Xu, TANG Hong-Wei, WEI Wen-Qiang, DAI Dong-Mei.Influence of Al Doping Content on the Structure and Electrochemical Properties of LiNi1/3Co2/3-xAlxO2[J]. Acta Phys. -Chim. Sin., 2010,26(03): 567-572
100. LU Hua-Quan, WU Feng, SU Yue-Feng, LI Ning, CHEN Shi, BAO Li-Ying.Electrochemical Performance of LiNi0.5Mn0.5O2 as Cathode Material for Lithium-Ion Batteries Prepared by Oxalate Co-Precipitation Method[J]. Acta Phys. -Chim. Sin., 2010,26(01): 51-56
101. ZHANG Ye, FAN Guang-Yin, WANG Lei, LI Rui-Xiang, CHEN Hua, LI Xian-Jun.Hydrogenation of Pyridine and Its Derivates Catalyzed by Poly(ethylene glycol)-Stabilized Amorphous RuB Nanoparticles[J]. Acta Phys. -Chim. Sin., 2009,25(11): 2270-2274
102. TAN Xiao-Lan, CHENG Xin-Qun, MA Yu-Lin, ZUO Peng-Jian, YIN Ge-Ping.Film Formation and Cycleability of LiBOB-Based Electrolyte[J]. Acta Phys. -Chim. Sin., 2009,25(10): 1967-1971
103. ZHENG Jun-Chao, LI Xin-Hai, WANG Zhi-Xing, LI Jin-Hui, WU Ling, LI Ling-Jun, GUO Hua-Jun.A Coalescence Mechanism for the Composite Cathode Material xLiFePO4·yLi3V2(PO4)3[J]. Acta Phys. -Chim. Sin., 2009,25(09): 1916-1920
104. ZHONG Mei-E, ZHOU Zhi-Hui, ZHOU Zhen-Tao.Electrochemical Performance of High-Density LiFePO4/C Composites Synthesized by Solid State-Carbothermal Reduction Method[J]. Acta Phys. -Chim. Sin., 2009,25(08): 1504-1510
105. JIANG Dong-Dong, FU Yan-Bao, MA Xiao-Hua.Fabrication and Characterization of Tin Nanorod Electrodes for Lithium Ion Rechargeable Batteries[J]. Acta Phys. -Chim. Sin., 2009,25(08): 1481-1484
106. FENG Ji-Jun, LIU Xiang-Zhe, LIU Xiao-Zhen, JIANG Jian-Zhuang, ZHAO Jing.Hydrothermal Syntheses and Properties of LiV3-xMnxO8 as Cathode Materials for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2009,25(08): 1490-1494
107. LI Li, MA Yu, CAO Yan-Zhen, JI Yuan, GUO Yi-Hang.Preparation of Periodic Mesoporous H6P2W18O62/TiO2(Brij-76) Composite and Microwave Enhanced Photocatalytic Degradation of Monochlorobenzene[J]. Acta Phys. -Chim. Sin., 2009,25(07): 1461-1466
108. HU Guo-Rong, CAO Yan-Bing, PENG Zhong-Dong, DU Ke, JIANG Qing-Lai.Preparation of Li2FeSiO4 Cathode Material for Lithium-Ion Batteries by Microwave Synthesis[J]. Acta Phys. -Chim. Sin., 2009,25(05): 1004-1008
109. GAO Hong-Quan, LAI Yan-Qing, ZHANG Zhi-An, LIU Ye-Xiang.Electrochemical Behaviors of New Lithium Salt LiBC2O4F2 in EC+DMC Solvents[J]. Acta Phys. -Chim. Sin., 2009,25(05): 905-910
110. FAN Xiao-Yong, ZHUANG Quan-Chao, WEI Guo-Zhen, KE Fu-Sheng, HUANG Ling, DONG Quan-Feng, SUN Shi-Gang.Fabrication and Performance of Cu6Sn5 Alloy Anode Using Porous Cu as Current Collector[J]. Acta Phys. -Chim. Sin., 2009,25(04): 611-616
111. WU Feng, WANG Meng, SU Yue-Feng, CHEN Shi.Surface Modification of LiCo1/3Ni1/3Mn1/3O2 by TiO2-Coating[J]. Acta Phys. -Chim. Sin., 2009,25(04): 629-634
112. ZHANG Guo-Qiang, MA Li, WU Zhong-Jie, ZHANG Hai-Yan, NI Pei.Electrochemical Behaviour of the Composite Polymer Electrolyte P(VDF-HFP)-PMMA/CaCO3(SiO2)[J]. Acta Phys. -Chim. Sin., 2009,25(03): 555-560
113. MA Ruo-Biao, FU Yan-Bao, MA Xiao-Hua.Preparation and Electrochemical Performance of Tin-Dioxide Filled Multi-Walled Carbon Nanotubes[J]. Acta Phys. -Chim. Sin., 2009,25(03): 441-445
114. ZHUANG Quan-Tiao, WEI Guo-Zhen, DONG Quan-Feng, SUN Shi-Gang.Influence of Temperature on the Performance of a Graphite Electrode[J]. Acta Phys. -Chim. Sin., 2009,25(03): 406-410
115. XU Jie; YAO Wan-Hao; YAO Yi-Wen; WANG Zhou-Cheng; YANG Yong.Effect of Fluoroethylene Carbonate Additive on the Performance of Lithium Ion Battery[J]. Acta Phys. -Chim. Sin., 2009,25(02): 201-206
116. LI Yang; XIE Hua-Qing; TU Jiang-Ping.SnS with Various Morphologies and Sizes as Anode Material for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2009,25(02): 365-370
117. WANG Tao, HE Jian-Ping, ZHANG Chuan-Xiang, ZHOU Jian-Hua, GUO Yun-Xia, CHEN Xiu, DI Zhi-Yong, SUN Dun, WANG Dao-Jun.Preparation and Electrochemical Properties of Ordered Mesoporous C/NiO Composites[J]. Acta Phys. -Chim. Sin., 2008,24(12): 2314-2320
118. WU Zhuang-Zhi; WANG De-Zhi; XU Bing.Preparation of Hollow MoS2 Microspheres by Addition of PEG as Template[J]. Acta Phys. -Chim. Sin., 2008,24(10): 1927-1931
119. YANG Shun-Yi; WANG Xian-You; WEI Jian-Liang; LI Xiu-Qin; TANG An-Ping.Preparation and Electrochemical Performance of Na-Mn-O Cathode Materials[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1669-1674
120. HUANG Jun-Jie; JIANG Zhi-Yu.Electrochemical Performance of LiMn2O4 Thin Film Electrode Fabricated by Ink-Jet Printing Technique[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1563-1567
121. ZHANG Hua; ZHOU Yong-Ning; WU Xiao-Jing; FU Zheng-Wen.Electrochemical Properties of CuF2 Films Fabricated by Pulsed Laser Deposition[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1287-1291
122. LI Fan-Qun; LAI Yan-Qing; ZHANG Zhi-An; GAO Hong-Quan; YANG Juan.Electrochemical Behaviors of Et4NBF4+LiPF6/EC+PC+DMC Electrolyte on Graphite Electrode[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1302-1306
123. WANG Meng; WU Feng; SU Yue-Feng; CHEN Shi.Electrochemical Characteristics of Y2O3-Coated LiCo1/3Ni1/3Mn1/3O2[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1175-1179
124. WANG Jian-Hua; LI Bin; WU Hai-Yan; GUO Yu-Zhong.Synthesis of Mesoporous SnO2 and Its Application in Lithium-Ion Battery[J]. Acta Phys. -Chim. Sin., 2008,24(04): 681-685
125. WU Yu-Cheng; LIU Xiao-Lu; YE Min; XIE Ting; HUANG Xin-Min.Preparation and Properties of Carbon Nanotube-TiO2 Nanocomposites[J]. Acta Phys. -Chim. Sin., 2008,24(01): 97-102
126. GUO Ying-Jun; LI Qi-Qi-Ge; NING Ying-Kun; QI Lu; TANG Hong-Wu.Performance of Liquid Electrolyte for Lithium-ion Battery at Elevated-temperature[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 1-4
127. WANG Ya-Dan; WANG Jian; MU Qi-Yong; LI Yong-Wei; QI Lu.Electrochemical Performances of LiMn2O4-based Electrode with Water-soluble Binder[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 14-17
128. QI Lu; SONG Zhao-Shuang; XU Hua; MAO Yong-Zhi; WU Ning-Ning; LIU Zheng-Yao.Electrochemical Performance of LithiumIon Battery Power Syetemfor Electric Vehicles[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 21-25
129. ZHANG Chun-Ling; JIANG Wei-Jun; ZHANG Jing; QI Lu.Performance of LiMn1.5Ni0.5-xCuxO4 as 5V Cathode Material for Lithium-ion Battery[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 31-35
130. TANG Ding-Guo.Application of Polymer LithiumIon Batteries Based on IPN[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 18-20
131. HOU Xian-Quan; JIANG Wei-Jun; QI Lu; HAN Li-Juan.Synthesis and Properties of Layered LiNi0.8Co0.2-xMgxO2 Cathode Material[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 40-45
132. FAN Mao-Song; LEI Xiang-Li; WU Ning-Ning; QI Lu.Electrochemical Performance of LiMn2O4 Power Battery[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 36-39
133. WANG Hai-Yan; LIU Xin-Hou; WU Da-Yong.Electrospinning and Electrospun Membranes[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 67-74
134. AN Hong-Li; WU Ning-Ning; LEI Xiang-Li; XU Jin-Long; QI Lu.Electrochemical Performance of LithiumIon Battery for Plug-in Hybrid Electric Vehicle Applications[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 60-66
135. GUO Ying-Jun; CHEN Hui; QI Lu.Progress in Electrolyte Solutions for Lithium-ion Battery[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 80-89
136. LEE Meng-Lung; LEE Yi-Da; CHANG Chie-Tai; GAO Tong-Han; LEE Torng-Jinn.Application and Technology of Aluminum Bag Lithium-Ion Polymer Battery[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 100-106
137. FENG Hua-Jun; CHEN Yuan;DAI Ke-Hua; SONG Zhao-Shuang; MA Jian-Wei; QI Lu.Preparation and Characterization of a Novel Kind of Polymer Electrolyte Composite Membrane for Lithium-Ion Battery[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1922-1926
138. ZHANG Lan; ZHANG Shi-Chao.Preparation and Characterization of Poly(acrylonitrile-methoxy polyethylene glycol (350) monoacrylate-lithium acrylate)[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1943-1947
139. CHEN Yong-Chong; XU Xing-Jun; CUI Hong-Zhi; DAI Ke-Hua; SONG Zhao-Shuang; JIANG Wei-Jun; QI Lu.Preferred Orientation of Crystals and the Intensity Ratios of XRD Peaks of Cathode Material LiCoO2[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1948-1953
140. HOU Chun-Ping; YUE Min.A Novel Cathode Material Lithium Vanadium Phosphate Synthesized by Liquid-phase Sphericizing Granulation[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1954-1957
141. WANG Feng; HAO Ya-Juan; JIN Guo-Qiang; GUO Xiang-Yun.Effects of the Reaction Conditions in Preparation of Si3N4 Nanowires[J]. Acta Phys. -Chim. Sin., 2007,23(10): 1503-1507
142. ZHANG Wei; WANG Shu-Liang; MA Yun-Qing; WANG Cui-Ping; LIU Xing-Jun.Influence of Interface Diffusion between Al Substrate and TiO2 Filmon Photocatalytic Activity[J]. Acta Phys. -Chim. Sin., 2007,23(09): 1347-1352
143. TANG Hong-Wei; ZHU Zhi-Hong; CHANG Zhao-Rong; CHEN Zhong-Jun.Drawing and Application of Phase Diagram Related to Eutectic Mixed Lithium Salts[J]. Acta Phys. -Chim. Sin., 2007,23(08): 1265-1268
144. WEI Ying-Jin; LI Xu; WANG Chun-Zhong; ZHAN Shi-Ying; CHEN Gang.Preparation and Electrochemical Properties of Cu Doped V2O5[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1090-1094
145. ZHANG Hong-Fang; FU Ping-Ping; SONG Ying-Jie; DU Chen-Shu; YANG Hua-Bin; ZHOU Zuo-Xiang; WU Meng-Tao; HUANG Lai-He.Preparation and Properties of Sandwich-type Si/Fe/Si Film Anode for Lithium-ion Battery[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1065-1070
146. HUANG Dong-Sheng; ZENG Ren-Jie; CHEN Chao-Feng; LI Yu-Hua.Hydrophilicity of TiO2 Thin Films Codoped with Iron and Nitrogen[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1037-1041
147. ZHAO Meng; WANG Jin-Xing; FENG Cai-Hui; ZOU Bo; CHEN Cheng; WANG Zhu-Yi; WU Feng-Qing; ZOU Le-Hui.Preparation and Gas Sensing Properties to Formaldehyde of TiO2/Ag2O Nanocrystalline[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1003-1006
148. CHEN Jian; HUANG Zheng-Ren; DONG Shao-Ming; JIANG Dong-Liang.Adsorption of Polyethylene Glycol on Silicon Carbide Measured by Thermal Gravimetric and Differential Thermal Analysis[J]. Acta Phys. -Chim. Sin., 2007,23(06): 926-928
149. LI Hong-Jian; CHEN Gang; LI Zhong-Hua; ZHOU Chao.Synthesis and Photocatalytic Decomposition of Water under Visible Light Irradiation of La2Ti2-xCoxO7 with Pyrochlore Structure[J]. Acta Phys. -Chim. Sin., 2007,23(05): 761-764
150. WU Lun-Peng; ZHAO Lian-Hua; ZHANG Hai-Ming; ZHAO Qing-Nan.Effects of the Adsorption of Oxygen on the Photocatalytic Activity of TiO2 Films Using PhotocurrentMethod[J]. Acta Phys. -Chim. Sin., 2007,23(05): 765-768
151. ZHANG Xiao-Fei; HU Rui-Sheng; GAO Guan-Jun; MENG He; SU Hai-Quan.Influence of Two Complexants on Structure and Performance of Ce-Sn-O Complex Oxides[J]. Acta Phys. -Chim. Sin., 2007,23(05): 659-663
152. LIU Su-Qin; LI Shi-Cai; HUANG Ke-Long; CHEN Zhao-Hui.Effect of Doping Ti4+ on the Structure and Performances of Li3V2(PO4)3[J]. Acta Phys. -Chim. Sin., 2007,23(04): 537-542
153. HUANG Ke-Long;YANG Sai;LIU Su-Qin;WANG Hai-Bo.Kinetics of Electrode Processes of LiFePO4 in Saturated Lithium Nitrate Solution[J]. Acta Phys. -Chim. Sin., 2007,23(01): 129-133
154. QIN Hai-Ying;XIE Jian;MI Jian-Li;TU Jian;ZHAO Xin-Bing.Solvothermal Synthesis and Electrochemical Lithiation/Delithiation Performance of FeSb2 Nanorods[J]. Acta Phys. -Chim. Sin., 2006,22(12): 1555-1559
155. HUANG Ling;JIANG Hong-Hong;KE Fu-Sheng;FAN Xiao-Yong;ZHUANG Quan-Chao;YANG Fang-Zu;SUN Shi-Gang.Structure and Properties of Three-dimensional Reticular Sn-Co Alloy Electrodes as Anode Material for Lithium Batteries[J]. Acta Phys. -Chim. Sin., 2006,22(12): 1537-1541
156. XU Yu-Hong;ZHANG Bao-Hong;GONG GUI-Ying;MA Ping .Electrochemical Properties Study of Sb2O3 doped Li4Ti5O12[J]. Acta Phys. -Chim. Sin., 2006,22(11): 1336-1341
157. XIE Jian;ZHAO Xin-Bing;YU Hong-Ming;QI Hao;CAO Gao-Shao;TU Jiang-Ping .Preparation, Characterization and Electrochemical Li-absorption/extraction Behaviors of Nanosized Co-Sn Intermetallic Compounds[J]. Acta Phys. -Chim. Sin., 2006,22(11): 1409-1412
158. QIAO Bin;TANG Zi-Long;ZHANG Zhong-Tai;CHEN Lei.Photoluminescent and Electroluminescent Characteristics of ZnGa2O4:Cr3+ Red Phosphor[J]. Acta Phys. -Chim. Sin., 2006,22(10): 1291-1295
159. FENG Chun-Bo;DU Zhi-Ping;Zhao Yong-Hong;TAI Xiu-Mei;LI Qiu-Xiao .Photocatalytic Activity of Au Modified Nano-TiO2 for NPE-10 Degradation[J]. Acta Phys. -Chim. Sin., 2006,22(08): 953-957
160. ZHUANG Da-Gao;ZHAO Xin-Bing;XIE Jian;TU Jian;ZHU Tie-Jun;CAO Gao-Shao.One-step Solid-state Synthesis and Electrochemical Performance of Nb-doped LiFePO4/C[J]. Acta Phys. -Chim. Sin., 2006,22(07): 840-844
161. LIU Yi-An;XUE Cheng-Shan;ZHUANG Hui-Zhao;ZHANG Xiao-Kai;TIAN De-Heng;WU Yu-Xin;SUN Li-Li;AI Yu-Jie;WANG Fu-Xue.Structure and Synthesis of GaN Powder by Sol-Gel Method[J]. Acta Phys. -Chim. Sin., 2006,22(06): 657-660
162. WANG Zhong;TIAN Wen-Huai;LI Xing-Guo.Synthesis and Electrochemical Properties of Sn-Sb Alloy Prepared by Hydrogen Plasma-metal Reaction[J]. Acta Phys. -Chim. Sin., 2006,22(06): 752-755
163. XUE Ming-Zhe; CHENG Sun-Chao; YAO Jia; FU Zheng-Wen.Electrochemical Properties of SnSe Thin Film Electrode Fabricated by Pulsed Laser Deposition[J]. Acta Phys. -Chim. Sin., 2006,22(03): 383-387
164. XU Meng-Qing; ZUO Xiao-Xi; LI Wei-Shan; ZHOU Hao-Jie; LIU Jian-Sheng; YUAN Zhong-Zhi.Effect of Butyl Sultone on the Li-ion Battery Performance and Interface of Graphite Electrode[J]. Acta Phys. -Chim. Sin., 2006,22(03): 335-340
165. YE Qing; XU Bo-Qing.Textural and Structure Characterizations of Ce1-xMnxO2Prepared by Citric Acid Sol-Gel Method[J]. Acta Phys. -Chim. Sin., 2006,22(03): 345-349
166. YANG Xiao; NI Jiang-feng; HUANG You-yuan; CHEN Ji-tao; ZHOU Heng-hui; ZHANG Xinxiang.Effect of Ti-Doping on Different Morphologic LiCoO2[J]. Acta Phys. -Chim. Sin., 2006,22(02): 183-188
167. ZHUANG Quan-chao; FAN Xiao-yong; XU Jin-mei; CHEN Zuo-feng; DONG Quan-feng; JIANG Yan-xia; HUANG Ling; SUN Shi-gang.Electrochemical Impedance Spectroscopic Study of the First Delithiation of Spinel Lithium Manganese Oxide[J]. Acta Phys. -Chim. Sin., 2006,22(02): 234-238
168. WANG Ying; LIU Wen-yuan; FU Zheng-wen.Electrochemistry of Mn4N with Lithium[J]. Acta Phys. -Chim. Sin., 2006,22(01): 65-70
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175. HUANG You-yuan; ZHOU Heng-hui; CHEN Ji-tao; GAO De-shu; SU Guang-yao.The Effect of Ti4+, Mg2+ Co-doping on Performance of LiNi0.4Co0.2Mn0.4O2[J]. Acta Phys. -Chim. Sin., 2005,21(07): 725-729
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180. Chang Xiao-Yan;Wang Zhi-Xing;Li Xin-Hai;Kuang Qiong;Peng Wen-Jie;Guo Hua-Jun;Zhang Yun-He.Synthesis and Performance of LiMnPO4 Used as Cathode Material for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2004,20(10): 1249-1252
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183. Liu Ying-Xin;Wei Zuo-Jun;Chen Ji-Xiang;Zhang Ji-Yan;Li Xin-Xue;Wei Xiong-Hui.Sol-gel Preparation,Characterization and Hydrogenation Property of Silica Supported Ni Catalyst[J]. Acta Phys. -Chim. Sin., 2004,20(07): 780-784
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186. Wang Zhan-Liang;Tang Zhi-Yuan.Research on the Interfacial Properties of Polymer Electrolyte by A.C.Impedance[J]. Acta Phys. -Chim. Sin., 2003,19(12): 1097-1101
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