ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2011,Vol.27>> Issue(03)>> 743-748     doi: 10.3866/PKU.WHXB20110318         中文摘要
Controlled Synthesis of Mesoporous MnO2 Nanospindles
HAN Ling, NI Ji-Peng, ZHANG Liang-Miao, YUE Bao-Hua, SHEN Shan-Shan, ZHANG Hao, LU Wen-Cong
Department of Chemistry, Shanghai University, Shanghai 200444, P. R. China
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We synthesized mesoporous MnO2 nanospindles by a one-step hydrothermal process in an aqueous solution of KMnO4 and glucose. The structure, morphology, purity, and size of the products were characterized by X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, transmission electron microscopy (TEM), high resolution transmission electron microscopy (HRTEM), scanning electron microscopy (SEM), and nitrogen adsorption/desorption (BET) measurements. The reaction time and concentrations of glucose influenced the final structures and shapes of the MnO2 nanospindles. The length to diameter ratio of the MnCO3 precursor nanospindles can be easily tuned from 1.35:1 to 2.89:1. A possible formation mechanism for the mesoporous MnO2 nanospindles is proposed and discussed.

Keywords: Hydrothermal method   Spindle   MnO2   Mesoporous  
Received: 2010-09-27 Accepted: 2010-11-15 Publication Date (Web): 2011-01-28
Corresponding Authors: LU Wen-Cong Email:

Fund: The project was supported by the Shanghai Special Nanotechnology Project, China (0852nm00700) and Innovation Fund of Shanghai University, China (A.10-0101-09-023).

Cite this article: HAN Ling, NI Ji-Peng, ZHANG Liang-Miao, YUE Bao-Hua, SHEN Shan-Shan, ZHANG Hao, LU Wen-Cong. Controlled Synthesis of Mesoporous MnO2 Nanospindles[J]. Acta Phys. -Chim. Sin., 2011,27 (03): 743-748.    doi: 10.3866/PKU.WHXB20110318

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71. WANG Cai-Cai, LI Jian-Hui, SUN Yi-Fei, ZHU Xiao-Quan, HUANG Chuan-Jing, WENG Wei-Zheng, WAN Hui-Lin.Synthesis and Catalytic Performances of Mesoporous CeNiO Catalysts for the Oxidative Dehydrogenation of Propane to Propene[J]. Acta Phys. -Chim. Sin., 2011,27(10): 2421-2426
72. WANG Xiao-Rong, HAO Guang-Ping, LU An-Hui, LI Wen-Cui.Adsorption and Release Behavior of Vitamin B12 in Tubular Structured Ordered Mesoporous Carbon[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2239-2243
73. YAN Hui, ZHANG Huan, ZHANG Ding, ZHU Zhi, QI Lu.Hydrothermal Synthesis of Spherical Li4Ti5O12 as Anode Material for High Power Lithium-Ion Secondary Battery[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2118-2122
74. LI Xue-Fei, ZHAO Yun, JIAO Qing-Ze, LI Han-Sheng, WU Hong-Yu, LIU Hong-Bo, CUI Wen-Jia.Preparation of One-Dimensional Titanate Nanomaterials Using Different Titania Sources[J]. Acta Phys. -Chim. Sin., 2011,27(08): 1996-2000
75. XU Qun-Jie, LI Jin-Guang, LI Qiao-Xia.Preparation of Mesoporous Carbon at Different Temperatures as a Catalyst Support for Direct Methanol Fuel Cells[J]. Acta Phys. -Chim. Sin., 2011,27(08): 1881-1885
76. LI Jian-Sheng, GU Juan, LING Xiao-Feng, SUN Xiu-Yun, SHEN Jin-You, HAN Wei-Qing, WANG Lian-Jun.Synthesis of Ordered Mesoporous Carbon Loaded Fe, Co, Ni Nanocrystals by the Soft Templating Route and Their Characterization[J]. Acta Phys. -Chim. Sin., 2011,27(07): 1772-1776
77. SHEN Shan-Shan, LU Wen-Cong, ZHANG Liang-Miao, YUE Bao-Hua, HAN Ling, ZHANG Hao.Fabrication of Mesoporous NiAl2O4 Nanorods and Their Catalytic Properties for Toluene Hydrocracking[J]. Acta Phys. -Chim. Sin., 2011,27(07): 1743-1750
78. YING Hong, WANG Zhi-Yong, GUO Zheng-Duo, SHI Zu-Jin, YANG Shang-Feng.Reduced Graphene Oxide-Modified Bi2WO6 as an Improved Photocatalyst under Visible Light[J]. Acta Phys. -Chim. Sin., 2011,27(06): 1482-1486
79. ZHOU Jin, LI Wen, XING Wei, ZHUO Shu-Ping.Capacitive Performance of Tunable Ordered Mesoporous Carbons in Organic and H2SO4 Electrolytes[J]. Acta Phys. -Chim. Sin., 2011,27(06): 1431-1438
80. LI Zhao, XU Ju-Liang, LI Xu-Yan, GUO Li-Fang, LI Jin, JIANG Yi-Ming.Preparation of Manganese Dioxide for Electrodes of Supercapacitors Based on Duplex Stainless Steel[J]. Acta Phys. -Chim. Sin., 2011,27(06): 1424-1430
81. MA Yan-Hui, ZHAO Hui-Ling, TANG Sheng-Jie, HU Jun, LIU Hong-Lai.Synthesis of Micro/Mesoporous Composites and Their Application as CO2 Adsorbents[J]. Acta Phys. -Chim. Sin., 2011,27(03): 689-696
82. LI Guo-Xian, WANG Tao, HE Jian-Ping, ZHOU Jian-Hua, XUE Hai-Rong, MAYi-Ou, HU Yuan-Yuan.Synthesis and Infrared Emissivity of Ordered Mesoporous C-Al2O3-TiO2 Nanocomposites with a Dual Pore System[J]. Acta Phys. -Chim. Sin., 2011,27(01): 248-254
83. CHEN Tian, WANG Tao, WANG Dao-Jun, ZHAO Jian-Qing, DING Xiao-Chun, WU Shi-Chao, XUE Hai-Rong, HE Jian-Ping.Selective Adsorption Behavior of Cu(II) and Cr(VI) Heavy Metal Ions by Functionalized Ordered Mesoporous Carbon[J]. Acta Phys. -Chim. Sin., 2010,26(12): 3249-3256
84. LIU Bai-Jun, MENG Qing-Lei, WANG Hui, MENG Qing-Min.Synthesis and Characterization of Al MCM-41 Mesoporous Molecular Sieves[J]. Acta Phys. -Chim. Sin., 2010,26(12): 3257-3262
85. ZHANG Fang, YUAN Chang-Zhou, ZHANG Xiao-Gang, ZHANG Luo-Jiang, XU Ke.5-Sulfosalicylic Acid-Assisted Hydrothermal Synthesis and Supercapacitive Properties of Co-Ni Layered Double Hydroxides[J]. Acta Phys. -Chim. Sin., 2010,26(12): 3175-3180
86. WU Tao, TAO Jie, DENG Jie, TANG Yu-Xin, ZHU Hong, GAO Peng.Preparation and Characterization of One-Dimensional TiO2 Nanowire Films on a Flexible Stainless Steel Substrate[J]. Acta Phys. -Chim. Sin., 2010,26(11): 3087-3094
87. CHEN Zhao-Yang, ZHAO Feng-Ming, MA Chun-An, QIAO Yun.Ultrasonic-Assisted Preparation of Bimodal Mesoporous HollowGlobal Tungsten Carbide and Its Electrocatalytic Performance[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2569-2574
88. ZHU Yan-Feng, DU Rong-Gui, LI Jing, QI Hai-Qing, LIN Chang-Jian.Photogenerated Cathodic Protection Properties of a TiO2 Nanowire FilmPrepared by a Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2349-2353
89. ZHANG Wei-Min, YANG Zhen-Dong, LIU Jia, SUN Zhong-Xi.Determination of Acid-Base Equilibrium Constants on Aqueous Mesoporous Silica Surfaces[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2109-2114
90. CHE Hong-Wei, HAN Shu-Hua, HOU Wan-Guo, LIU Ai-Feng.Novel Synthesis of Mesoporous Nanocrystalline Zirconia[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2177-2181
91. LIU Shu-Ping, YUE Ming-Bo, WANG Yi-Meng.One-Step Synthesis of Mesoporous Beta Zeolite Using Phosphate[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2224-2228
92. WU Bao-Hu, ZHANG Shu-Cui, TANG Tao, XU Yao, LIU Yi, WU Zhong-Hua.Small-Angle X-Ray Scattering Studies of Carboxyl Functionalized[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2217-2223
93. LIU Si-Yu, MENG Xiang-Ju, XIAO Feng-Shou.Hydrothermal Synthesis of Ordered Mesoporous Materials with High Stability at High Temperatures[J]. Acta Phys. -Chim. Sin., 2010,26(07): 1852-1859
94. SHEN Bin, WANG Yong-An, WANG Zhi-Fei, ZHANG Ling.Catalytic Activity of an Oxime Carbapalladacycle Complex Grafted onto Superparamagnetically Mesoporous Nanoparticles for the Heck Reaction[J]. Acta Phys. -Chim. Sin., 2010,26(07): 1860-1866
95. ZHANG Jing, KONG Ling-Bin, CAI Jian-Jun, YANG Zhen-Sheng, LUO Yong-Chun, KANG Long.Novel Polypyrrole/Mesoporous Carbon Nanocomposite Electrode for an Electrochemical Hybrid Capacitor[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1515-1520
96. LIU Yi-Wu, YU Huan, ZHANG Xiao-Ming, SUO Ji-Shuan.Direct Gas-Phase Epoxidation of Propylene over Au/Ti-MCM-41(H) Catalysts[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1585-1592
97. YUAN Jin-Fang, LI Jian-Sheng, GU Juan, WANG Fang, SUN Xiu-Yun, HAN Wei-Qing, WANG Lian-Jun.Synthesis and Adsorption Properties of Amino-Functionalized H2N-Zr-Ce-SBA-15 Mesoporous Materials with Short Mesochannels[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1711-1716
98. HE Yue, DONG Mei, LI Jun-Fen, WANG Jian-Guo, FAN Wei-Bin.Synthesis and Catalytic Properties of MeAPO-5 Molecular Sieves for Selective Oxidation of Cinnamyl Alcohol[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1305-1310
99. ZHANG Ai-Ping, ZHANG Jin-Zhi.Syntheses and Activities of Visible-Light-Driven Cu/BiVO4 Composite Photocatalysts[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1337-1342
100. SUN Dun, HE Jian-Ping, ZHOU Jian-Hua, WANG Tao, DI Zhi-Yong, WANG Dao-Jun, DING Xiao-Chun.MClx(M=Pd, Fe, Cr) Assisted Synthesis of Ordered Mesoporous Carbon and Their Electrocatalytic Performance after Loading with Pt Nanoparticles[J]. Acta Phys. -Chim. Sin., 2010,26(02): 385-391
101. YAN Dong-Xia, WANG Hua, LI Kong-Zhai, WEI Yong-Gang, ZHU Xing, CHENG Xian-Ming.Structure and Catalytic Property of Ce1-xFexO2 Mixed Oxide Catalysts for Low Temperature Soot Combustion[J]. Acta Phys. -Chim. Sin., 2010,26(02): 331-337
102. WANG Jin-E, YANG Chun.Direct Syntheses and Characterizations of PW11/SBA-15 Mesoporous Hybrid Materials[J]. Acta Phys. -Chim. Sin., 2010,26(02): 515-520
103. LI Kui-Ying, LIU Tong, ZHOU Bing-Jing, WEI Sai-Ling, YANG Wei-Yong.Transient Photovoltaic and Surface Photoacoustic Characteristics of Mesoporous Crystalline La-doped TiO2 Nanoparticles[J]. Acta Phys. -Chim. Sin., 2010,26(02): 403-408
104. HU Long-Xing, DANG Song-Tao, YANG Xia-Ping.Incorporation of CuO into Mesoporous Carbon CMK-3 and Its Adsorption and Catalytic Oxidation of Phenol[J]. Acta Phys. -Chim. Sin., 2010,26(02): 373-377
105. GENG Wang-Chang, LAI Xiao-Yong, LI Xiao-Tian.Ordered Mesoporous MgZnO with Crystalline Walls[J]. Acta Phys. -Chim. Sin., 2010,26(02): 527-530
106. XU Xin, WANG Xiao-Jing, HU Zhong-Hua, LIU Ya-Fei, WANG Chen-Chen, ZHAO Guo-Hua.Influence of Sol-Gel and Dip-Hydrothermal Preparation Methods on Structure and Performance of TiO2/AC Photocatalysts[J]. Acta Phys. -Chim. Sin., 2010,26(01): 79-86
107. WANG Tao, ZHOU Jian-Hua, WANG Dao-Jun, SUN Dun, DI Zhi-Yong, HE Jian-Ping.Syntheses and Infrared Emissivities of Ordered Mesoporous C-Al2O3 Nanocomposites[J]. Acta Phys. -Chim. Sin., 2009,25(10): 2155-2160
108. WANG Run-Han, JIANG Ji-Sen, HU Ming.Controlled Syntheses of FeNi3 Alloy Nanostructures via Reverse Microemulsion-Directed Hydrothermal Motheds[J]. Acta Phys. -Chim. Sin., 2009,25(10): 2167-2172
109. SUN Zhe, LIU Kai-Yu, ZHANG Hai-Feng, LI Ao-Sheng, XU Xiao-Cun.Study on Meso-C/MnO2 Asymmetric Supercapacitors[J]. Acta Phys. -Chim. Sin., 2009,25(10): 1991-1997
110. DONG Xiang, TAO Jie, LI Ying-Ying, WANG Tao, ZHU Hong.Photoelectrochemical Properties of Three-Dimensional Network TiO2 Nanowire Film Prepared by Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2009,25(09): 1874-1882
111. YU Yong, LIU Shi-Jun, LI Jie, CHEN Qi-Yuan.Preparation and Characterization ofMesoporous Tungsten Oxides[J]. Acta Phys. -Chim. Sin., 2009,25(09): 1890-1894
112. LV Yong, LU Wen-Cong, ZHANG Liang-Miao, YUE Bao-Hua, SHANG Xing-Fu, NI Ji-Peng.Synthesis, Characterization and Growth Mechanism of Core/Shell AlOOH Microspheres[J]. Acta Phys. -Chim. Sin., 2009,25(07): 1391-1396
113. SHEN Jing-Jing, LIU Chang, ZHU Yu-Dan, LI Wei, FENG Xin, LU Xiao-Hua.Photocatalytic Properties of Mesoporous TiO2 Prepared by Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2009,25(05): 1013-1018
114. CHEN Qi-Feng, JIANG Dong, XU Yao, WU Dong, SUN Yu-Han.Visible Region Photocatalysis of Ce-Si/TiO2 Synthesized Using Sol-Gel-Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2009,25(04): 617-623
115. LU Xia; TANG Jing; FAN Yu-Bing; HU Jun; LIU Hong-Lai.Synthesis of Mesoporous Polystyrene Using Reversed Microemulsion Template Method[J]. Acta Phys. -Chim. Sin., 2009,25(01): 178-182
116. JIN Zheng-Wei; LIU Chang-Ling; LIANG Hao.Effects of pH on the Structure of Non-Ionically Templated MSU-X Mesoporous Silica via a Two-Step Synthesis[J]. Acta Phys. -Chim. Sin., 2009,25(01): 150-154
117. WANG Tao, HE Jian-Ping, ZHANG Chuan-Xiang, ZHOU Jian-Hua, GUO Yun-Xia, CHEN Xiu, DI Zhi-Yong, SUN Dun, WANG Dao-Jun.Preparation and Electrochemical Properties of Ordered Mesoporous C/NiO Composites[J]. Acta Phys. -Chim. Sin., 2008,24(12): 2314-2320
118. ZHAO Rui-Hua, DONG Mei, QIN Zhang-Feng, DING Jian-Fei, GUO Xing-Cui, WANG Jian-Guo.Synthesis and Characterization of CoAPO-5 with different Cobalt Contents and Their Catalytic Performance for Cyclohexane Oxidation[J]. Acta Phys. -Chim. Sin., 2008,24(12): 2304-2308
119. JIN Zheng-Wei; WANG Xiao-Dong.Mechanism of Acidity-Induced Mesostructure Transformation for Highly Ordered Mesoporous Silica Materials and Their Functionalizations[J]. Acta Phys. -Chim. Sin., 2008,24(08): 1519-1523
120. LI Hai-Long; LUO Wu-Lin; CHEN Tao; TIAN Wen-Yu; SUN Mao; LI Chun; ZHU Di; LIU Ran-Ran; ZHAO Yu-Liang; LIU Chun-Li.Preparation and Photocatalytic Performance of Titania Nanotubes Loaded with Ag Nanoparticles[J]. Acta Phys. -Chim. Sin., 2008,24(08): 1383-1386
121. WANG Bai-Qi; XIA Chun-Hui; FU Qiang; WANG Peng-Wei; SHAN Xu-Dong; YU Da-Peng.Hydrothermal Preparation and Photoluminescence Property of Co-Doped ZnO Nanorods[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1165-1168
122. ZHOU Jian-Hua; HE Jian-Ping; JI Ya-Jun; ZHAO Gui-Wang; ZHANG Chuan-Xiang; CHEN Xiu; WANG Tao.Influence of Hierarchical Porosity in Carbon Material on Electrocatalytic Property of Supported Pt Nanoparticles[J]. Acta Phys. -Chim. Sin., 2008,24(05): 839-843
123. PEI Su-Peng; ZHANG Bin; JIAO Kun; BAO Ren-Lie; YUE Bin; HE He-Yong.Nanostructured CoMoO4 Supported on Mesoporous SBA-15 for Catalytic Oxidative Dehydrogenation of Propane to Propene[J]. Acta Phys. -Chim. Sin., 2008,24(04): 561-564
124. WANG Jian-Hua; LI Bin; WU Hai-Yan; GUO Yu-Zhong.Synthesis of Mesoporous SnO2 and Its Application in Lithium-Ion Battery[J]. Acta Phys. -Chim. Sin., 2008,24(04): 681-685
125. LIU Xiao-Lei; HE Jian-Ping; DANG Wang-Juan; JI Ya-Jun; ZHAO Gui-Wang; ZHANG Chuan-Xiang.Structural Characteristics and Humidity Sensing of Mesoporous SnO2[J]. Acta Phys. -Chim. Sin., 2008,24(03): 475-480
126. MA Xue-Hui; ZHAO Yan-Bao; XIAO Gao-Feng; WU Zhi-Shen.Synthesis of Mercaptopropyl Functionalized Nanosized Mesoporous Silica[J]. Acta Phys. -Chim. Sin., 2008,24(03): 492-496
127. CAO Ji-Lin; XING Dong-Qiang; LIU Xiu-Wu; TAN Zhao-Yang.Synthesis of Magnetic 4A Zeolite at Ultrasonic Condition[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1893-1898
128. SU Zhao-Hui; CHEN Qi-Yuan; LI Jie; LIU Shi-Jun.Preparation and Characterization of Mesoporous Silicon Dioxide Doped with Tungsten[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1760-1764
129. MA Na; JI Sheng-Fu; WU Ping-Yi; HU Lin-Hua; NIE Ping-Ying.Preparation, Characterization and Catalytic Performance for Hydrodesulfurization of WxC/SBA-16 Catalysts[J]. Acta Phys. -Chim. Sin., 2007,23(08): 1189-1194
130. DANG Wang-Juan; HE Jian-Ping; ZHOU Jian-Hua; JI Ya-Jun; LIU Xiao-Lei; MEI Tian-Qing; LI Hu-Lin.Dispersion and Electrocatalytic Performance of Platinum Nanoparticles Supported on Ordered Mesoporous Carbon[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1085-1089
131. ZHAO Hai-Jun; HOU Hai-Tao; CAO Jie-Ming ZHENG Ming-Bo; LIU Jing-Song; ZHANG Fang.Solvothermal Synthesis of Mesoporous SnO2 with Spongy Structure[J]. Acta Phys. -Chim. Sin., 2007,23(06): 959-963
132. ZHANG Xia; ZHAO Yan; ZHANG Cai-Bei; MENG Hao.Synthesis and Characterization of TiO2 Nano-crystalline with Different Morphologies by Low-temperature Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2007,23(06): 856-860
133. KE Xing-Fei; CAO Jie-Ming; ZHENG Ming-Bo; CHEN Yong-Ping; LIU Jin-Song.Synthesis of Hierarchically Meso-Macroporous Structured Carbon Sieve by Dual-template Method[J]. Acta Phys. -Chim. Sin., 2007,23(05): 757-760
134. LIU Yong; MENG Ming; YAO Jin-Song; ZHA Yu-Qing.Preparation and Characterization of the Multi-component Mesoporous Mixed Oxide La-Mn-Ce-O Catalysts[J]. Acta Phys. -Chim. Sin., 2007,23(05): 641-646
135. HAO Zhi-Xian;LIU Hui;GUO Bin;LI Hong;ZHANG Jia-Wei;GAN Li-Hua;XU Zi-Jie;CHEN Long-Wu.Sol-Gel Synthesis of Alumina Using Inorganic Salt Precursor[J]. Acta Phys. -Chim. Sin., 2007,23(03): 289-294
136. LI Cui-Ping;ZHAO Rui-Hong;GUO Fen;CHEN Jian-Feng.Preparation and Characterization of Ni Catalysts Supported on Organized Mesoporous Alumina[J]. Acta Phys. -Chim. Sin., 2007,23(02): 157-161
137. SONG Xu-Chun;ZHENG Yi-Fan;LIN Shen;WANG Yun.A Simple Method to Synthesize α-MnO2 and β-MnO2 Single-crystalline Nanorods[J]. Acta Phys. -Chim. Sin., 2007,23(02): 258-261
138. FANG Li-Mei;LI Zhi-Jie;LIU Chun-Ming;ZU Xiao-Tao.Synthesis of Fe3+-modified SnO2 Nanoparticles by Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2006,22(10): 1212-1216
139. ZHAO Chun-Xia;CHEN Wen;LIU Qi;TIAN Gao.Influence of HCl on the Mesostructure and Morphology of the Ordered Mesoporous Silica[J]. Acta Phys. -Chim. Sin., 2006,22(10): 1201-1205
140. HU Jun;WANG Jian-Jun;ZHOU Li-Hui;XIE Song-Hai;LIU Hong-Lai.The Mechanism of Mesoporous Phase Transition of Titanic-Silica Mesoporous Materials[J]. Acta Phys. -Chim. Sin., 2006,22(06): 679-683
141. ZHANG Xue-Hong;TANG Xing-Hua;CHENG Xin-Sun.Synthesis and Application of Ce-doped Mesoporous TiO2[J]. Acta Phys. -Chim. Sin., 2006,22(05): 532-537
142. HAO Yan-Zhong; HAN Wen-Tao.Preparation and Photoelectrochemical Properties of Titanate Nanotubes[J]. Acta Phys. -Chim. Sin., 2006,22(02): 221-225
143. HU Jun; ZHOU Li-hui; LI Hong-ning; LI Wan-xin; LIU Hong-lai; HU Ying.The Influences of the Spacer of Gemini Surfactants on the Structure of Silicic Mesoporous Materials[J]. Acta Phys. -Chim. Sin., 2005,21(11): 1217-1222
144. LIU Li-cheng; LI Hui-quan; CAI Wei-quan; ZHANG Yi.Synthesis, Characterization and Catalytic Activity of Mesoporous Cr-MSU-1[J]. Acta Phys. -Chim. Sin., 2005,21(11): 1311-1314
145. SONG Xu-chun; ZHENG Yi-fan; YIN Hao-yong; CAO Guang-sheng.Synthesis and Characterization of Transition Element Substituted Titanate Nanotubes[J]. Acta Phys. -Chim. Sin., 2005,21(10): 1076-1080
146. JIN Sheng-ming; QIU Guan-zhou; YANG Hua-ming; DENG Zhen-xia.Preparation of HMS and AlSBA Mesoporous Materials from Sepiolite[J]. Acta Phys. -Chim. Sin., 2005,21(07): 796-799
147. ZHENG Jun-Lin; ZHAI Shang-Ru; YANG Dong-Jiang; ZHANG Ye; WU Dong; SUN Yu-Han.Comparison on the Catalytic Cracking and Alkylation Activities between MSU-SMFI and MCM-41 Aluminosilicates[J]. Acta Phys. -Chim. Sin., 2005,21(03): 324-327
148. Dai Zhi-Hui;Ju Huang-Xian.Direct Electron Transfer of Protein Immobilized on Mesoporous Molecular Sieves Matrix[J]. Acta Phys. -Chim. Sin., 2004,20(10): 1262-1266
149. Zhu Jian-Hua;Xu Yang;Wang Ying;Zhou Shi-Lu;Zhou Chun-Fang.Adsorption and Catalytic Degradation of Nitrosamines by Zeolites and Molecular Sieves[J]. Acta Phys. -Chim. Sin., 2004,20(08S): 946-952
150. Cai Wei-Quan;Li Hui-Quan;Zhang Yi.Hydrothrmal Crystal Growth of Very Light Boehmite products[J]. Acta Phys. -Chim. Sin., 2004,20(07): 717-721
151. Shi Xi-E;Zhai Shang-Ru;Dai Li-Yi;Shan Yong-Kui;He Ming-Yuan;Wei Wei;Wu Dong;Sun Yu-Han.Synthesis of Mesoporous Aluminosilicate Nanoparticles and Its Performance in Catalytic Cracking[J]. Acta Phys. -Chim. Sin., 2004,20(03): 265-270
152. Nie Chun-Fa;Suo Ji-Shuan.Synthesis,Characterization and Catalytic Applications of Asymmetric Hydrogenation Catalyst Immobilized on Hybrid MCM-41[J]. Acta Phys. -Chim. Sin., 2004,20(02): 149-153
153. Liu Lei;Zhang Gao-Yong;Dong Jin-Xiang.Effects of Different Templating Agent on the Structure of Silica MCM-41 Mesoporous Molecular Sieves[J]. Acta Phys. -Chim. Sin., 2004,20(01): 65-69
154. Zheng Jun-Lin;Zhang Ye;Wei Wei; Wu Dong;Sun Yu-Han;Deng Feng;Luo Qing;Yue Yong.Hydrothermally Stable Mesoporous Aluminosilicates with Strongly Acidic Sites[J]. Acta Phys. -Chim. Sin., 2003,19(10): 907-912
155. Ni Qi-Liang;Zhang Jian-Cheng;Liu Jian-Min;Shen Yue.Fe/SAB-3 Composite Mesoporous Materials and Magnetic Properties[J]. Acta Phys. -Chim. Sin., 2003,19(10): 944-947
156. Guo Min;Diao Peng;Ren Yan-Jie;Wang Bin;Cai Sheng-Min.Preparation and Characterization of Highly Oriented ZnO Single Crystal Submicrorod Arrays[J]. Acta Phys. -Chim. Sin., 2003,19(05): 478-480
157. Cheng Hu-Min;Ma Yu-Rong;Liao Fu-Hui;Ma Ji-Ming;Qi Li-Min.Synthesis of Mesoporous Zirconia with Hydrothermal Homogeneous Precipitation Method[J]. Acta Phys. -Chim. Sin., 2003,19(04): 326-328
158. Zhang Bao-Hong;Zhang Na.Research on Nanophase MnO2 for Electrochemical Supercapacitor[J]. Acta Phys. -Chim. Sin., 2003,19(03): 286-288
159. Wang Jin-Zhong;Zhao Yan;Zhang Cai-Bei.Synthesis of Ordered Mesoporous TiO2 on a Composite Surfactant Template[J]. Acta Phys. -Chim. Sin., 2003,19(03): 251-255
160. Zhai Shang-Ru;Pu Min;Gong Yan-Jun;Zhang Ye;Wu Dong;Sun Yu-Han.The Synthesis of Mesoporous Molecular Sieve MCM-48 Using Two Surfactants as Co-template[J]. Acta Phys. -Chim. Sin., 2002,18(10): 911-915
161. Song Chun-Min;Yan Zi-Feng;Max Lu.Synthesis and Characterization of Supersurface MCM-41 Zeolites[J]. Acta Phys. -Chim. Sin., 2002,18(03): 279-283
162. Zhao Li-Li;Wang Rong-Shu;Niu Wen-Tai;Li Xiang.Synthesis of γ-MnO2 Nano Powder Used for SieveMembrane Reactor[J]. Acta Phys. -Chim. Sin., 2002,18(03): 197-200
163. Yao Yun-Feng;Zhang Mai-Sheng;Yang Yan-Sheng.Synthesis of Nano-sized MCM-41 Mesoporous Molecular Sieve by[J]. Acta Phys. -Chim. Sin., 2001,17(12): 1117-1121
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165. Gao En-Qin;Zhang Li;Yang Mai-Zhi;Cai Sheng-Min.Preparation of TiO2 Nanoparticles by Hydrothermal Method and its Application for Photoelectrochemical Cell[J]. Acta Phys. -Chim. Sin., 2001,17(02): 177-180
166. Wang Tong-Wen;Dai Le-Rong.Synthesis of Hexagonal Mesostructured Titaniumcontaining Silica by Mixed Supramolecular Templating[J]. Acta Phys. -Chim. Sin., 2001,17(01): 10-14
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168. Wang Tong-Wen, Chen Jing-Lei, Dai Le-Rong.Synthesis of Cubic Mesoporous Titanium-containing Silica by Mixed Surfactant Templating[J]. Acta Phys. -Chim. Sin., 2000,16(05): 385-388
169. Tian Jian-Hua,Gu Lin-Ying.Study of the Reduction Mechanism of MnO2 by Rotating Ring-Disk Electrode[J]. Acta Phys. -Chim. Sin., 1996,12(05): 446-450
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