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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2011,Vol.27>> Issue(03)>> 736-742     doi: 10.3866/PKU.WHXB20110320         中文摘要
PHYSICAL CHEMISTRY OF MATERIALS
Synthesis and Structural Characterization of Graphene-Based Membranes
YANG Yong-Hui1, SUN Hong-Juan2, PENG Tong-Jiang2, HUANG Qiao1
1. College of Science, Southwest University of Science and Technology, Mianyang 621010, Sichuan Province, P. R. China;
2. Institute of Mineral Materials & Application, Southwest University of Science and Technology, Mianyang 621010, Sichuan Province, P. R. China
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A stable hydrosol of graphene was synthesized by oxidation reduction and then a flow assembly of this graphene was used to form a graphene-based membrane by vacuum extraction filtering method. X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, Raman spectroscopy, particle size analysis, and scanning probe microscopy (SPM) were used to characterize the crystal structure, granularity, and characteristic change of the molecular spectrum of the samples in the reaction. FTIR tests show that the structural layer of graphite during the oxidation process bonds to a large number of functional groups and parts of these stable functional groups remain on the reduced structural layer of graphene. X-ray diffraction results show that the peaks of the graphite oxide shift to lower angles, become broader and the original graphite peak disappears. Suspensions of graphene oxide form condensed matter and graphene flocculating constituent during film deposition. Particle size analysis and SPM tests show that the particle sizes of the graphene oxide sheets that are dispersed in water show a tailing peak and a broad distribution while the graphene sheets show a singlet, narrower distribution, and smaller dimensions. Raman results show that during oxidation and reduction, the D peak and G peak of the samples gradually extend, ID/IG increases gradually and the degree of sample disorder increases. On the basis of the above analyses, the structural characteristics of the samples in the reaction are summarized.



Keywords: Graphite   Graphite oxide   Graphene   Oxidation reduction   Crystal structure  
Received: 2010-09-30 Accepted: 2010-12-26 Publication Date (Web): 2011-02-15
Corresponding Authors: SUN Hong-Juan Email: sunhongjuan@swust.edu.cn

Fund: The project was supported by the Postgraduate Innovation Fund of Southwest University of Science and Technology, China (10ycjj21).

Cite this article: YANG Yong-Hui, SUN Hong-Juan, PENG Tong-Jiang, HUANG Qiao. Synthesis and Structural Characterization of Graphene-Based Membranes[J]. Acta Phys. -Chim. Sin., 2011,27 (03): 736-742.    doi: 10.3866/PKU.WHXB20110320

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68. LI Shang, WANG Jia-Tang, CHEN Rui-Xin, ZHAO Wei, QIAN Liu, PAN Mu.Catalytic Performance of Heat-Treated Fe-Melamine/C and Fe-g-C3N4/C Electrocatalysts for Oxygen Reduction Reaction[J]. Acta Phys. -Chim. Sin., 2013,29(04): 792-798
69. HONG Zhou-Qin, LI Jin-Xia, ZHANG Fang, ZHOU Li-Hui.Synthesis of Magnetically Graphitic Mesoporous Carbon from Hard Templates and Its Application in the Adsorption Treatment of Traditional Chinese Medicine Wastewater[J]. Acta Phys. -Chim. Sin., 2013,29(03): 590-596
70. PAN Hui, ZHAO Tian, ZHANG Yu-Dong, ZHANG Zhi-Jun.Preparation, Characterization and Properties of Titania/Graphite Oxide Nanocomposite[J]. Acta Phys. -Chim. Sin., 2013,29(03): 660-666
71. XU Gui-Yin, DING Bing, NIE Ping, LUO Hong-Jun, ZHANG Xiao-Gang.Preparation and Electrochemical Performance of Carbon Nanotubes/ Graphene Oxide/Sulfur Complex Cathode Material[J]. Acta Phys. -Chim. Sin., 2013,29(03): 546-552
72. GAN Yong-Ping, QIN Huai-Peng, HUANG Hui, TAO Xin-Yong, FANG Jun-Wu, ZHANG Wen-Kui.Preparation and Photocatalytic Activity of Rutile TiO2-Graphene Composites[J]. Acta Phys. -Chim. Sin., 2013,29(02): 403-410
73. ZOU Hui, NI Xiang, PENG Sheng-Lin, OUYANG Jun, CHEN Yu, OUYANG Fang-Ping.First-Principles Study of Graphene-Based Biomolecular Sensor[J]. Acta Phys. -Chim. Sin., 2013,29(02): 250-254
74. HU Ying-Ying, HU Zhong-Ai, ZHANG Ya-Jun, LU Ai-Lian, XU Huan, ZHANG Zi-Yu, YANG Yu-Ying, LI Li, WU Hong-Ying.Synthesis and Electrochemical Characterization of RuO2·xH2O/Graphite Nanosheet Composite Array Electrodes for Supercapacitors[J]. Acta Phys. -Chim. Sin., 2013,29(02): 305-310
75. WANG Hong-Zhi, GAO Cui-Xia, ZHANG Peng, YAO Su-Wei, ZHANG Wei-Guo.Synthesis and Electrochemical Performance of Graphene/Polyaniline[J]. Acta Phys. -Chim. Sin., 2013,29(01): 117-122
76. WANG Wan-Li, MA Zi-Feng.Synthesis and Characteristics of Pt/graphene by Co-Reduction Method for Oxygen Reduction Reactions[J]. Acta Phys. -Chim. Sin., 2012,28(12): 2879-2884
77. LI Song-Mei, WANG Bo, LIU Jian-Hua, YU Mei, AN Jun-Wei.Synthesis and Microwave Absorption Properties of Nickel Nanoparticles-Graphene Composites with Different Morphologies[J]. Acta Phys. -Chim. Sin., 2012,28(11): 2754-2760
78. SU Peng, GUO Hui-Lin, PENG San, NING Sheng-Ke.Preparation of Nitrogen-Doped Graphene and Its Supercapacitive Properties[J]. Acta Phys. -Chim. Sin., 2012,28(11): 2745-2753
79. LING Xi, ZHANG Jin.Investigation of the Adsorption Behavior of PbPc on Graphene by Raman Spectroscopy[J]. Acta Phys. -Chim. Sin., 2012,28(10): 2355-2362
80. ZHANG Yan-Feng, GAO Teng, ZHANG-Yu, LIU Zhong-Fan.Controlled Growth of Graphene on Metal Substrates and STM Characterizations for Microscopic Morphologies[J]. Acta Phys. -Chim. Sin., 2012,28(10): 2456-2464
81. FAN Cheng-Wei, ZHANG Xin, CHEN Sheng, WANG Hai-Fang, CAO Ao-Neng.Solution-Processable, Highly Conductive, Permanently Rippled Graphene Sheets[J]. Acta Phys. -Chim. Sin., 2012,28(10): 2465-2470
82. GAO Shuai, WU Yong-Quan, SHEN Tong, ZHANG Ning, LAI Li-Shan.Analysis of Zn-Mg Alloy Structure and Phases Distribution of Zn-Mg Diffusion System[J]. Acta Phys. -Chim. Sin., 2012,28(09): 2037-2043
83. HUA Xiao-Hui, LI Wei-Hong, XU Yi-Zhuang, WU Jin-Guang.Crystal Structures and Pore Stability of Coordination Polymers Constructed by Nicotinic Acid and Isonicotinic Acid with Co(II)[J]. Acta Phys. -Chim. Sin., 2012,28(08): 1815-1822
84. ZHANG Jun-Jun, ZHANG Zhen-Hua, GUO Chao, LI Jie, DENG Xiao-Qing.Electronic Transport Properties for a Zigzag-Edged Triangular Graphene[J]. Acta Phys. -Chim. Sin., 2012,28(07): 1701-1706
85. SHEN Bao-Shou, FENG Wang-Jun, LANG Jun-Wei, WANG Ru-Tao, TAI Zhi-Xin, YAN Xing-Bin.Nitric Acid Modification of Graphene Nanosheets Prepared by Arc- Discharge Method and Their Enhanced Electrochemical Properties[J]. Acta Phys. -Chim. Sin., 2012,28(07): 1726-1732
86. RAN Ke, CHEN Qing, ZUO Jian-Min.Fabrication and Structure Characterization of Quasi-2-Dimensional Amorphous Carbon Structures[J]. Acta Phys. -Chim. Sin., 2012,28(07): 1551-1555
87. ZHANG Xiao, YANG Rong, WANG Chen, HENG Cheng-Lin.Cell Biocompatibility of Functionalized Graphene Oxide[J]. Acta Phys. -Chim. Sin., 2012,28(06): 1520-1524
88. LIU Bo, SUN Hong-Juan, PENG Tong-Jiang.Factor Group Analysis of Molecular Vibrational Modes of Graphene and Density Functional Calculations[J]. Acta Phys. -Chim. Sin., 2012,28(04): 799-804
89. SUN Ya-Ping, FAN Xin-Zhuang, LU Yong-Hong, XU Hai-Bo.Electrocatalytic Performance and Pseudo-Capacitive Characteristics of Modified Graphite Electrode with Fe3+/Fe2+ in H2SO4 Solution[J]. Acta Phys. -Chim. Sin., 2012,28(03): 603-608
90. JIN Yu, CHEN Hong-Yuan, CHEN Ming-Hai, LIU Ning, LI Qing-Wen.Carbon Nanotube/Polyaniline/Graphene Composite Paper and Its Electrochemical Capacitance Behaviors[J]. Acta Phys. -Chim. Sin., 2012,28(03): 609-614
91. XIE Peng-Yang, ZHUANG Gui-Lin, LÜ Yong-An, WANG Jian-Guo, LI Xiao-Nian.Enhanced Bonding between Noble Metal Adatoms and Graphene with Point Defects[J]. Acta Phys. -Chim. Sin., 2012,28(02): 331-337
92. XU Ke, SHEN Lai-Fa, MI Chang-Huan, ZHANG Xiao-Gang.Synthesis and Electrochemical Performance of Graphene Modified LiFePO4 Cathode Materials[J]. Acta Phys. -Chim. Sin., 2012,28(01): 105-110
93. ZHANG Xiao-Yan, SUN Ming-Xuan, SUN Yu-Jun, LI Jing, SONG Peng, SUN Tong, CUI Xiao-Li.Photoelectrochemical Properties of Graphene Oxide Thin Film Electrodes[J]. Acta Phys. -Chim. Sin., 2011,27(12): 2831-2835
94. DU Xiao-Ming, LI Wu-Hui, HUANG Yong, WU Er-Dong.First-Principles Calculation of the Crystal Structure and Stabilization of Mg-Ti-H System[J]. Acta Phys. -Chim. Sin., 2011,27(12): 2793-2798
95. ZHOU Ai-Jun, CUI Heng-Guan, LI Jing-Ze, ZHAO Xin-Bing.Structure and Morphology of Induction-Melted Higher Manganese Silicide[J]. Acta Phys. -Chim. Sin., 2011,27(12): 2915-2919
96. TANG Jun, KANG Chao-Yang, LI Li-Min, XU Peng-Shou.Direct Graphene Growth by Depositing Carbon Atoms on Si Substrate Covered by SiC Buffer Layers[J]. Acta Phys. -Chim. Sin., 2011,27(12): 2953-2959
97. LIU Dong-Yang, CHENG Jie, PAN Jun-Qing, WEN Yue-Hua, CAO Gao-Ping, YANG Yu-Sheng.All-Lead Redox Flow Battery in a Fluoroboric Acid Electrolyte[J]. Acta Phys. -Chim. Sin., 2011,27(11): 2571-2576
98. YANG Xiao-Wei, HE Yu-Shi, LIAO Xiao-Zhen, MA Zi-Feng.Improved Graphene Film by Reducing Restacking for Lithium Ion Battery Applications[J]. Acta Phys. -Chim. Sin., 2011,27(11): 2583-2586
99. LU Xiang-Jun, DOU Hui, YANG Su-Dong, HAO Liang, ZHANG Fang, ZHANG Xiao-Gang.Fabrication and Electrochemical Capacitive Behavior of Freestanding Graphene/Polyaniline Nanofibre Film[J]. Acta Phys. -Chim. Sin., 2011,27(10): 2333-2339
100. XU Ning, ZHANG Chao, KONG Fan-Jie, SHI You-Jin.Transport Properties of Corrugated Graphene Nanoribbons[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2107-2110
101. YUAN Wen-Hui, LI Bao-Qing, LI Li.Superior Graphene for Hydrogen Adsorption Prepared by the Improved Liquid Oxidation-Reduction Method[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2244-2250
102. MIN Shi-Xiong, Lü Gong-Xuan.Preparation of CdS/Graphene Composites and Photocatalytic Hydrogen Generation from Water under Visible Light Irradiation[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2178-2184
103. GAO Wen-Chao, HUANG Tao, SHEN Yu-Dong, YU Ai-Shui.Phenolic Resin Coated Natural Graphite Oxide as an Anode Material for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2129-2134
104. LI Xue-Fei, ZHAO Yun, JIAO Qing-Ze, LI Han-Sheng, WU Hong-Yu, LIU Hong-Bo, CUI Wen-Jia.Preparation of One-Dimensional Titanate Nanomaterials Using Different Titania Sources[J]. Acta Phys. -Chim. Sin., 2011,27(08): 1996-2000
105. JIN Jing, GONG Yuan-Yuan, WU Han-Qing, LI Lei, NIU Shu-Yun.Crystal Structure and Surface Photoelectric Property of Mn(II) Coordination Complexes[J]. Acta Phys. -Chim. Sin., 2011,27(07): 1587-1594
106. YING Hong, WANG Zhi-Yong, GUO Zheng-Duo, SHI Zu-Jin, YANG Shang-Feng.Reduced Graphene Oxide-Modified Bi2WO6 as an Improved Photocatalyst under Visible Light[J]. Acta Phys. -Chim. Sin., 2011,27(06): 1482-1486
107. ZHANG Yi, CHEN Biao, YANG Zu-Pei, ZHANG Zhi-Jun.Controlled Synthesis and Characterization of the Structure and Property of Fe3O4 Nanoparticle-Graphene Oxide Composites[J]. Acta Phys. -Chim. Sin., 2011,27(05): 1261-1266
108. SUN Da-Li, PENG Sheng-Lin, OUYANG Jun, OUYANG Fang-Ping.Electronic Transport Properties of Graphene Nanoribbons with Nanoholes[J]. Acta Phys. -Chim. Sin., 2011,27(05): 1103-1107
109. LI Yun-Xia, WEI Zi-Dong, ZHAO Qiao-Ling, DING Wei, ZHANG Qian, CHEN Si-Guo.Preparation of Pt/Graphene Catalyst and Its Catalytic Performance for Oxygen Reduction[J]. Acta Phys. -Chim. Sin., 2011,27(04): 858-862
110. FAN Xin-Zhuang, LU Yong-Hong, KONG Xiang-Feng, XU Hai-Bo, WANG Jia.Pseudo-Capacitive and Electrocatalytic Properties of Electrochemically Modified Graphite Electrode in Different Solutions[J]. Acta Phys. -Chim. Sin., 2011,27(04): 887-892
111. XU Ning, KONG Fan-Jie, WANG Yan-Zong.Electronic Transport in Z-Shaped Graphene-Nanoribbons: Shape and Size Effects[J]. Acta Phys. -Chim. Sin., 2011,27(03): 559-563
112. CAO Yun-Zhu, WEI Dong-Ming, REN Dong-Xue, CHEN Chen, XING Yong-Heng, SHI Zhan.Design, Synthesis and Mimic Catalytic Activity of a Vanadium Haloperoxidase Conformation Model Molecule[J]. Acta Phys. -Chim. Sin., 2011,27(03): 539-546
113. DAI Xian-Qi, LI Yan-Hui, ZHAO Jian-Hua, TANG Ya-Nan.Effects of Vacancy and Boron Doping on Si Adsorption on Graphene[J]. Acta Phys. -Chim. Sin., 2011,27(02): 369-373
114. XU Zi-Jie, JI Tao, WANG Wei-Yan, XIA Bing-Zhong, MA Chao, GAN Li-Hua.Phase Transformation of Pyrocarbon in Molten Sodium Metal[J]. Acta Phys. -Chim. Sin., 2011,27(01): 262-266
115. WU Xiao-Qin, ZONG Rui-Long, MU Hao-Jie, ZHU Yong-Fa.Cataluminescence Performance on Catalysts of Graphene Supported Platinum[J]. Acta Phys. -Chim. Sin., 2010,26(11): 3002-3008
116. FENG Jin-Ling, ZHANG Jian-Guo, ZHANG Tong-Lai, CUI Yan.Synthesis, Crystal Structure, Thermal Behavior and Sensitivity of [Mn(AZT)2(H2O)4] (HTNR)2·4H2O[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2410-2416
117. HU Yao-Juan, JIN Juan, ZHANG Hui, WU Ping, CAI Chen-Xin.Graphene: Synthesis, Functionalization and Applications in Chemistry[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2073-2086
118. ZHAO Jun, ZHENG Ming-Xian, LIN Yi-Ji, CHEN Yuan-Chuan, RUAN Yuan-Ping, ZHANG Hui.Inclusion Resolution of 1,1'-Bi-2-naphthol: Crystal Structure and CD Spectroscopy of the Inclusion Complexes[J]. Acta Phys. -Chim. Sin., 2010,26(07): 1832-1836
119. WEN Zhu-Liang, YANG Su-Dong, SONG Qi-Jun, HAO Liang, ZHANG Xiao-Gang.High Activity of Pd/Graphene Catalysts for Ethanol Electrocatalytic Oxidation[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1570-1574
120. YU Yu-Ye, LIU Jian-Feng, LI Hua-Qiong, ZHAO Guo-Liang.Synthesis, Crystal Structure and Fluorescence Spectrum of a Ytterbium(III) Complex with 3,4-Dimethoxyphenylacetic Acid and 1,10-Phenanthroline[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1535-1540
121. LU Hui-Zhe, FENG Zhen-Gao, LI Chang, YUAN Hui-Zhu, QIN Zhao-Hai.Electronic Structure Comparison between Pyrimorph and Its Phenyl Analog[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1623-1628
122. GAN Lin, LIU Song, LI Dan-Na, GU Hang, CAO Yang, SHEN Qian, WANG Zhen-Xing, WANG Qing, GUO Xue-Feng.Facile Fabrication of the Crossed Nanotube-Graphene Junctions[J]. Acta Phys. -Chim. Sin., 2010,26(04): 1151-1156
123. WANG Yong-Feng, ZHANG Xin-Ran, YE Ying-Chun, LIANG De-Jian, WANG Yuan, WU Kai.Self-Assemblies of Oxovanadium Phthalocyanine Molecules and Nanoclusters on Highly Oriented Pyrolytic Graphite[J]. Acta Phys. -Chim. Sin., 2010,26(04): 933-938
124. QIAN Bao-Hua, MA Wei-Xing, LU Lu-De, YANG Xu-Jie, WANG Xin.Synthesis, Characterization, Crystal Structure and Quantum Chemistry Calculation of an Arenedisulfonate Bridged Zn(II) Coordination Polymer[J]. Acta Phys. -Chim. Sin., 2010,26(03): 610-616
125. ZHANG Qiong, HE Yun-Qiu, CHEN Xiao-Gang, HU Dong-Hu, LI Lin-Jiang, YIN Ting, JI Ling-Li.Intercalated Structure and Photocatalytic Properties of TiO2-Graphite Oxide Composite[J]. Acta Phys. -Chim. Sin., 2010,26(03): 654-662
126. LIANG Peng, XU Hong-Feng, LIU Ming, LU Lu, FU Jie.Electrochemical Performance Testing and Characterization of Silver-Plated and Graphite-Coated 316L Stainless Steel Bipolar Plates[J]. Acta Phys. -Chim. Sin., 2010,26(03): 595-600
127. TANG Jun, LIU Zhong-Liang, KANG Chao-Yang, YAN Wen-Sheng, XU Peng-Shou, PAN Hai-Bin, WEI Shi-Qiang, GAO Yu-Qiang, XU Xian-Gang.Annealing Time Dependence of Morphology and Structure of Epitaxial Graphene on 6H-SiC(0001) Surface[J]. Acta Phys. -Chim. Sin., 2010,26(01): 253-258
128. LI Ye, HAN Wei-Wei, LIAO Ming-Xia.Spectroscopic and Crystal Structural Analyses of Zinc (II) Tetraphenylporphyrin J-aggregates[J]. Acta Phys. -Chim. Sin., 2009,25(12): 2493-2500
129. YU Hong-Ming, ZHENG Wei, CAO Gao-Shao, ZHAO Xin-Bing.Effects of Optimized Carbon-Coating on High-Rate Performance of LiFePO4/C Composites[J]. Acta Phys. -Chim. Sin., 2009,25(11): 2186-2190
130. FU Mao-Hua, HUANG Ke-Long, LIU Su-Qin, LIU Jian-Sheng, LI Yong-Kun.Effect of Lithium Difluoro(oxalato)borate on the High-Temperature Performance of LiFePO4/Graphite Batteries[J]. Acta Phys. -Chim. Sin., 2009,25(10): 1985-1990
131. ZHAO Jian-Wei, WANG Fen-Ying, JIANG Lu-Yun, YIN Xing, LIU Yun-Hong.Breaking Behavior of a Bicrystal Copper Nanowire Studied Using a Fourier Transformation Method[J]. Acta Phys. -Chim. Sin., 2009,25(09): 1835-1840
132. WANG Chun-Guang, XING Yong-Heng, XIE Yan, LI Zhang-Peng, LI Jing, ZENG Xiao-Qing, GE Mao-Fa.Syntheses, Structures and Luminescent Properties of the Heterometallic Complexes [Ln2Zn2(2,5-pydc)5(H2O)2]·4H2O[J]. Acta Phys. -Chim. Sin., 2009,25(08): 1545-1549
133. ZHANG Li, NIU Shu-Yun, JIN Jing, SUN Li-Ping, SHI Zhong-Feng, LI Lei.Preparation and Light-Induced Surface Electron Behavior of Ni(II) Based on Aromatic Polycarboxyl Acids[J]. Acta Phys. -Chim. Sin., 2009,25(06): 1161-1166
134. LI Zhang-Peng, XING Yong-Heng, ZHANG Yuan-Hong, BAI Feng-Ying, ZENG Xiao-Qing, GE Mao-Fa.Synthesis, Structure and Quantum Chemistry Calculation of Scorpionate Oxovanadium Complexes with Benzoate[J]. Acta Phys. -Chim. Sin., 2009,25(04): 741-746
135. ZHUANG Quan-Tiao, WEI Guo-Zhen, DONG Quan-Feng, SUN Shi-Gang.Influence of Temperature on the Performance of a Graphite Electrode[J]. Acta Phys. -Chim. Sin., 2009,25(03): 406-410
136. ZHANG Hai-Quan; YANG Bing; YANG Guang-Di; MA Yu-Guang.Investigation on Conformation of a Series of Functional Bridged Biphenyl Containing Seven-Member Heterocycle by X-ray Single Crystal Diffraction[J]. Acta Phys. -Chim. Sin., 2008,24(10): 1879-1883
137. QIAN Bao-Hua; MA Wei-Xing; XU Xing-You; LU Lu-De; YANG Xu-Jie; WANG Xin.Synthesis, Characterization and Quantum Chemistry Study of a One-dimensional Chain Coordination Polymer [Zn(acac)2(4,4’-bipy)]n[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1650-1654
138. LIU Zhen-Hua; AO Guo-Jun; ZHANG Tong-Lai; YANG Li; ZHANG Jian-Guo; ZANG Yan.Synthesis, Crystal Structure and Thermal Analysis of (TAGH)2(TNR)[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1155-1159
139. ZHANG Jin; ZHANG Tong-Lai; YANG Li; ZHANG Jian-Guo; CUI Yan.Preparation, Crystal Structure and Thermal Decomposition Character of [Ni(CHZ)3]SO4·3H2O[J]. Acta Phys. -Chim. Sin., 2008,24(05): 760-766
140. HU Xiao-Chun; ZHANG Tong-Lai; QIAO Xiao-Jing; YANG Li; ZHANG Jian-Guo; CUI Yan; ZHANG Jin.Crystal Structure and Thermal Decomposition of 5-Aminotetrazole Trinitrophloroglucinolate[J]. Acta Phys. -Chim. Sin., 2008,24(04): 576-580
141. QIAN Li-Ping; DENG Wen-Li.Adsorption Characteristics of Self-assembled 1-Octadecanol Layer on HOPG[J]. Acta Phys. -Chim. Sin., 2008,24(03): 443-447
142. SHI Zhi-Qiang; CHEN Ming-Ming; ZHAO Shuo; WANG Cheng-Yang.Structure and Electrochemical Capacitive Behavior of Novel Crystallite Carbon[J]. Acta Phys. -Chim. Sin., 2008,24(02): 237-242
143. OUYANG Fang-Ping; XU Hui; LI Ming-Jun; XIAO Jin.Electronic Structure and Transport Properties of Armchair Graphene Nanoribbons[J]. Acta Phys. -Chim. Sin., 2008,24(02): 328-332
144. YANG Wei-Chun; JU Chuan-Chuan; FAN Su-Hua; SUN Hao-Ling; WANG Ke-Zhi.Crystal Structure and Acid-Base Properties of Ozagrel[J]. Acta Phys. -Chim. Sin., 2008,24(01): 176-178
145. ZHANG Bao-Li; XING Yong-Heng; GE Mao-Fa; SUN Zheng; LI Zhang-Peng; HAN Jing; NIU Shu-Yun.Synthesis, Structure and Non-thermal Decomposition Kinetics of Scorpionates Oxovanadium Complexes with Carboxyl Acid Ligand[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1701-1706
146. XIONG Jing; CAI Xiao-Qing; YIN Ping; HU Mao-Lin.Crystal Structure, Spectroscopic and Thermal Properties of 2-(toluene-4-sulfonylamino)-benzoic Acid[J]. Acta Phys. -Chim. Sin., 2007,23(08): 1183-1188
147. YANG Zi-Liang;YANG Si-Hai;LI Guo-Bao;LIN Jian-Hua.Synthesis, Structure and Thermal Properties of [HN(C2H5)3][B5O6(OH)4][J]. Acta Phys. -Chim. Sin., 2007,23(03): 285-288
148. GUO Jin-Yu;ZHANG Jian-Guo;ZHANG Tong-Lai;WU Rui-Feng;YU Wei.Thermal Decomposition Mechanisms of a Three-dimensional Framework Coordination Polymer [Cu(HCOO)2(H2O)2][J]. Acta Phys. -Chim. Sin., 2006,22(10): 1206-1211
149. YUAN Wei;LI He-Xian;WANG Ying;WANG Guo-Chang.Theoretical Prediction of Crystal Structure of N-(1-naphthyl) Succinimide Compound[J]. Acta Phys. -Chim. Sin., 2006,22(09): 1071-1074
150. CHEN Hu;XU Xing-You;GAO Jian;YANG Xu-Jie;LU Lu-De;WANG Xin.Study on Crystal Structure of [Ni(phen)3](ClO4)2[J]. Acta Phys. -Chim. Sin., 2006,22(07): 856-859
151. DIAO Yu-Xia;ROHDE Dirk;WAN Li-Jun.Ordered Self-assembled Monolayers of β-dicarbonyl Derivatives Studied by STM[J]. Acta Phys. -Chim. Sin., 2006,22(06): 691-695
152. YANG Jian;QIU Tai;SHEN Chun-Ying.Synthesis and Characterization of a Novel Precursor for BCN Compound[J]. Acta Phys. -Chim. Sin., 2005,21(12): 1373-1377
153. LI Lin-yan; LI Guo-bao; LIAO Fu-hui; LIN Jian-hua.Synthesis and Structure of La[B5O8(OH)(H2O)]NO3•2H2O[J]. Acta Phys. -Chim. Sin., 2005,21(07): 769-773
154. Shi Xue-Song;Du Miao;Bu Xian-He.Development of the Coordination Chemistry of Diazamesocycles[J]. Acta Phys. -Chim. Sin., 2004,20(08S): 917-923
155. Li Zeng-He;Yin Chen;Wang Ru-Ji;Wang Ping;Guo Hong-You.Synthesis and Crystal Structure of an Inorganic-Organic Hybrid CompoundCo(μ2-bpy)V2O6 (bpy=4,4’-bipyridine)[J]. Acta Phys. -Chim. Sin., 2003,19(12): 1133-1137
156. Xu Kang;Xue Qun-Ji.A New Method for Deaggregation of Nanodiamond from Explosive Detonation—— Graphitization-Oxidation Method[J]. Acta Phys. -Chim. Sin., 2003,19(11): 993-995
157. Chen Ji-Tao;Zhou Heng-Hui;Chang Wen-Bao;Ci Yun-Xiang.Effect of Particle Size on Lithium Intercalation Performance of Graphite Anode[J]. Acta Phys. -Chim. Sin., 2003,19(03): 278-282
158. Wang Wen-Zhi;Fan Neng-Ting.Synthesis and Crystal Structure of 4,4’-Oxobis(propham)[J]. Acta Phys. -Chim. Sin., 2003,19(01): 75-78
159. Ning Jia-Cheng;Yang Ao;Guan Ye-Di;Wang Zhe-Ming;Yan Chun-Hua.The Resolution of the Optical Active Derivatives of Ketorolac and the Determination of its Absolute Configuration[J]. Acta Phys. -Chim. Sin., 2002,18(09): 821-824
160. Tang Xin-Cun;He Li-Ping;Chen Zong-Zhang;Xia Xi.Determination of the Li+ Diffusion Coefficient in Graphite By the Method of the Ratio of Potentio-charge Capacity to Galvano-charge Capacity[J]. Acta Phys. -Chim. Sin., 2002,18(08): 705-709
161. Zhang Hao;Suo Quan-Ling;Wang Yi-Bin;Wang Li;Weng Lin-Hong;Leng Xue-Bing.Synthesis and Crystal Structure of (μ3-S)FeCo2(CO)7(dppfe)[J]. Acta Phys. -Chim. Sin., 2002,18(08): 746-749
162. Liu Guang;Zhang ShiWei.Synthesis and Structure of a Novel 18Mo Polyoxomolybdate[J]. Acta Phys. -Chim. Sin., 2002,18(07): 624-628
163. Li Qi;Wen Xiao-Quan;Cai Xiao-Hai;Wang Xian-Rong;Xie You-Chang.Software BVStr for Analyzing the Structure of Crystal and Surface Based on the Bond Valence Theory[J]. Acta Phys. -Chim. Sin., 2002,18(06): 558-562
164. Song Xiang-Zhi;Liu Guang;Zhang Shi-Wei.Synthesis and Crystal Structures of Cancer Cell Inducers of Differentiation PMDH[J]. Acta Phys. -Chim. Sin., 2002,18(06): 545-549
165. Chen Ji-Tao;Zhou Heng-Hui;Chang Wen-Bao;Ci Yun-Xiang.pyrolytic Carbon Coated Graphite Anode for Lithium Ion Battery[J]. Acta Phys. -Chim. Sin., 2002,18(02): 180-182
166. Lu Xue-Fang;Zhang Hai-Rong;Li Yi;Liu Jing;Yang Guo-Qiang.Luminescence Properties and Crystal Structure of Two Metal 8-hydroxyquinoline Complexes at High Pressure[J]. Acta Phys. -Chim. Sin., 2001,17(10): 898-903
167. Liu Xin-Mei;Yan Zi-Feng;Wang Huai-Ping.Optimization of Zeolite for Producing Lighter Olefin and Diesel in FCC Process[J]. Acta Phys. -Chim. Sin., 2001,17(06): 547-551
168. Tang Zhi-Yuan;Xue Jian-Jun;Li Jian-Gang;Wang Zhan-Liang.Discharge Process of Insertion Electrodes Controlled by Lithium Ion Diffusion in Solid Materials[J]. Acta Phys. -Chim. Sin., 2001,17(06): 526-530
169. Tang Zhi-Yuan;Xue Jian-Jun;Liu Chun-Yan;Zhuang Xin-Guo.Determination of the Lithium Ion Diffusion Coefficient in Graphite Anode Material[J]. Acta Phys. -Chim. Sin., 2001,17(05): 385-388
170. Zeng Xi-Rui;Zhang Yong;You Xiao-Zeng.Substituent Effect of the Peroxyoxalate Chemiluminescence[J]. Acta Phys. -Chim. Sin., 2001,17(04): 361-363
171. Zhao Bo, Zhang Dao, Cao Yang, Chen Wen-Jian, Sun Zhen-Rong, Wang Zu-Geng.Analysis of the Second-order Nonlinear Optical Properties of some Chalcones[J]. Acta Phys. -Chim. Sin., 2000,16(05): 422-425
172. Zhang Wen-Qin, Zhang Zhi-Ming, Zheng Yan, Wang Shu-Li, Zhao Shu-Na.Crystal Structure and Photochemical Properties of r-1,c-2,t-3,t-4-1,3-bis(4-biphenyl)-2,4-di(4-pyridyl)cyclobutane[J]. Acta Phys. -Chim. Sin., 2000,16(03): 207-213
173. Chen Zhen, Wang Ru-Ji.Synthesis of Transition Metal Chalcogenide [M(en)3]2Sn2Se6(M=Mn,Zn) and Studies of Thermogravimeric Properties[J]. Acta Phys. -Chim. Sin., 1999,15(12): 1070-1075
174. Miao Fang-Ming, Fan Zhi, Zhou Wei-Hong, Qi Li-Ning, Li Ai-Xiu, Liu Xiao-Lan.Synthesis and Crystal Structure and Quantum Chemistry of Tris(2-benzimidazylmethyl)amine with Manganese(II)[J]. Acta Phys. -Chim. Sin., 1999,15(09): 775-782
175. Wang Xiao-Ling, Suo Quan-Ling, Wang Yi-Bing, Sun Jie.Synthesisi and Crystal Structure of FeCo2(CO)73-S)(O[P(SCH2)2]2)[J]. Acta Phys. -Chim. Sin., 1999,15(08): 757-760
176. Ding Er-Run, Wu Shu-Lin, Li Qing-Shan, Yin Yuan-Qi.Synthesis,Structural Characterization and Reaction of the Chiral Clusters[J]. Acta Phys. -Chim. Sin., 1999,15(03): 241-246
177. Wei Kun, Shi Yan, He Lun-Yan.Crystal Structure and Infrared Spectra of Nanocrystalling Rare Earth Mixed Oxides Dy1-xSrxCoO3-y[J]. Acta Phys. -Chim. Sin., 1998,14(10): 957-960
178. Li Yue-Qing, Deng Li-Zhi, Zhou Xiao-Hai, Zhang Shao-Hui, Yang Qing-Chuan.The Crystal Structure and the Second Harmonic Generation Efficiency of the Sulfosalicylate[J]. Acta Phys. -Chim. Sin., 1998,14(09): 778-783
179. Chen Xue-An,Zhao Ling,Li Yan,Chen Ben-Ming.Preparation and Crystal Structure of PbCuP2O7[J]. Acta Phys. -Chim. Sin., 1997,13(02): 113-118
180. Zhuang Hong-Hui,Wu Ding-Ming,Huang Jian-Quan,Huang Jin-Ling.Synthesis and Crystal Structure of [Cu4Cl4(TTTA)2][J]. Acta Phys. -Chim. Sin., 1996,12(08): 761-765
181. Cao Nai-Zhen,Shen Wan-Ci,Wen Shi-Zhu.The Characterization of the Porous Structure of Expanded Graphite[J]. Acta Phys. -Chim. Sin., 1996,12(08): 766-768
182. Lu Qing-Wei,Wang Yi-Bing,Suo Quan-Ling,Wu Bao-Shan,Sun Jie.Synthesis and Crystal Strucutre of Fe3(CO)8(C6H5NC)(μ3-S)2[J]. Acta Phys. -Chim. Sin., 1996,12(06): 532-536
183. Jin Xiang-Lin,Jiang Yi-Jia,Zhang Shi-Wei,Tang You-Qi.Synthesis and Crystal Structure of the Imidazale-bridged Dicopper(II) Complex with Tetraaza Macrocycles[J]. Acta Phys. -Chim. Sin., 1995,11(10): 932-936
184. Miao Fang-Ming, Liu Xiao-Lan, Chen Hong-Li, Cui Xue-Qi, Wang Hong-Gen, Wang Ru-Ji, Yao Xin-Kan.Synthesis and Structural Study of Bis(N-Phenylsalicylaldiminato)(1,10-Phenanthroline) Co(II)[J]. Acta Phys. -Chim. Sin., 1995,11(09): 824-827
185. Guo Jin-Liang,Sun Feng,Li Yong,Dong Chang-Xiong.Crystal Structure of Dichloro-(5,10,15,20-tetraphenylporphinato) phosphorus(V) Chloride Dichloromethane Solvate[J]. Acta Phys. -Chim. Sin., 1995,11(04): 360-364
186. Hou Yong-Kang, Gao Min, Li Li-Pu, Ma Zhi-Mei.Studies of Trail and Error Method for Cyrstal Structural Determinations(III) Application and Program System of SYSTEM 90[J]. Acta Phys. -Chim. Sin., 1994,10(12): 1087-1092
187. Wu Bing-Fang, Su Hai-Quan, Yan Xiu-Ying, Hu Xiang, Liu Shu-Tang, Liu Qi-Wang, Shi Jian-Qiu.Synthesis and Crystal Structure of Rh2(μ-SC6H5)2(CO)4[J]. Acta Phys. -Chim. Sin., 1994,10(09): 847-851
188. Zhang Bin, Wang Zhe-Min, Liu Shi-Xiong, Huang Jin-Ling.Synthesis and Crystal Structure of a New Metal-rich Layered Ternary Tantalum Telluride TaNi2Te2[J]. Acta Phys. -Chim. Sin., 1994,10(06): 508-513
189. Wang Zhe-Min, Guan Tie-Tang, Zhuang Hong-Hui.Crystal Structure of Soft X-Ray Analyzer Crystal——Octadecyl Hydrogen Maleate(OHM, C22H40O4)[J]. Acta Phys. -Chim. Sin., 1994,10(05): 413-417
190. Zheng Ji-Min, Che Yun-Xia, Wang Ru-Ji, Wang Hong-Gen.Crystal Structure of 1:1 Adduct of Glycine and m-nitrobenzoic Acid[J]. Acta Phys. -Chim. Sin., 1994,10(01): 64-68
191. Ma Jian-Fang; Wei Ge-Cheng; Ni Jia-Zuan.Syntheses and Crystal Structures of the Complexes of rare Earth with Fumaric Acid[J]. Acta Phys. -Chim. Sin., 1993,9(06): 752-759
192. Yang Qing-Chuan; Dai Sheng; Zhou Hong-Bing; Zhou Qi-Feng; Tang You-Qi.The Molecular and Crystal Structures and Thermal Properties of the Mesogenic 2,5-BIS(4-Ethylbenzoyl) Oxystyrene and 2,5-BIS(4-Methoxybenzoyl) Oxybenzaldehyde[J]. Acta Phys. -Chim. Sin., 1993,9(06): 795-801
193. Ye Dai-Qi; Liang Hong; Huang Zhong-Tao.Study on the Interaction Between the Active Phase and Support on V2O5/TiO2 Catalyst[J]. Acta Phys. -Chim. Sin., 1993,9(04): 501-508
194. Zhuang Hong-Hui; Wu Ding-Ming; Lu Can-Zhong; Tong Wen.Synthesis and Crystal Structure of (C5H7S2)2[Cu3I5][J]. Acta Phys. -Chim. Sin., 1993,9(04): 548-552
195. Wu Bing-Fang; Yan Xiu-Ying; Liu Qi-Wang; Liu Shu-Tang; Hu Xiang.Synthesis and Crystal Structure of Cluster (μ-SC6H5)(μ-P(SC6H5)2)Fe2(CO)6[J]. Acta Phys. -Chim. Sin., 1992,8(06): 749-752
196. Zeng Guang-Fu; Guo Xin; Wang Cui-Ying; Lin Yong-Hua; Li Han.Infrared Spectra and Crystal Structure of BIS-(Dimethoxylphosphato) Copper[J]. Acta Phys. -Chim. Sin., 1992,8(06): 778-782
197. Wang Zeng-Lin; Hu Ning-Hai; Niu Chun-Ji; Ni Jia-Zuan; Cui Ai-Li.Crystal Structure and Thermal Analysis of Erbium Complex with Benzene Acetic Acid[J]. Acta Phys. -Chim. Sin., 1992,8(05): 642-646
198. Du Shao-Bin; Wang Jin; Ma Fu-Tai; Zheng Hong-Yuan; Lou Hui; Jing Cheng-Heng.Correlation of Composition、Crystal Structure、Reducibility and Catalytic Oxidation Activity on La-Mn-Ni-O System[J]. Acta Phys. -Chim. Sin., 1992,8(05): 630-635
199. Fan Guang-Yu; Wang Huan-Zhong; Cui Xiu-Shan; Li Yun-Zheng; Zhu He-Sun.Crystal Structures of 1,2-Dimethyl-3-Indolmethyl-Idene Succinic Fulgide Anhydride and 1,2-Dimethyl-3-Indolylethylidene Succinic Fulgide Anhydride[J]. Acta Phys. -Chim. Sin., 1992,8(04): 545-549
200. Liu Yong-Sheng; Shu Ning-Cheng; Hu Ning-Hai.An Algebraic Method to Estimate General Type of Phases of Structure Factors[J]. Acta Phys. -Chim. Sin., 1992,8(02): 255-260
201. Liu Xiao-Lan; Sun Ming; Miao Fang-Ming; Li Yu-Gui; Wang Jian-Ji; Han Yu-Zhen; Xu Xiao-Jie.Crystal and Molecular Structure of 1-Oxo-4-(Substituent)-1-Phospha-2,6,7-Trioxacyclo(2,2,2) Octane[J]. Acta Phys. -Chim. Sin., 1992,8(01): 100-108
202. Huang Ming-Sheng; Zhang Peng; Zhang Ying; Yang Hua-Hui; Zheng Lan-Sun.Synthesisi and Structure of a new Polynuclear Silver Complex [Ag4(dppe)3(NO3)4][J]. Acta Phys. -Chim. Sin., 1991,7(06): 694-698
203. Jin Xiang-Lin; Tong You-Zhi; Xu Xiao-Jie; Tang You-Qi.The Synthesis and Crystal Structure of Thiocyanate-Bridged Bi-Copper(II) Macrocyclic Complex of 1,4,7,12,15,18-Hexaazacyclodocosane [Cu2(SCN)3(C16H38N6)]2(ClO4)2[J]. Acta Phys. -Chim. Sin., 1991,7(03): 323-328
204. Xin Min; Sun Xiao-Lin; Liu Qi-Wang; Hu Yu-Cai.The Crystal and Molecular Structure of β-Cyanoethyl-α-Ferrocenylhalogenbenzyl Ethers[J]. Acta Phys. -Chim. Sin., 1991,7(02): 136-139
205. Hu Sheng-Zhi; Chen Ming-Dan; Liu Xiao-Yun; Zhou Yuan-Lang.Crystal Structure and Molecular Mechanics Calculations of the Addition Product of Acetylacetone and Methyl 1-Naphthoate, C17H18O4[J]. Acta Phys. -Chim. Sin., 1991,7(02): 191-195
206. Hu Sheng-Zhi; Huang Ming-Sheng; Cheng Xian-En; Zhou Yuan-Lang.Crystal Structure and Molecular Mechanics Calculations of the Photodimerization Product of Acetylacetone, C10H16O4[J]. Acta Phys. -Chim. Sin., 1991,7(02): 196-201
207. Shangguan Guo-Qiang; Zhang Shu-Gong; Jin Zhong-Sheng; Liu Shu-Ying; Ni Jia-Zuan.Crystal and Molecular Structures and MS Analyse of β-Carboxylethyl (or α-methylethyl) Germanium Trichlorides[J]. Acta Phys. -Chim. Sin., 1991,7(02): 223-226
208. Yang Qing-Chuan; Li Yi-Li; Tang You-Qi; Fu Heng.Study on the Thermal Motion N-Phenylphthalimide and 2-Phenylquinoxaline in Solid State[J]. Acta Phys. -Chim. Sin., 1991,7(01): 77-81
209. LI Guang-Yong, WU Xiao-Han, HE Wei-Na, FANG Jian-Hui, ZHANG Xue-Tong.Controlled Assembly of the Graphene-based Aerogel[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
210. WANG Cheng-Xian, YU Fei, MA Jie.Applications of Graphene-based Hybrid Material as Electrodes in Microbial Fuel Cells[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
211. ZHU Jie-Jun, SUN Hai-Bin, WU Yao-Zheng, WAN Jian-Guo, WANG Guang-Hou.Graphene: Synthesis, Characterization and Application in Transparent Conductive Films[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
212. WANG Yun-Jing, LIU Ying-Qiu, GAO Xiu-Xiu, ZHAN Yan-Shan, PAN Li-Yang, ZHANG Wen-Kai, FANG Xiao-Min.Surface Defects Passivation of Graphene Quantum Dots by Amino Functionalization and its Photoluminescence Emission Enhancement[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
213. LIANG Jia-Xu, XIAO Zhi-Chang, ZHI Lin-Jie.Graphenal Polymers: 3D Carbon-rich Polymers as Energy Materials with both Electronic and Ionic Transport Path[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
214. XIA Kai-Lun, JIAN Mu-Qiang, ZHANG Ying-Ying.Advances in Flexible Conductors Based on Nanocarbon Materials[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
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