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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2011,Vol.27>> Issue(03)>> 620-626     doi: 10.3866/PKU.WHXB20110331         中文摘要
ELECTROCHEMISTRY AND NEW ENERGY
Preparation of Microporous Carbon Using a Zeolite HY Template and Its Capacitive Performance
LI Wen, ZHOU Jin, XING Wei, ZHUO Shu-Ping, Lü Yi-Min
School of Chemical Engineering, Shandong University of Technology, Zibo 255049, Shandong Province, P. R. China
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Several microporous carbons were prepared by polyfurfuryl alcohol-impregnation and impregnation-acetonitrile chemical vapor deposition (CVD) using zeolite HY as a template, denoted as PFA carbons and AN carbons, respectively. These were used as electrode materials for supercapacitors. X-ray diffraction (XRD) patterns show that the structural regularity of the zeolite was well-replicated by the carbon structures prepared by impregnation-CVD. X-ray photoelectron spectroscopy (XPS) confirmed that the AN carbons possess abundant nitrogen-containing groups because of the CVD of acetonitrile. The prepared carbons were typical microporous materials as determined by N2 adsorption/desorption test and they had a high BET surface area and narrow pore size distribution. Electrochemical tests showed that the AN carbons had higher capacitance because of their evident pseudo-capacitance from the nitrogen- containing groups. AN8 had a high capacitance up to 210 F·g-1. The capacitance retention ratio of the AN carbons were determined to its electric conductivity and mesoporosity.



Keywords: HY zeolite   Microporous carbon material   Chemical vapor deposition   Supercapacitor   Templating method  
Received: 2010-10-07 Accepted: 2010-12-16 Publication Date (Web): 2011-02-17
Corresponding Authors: ZHOU Jin, ZHUO Shu-Ping Email: zhuosp_academic@yahoo.com;zhoujin820514@163.com

Fund: The project was supported by the Outstanding Young Scientist Foundation of Shandong Province, China (BS2009NJ014) and Science and Technology Research Program of Shandong Province, China (2009GG10007006).

Cite this article: LI Wen, ZHOU Jin, XING Wei, ZHUO Shu-Ping, Lü Yi-Min. Preparation of Microporous Carbon Using a Zeolite HY Template and Its Capacitive Performance[J]. Acta Phys. -Chim. Sin., 2011,27 (03): 620-626.    doi: 10.3866/PKU.WHXB20110331

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