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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2011,Vol.27>> Issue(06)>> 1424-1430     doi: 10.3866/PKU.WHXB20110611         中文摘要
ELECTROCHEMISTRY AND NEW ENERGY
Preparation of Manganese Dioxide for Electrodes of Supercapacitors Based on Duplex Stainless Steel
LI Zhao, XU Ju-Liang, LI Xu-Yan, GUO Li-Fang, LI Jin, JIANG Yi-Ming
Department of Materials Science, Fudan University, Shanghai 200433, R. P. China
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A nano-structured manganese dioxide thin film was electrochemically deposited onto a 2304 duplex stainless steel (DSS) electrode. The structure, surface morphology, and composites of the obtained manganese dioxide were studied by X-ray diffraction (XRD), scanning electron microscopy (SEM), and X-ray energy dispersive spectroscopy (EDS), respectively. The electrochemical characteristics of the manganese dioxide electrodes were investigated by cyclic voltammetry (CV), chronopotentiometry, and electrochemical impedance spectroscopy (EIS). The obtained manganese dioxide was found to be amorphous and the surface was composed of nanorods with lengths between 100 and 200 nm. As the mass of the manganese dioxide increased the capacitance also increased while the specific capacitance decreased. With an increase in the CV scan rate the specific capacitance decreased as well. The highest specific capacitance value of 288.9 F·g-1 was obtained at a scan rate of 20 mV·s-1 when the mass of manganese dioxide was 0.09 mg. 500 cycles were carried out at a rate of 100 mV·s-1 and we found that the specific capacitance remained stable and even increased slightly as the cycles increased.



Keywords: Supercapacitor   MnO2   Electrodeposition   Specific capacitance   Electrode material  
Received: 2011-01-07 Accepted: 2011-04-06 Publication Date (Web): 2011-04-25
Corresponding Authors: JIANG Yi-Ming Email: corrosion@fudan.edu.cn

Fund: The project was supported by the Shanghai Natural Science Foundation, China (09ZR1402600), Shanghai Science and Technology Development Key Research Funds, China (09JC1401600), Shanghai High and New Technology′s Industrialization Project and FDUROP, China.

Cite this article: LI Zhao, XU Ju-Liang, LI Xu-Yan, GUO Li-Fang, LI Jin, JIANG Yi-Ming. Preparation of Manganese Dioxide for Electrodes of Supercapacitors Based on Duplex Stainless Steel[J]. Acta Phys. -Chim. Sin., 2011,27 (06): 1424-1430.    doi: 10.3866/PKU.WHXB20110611

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78. ZHANG Lei-Yong, HE Shui-Jian, CHEN Shui-Liang, GUO Qiao-Hui, HOU Hao-Qing.Preparation and Electrochemical Properties of Polyaniline/Carbon Nanofiber Composite Materials[J]. Acta Phys. -Chim. Sin., 2010,26(12): 3181-3186
79. ZHANG Fang, YUAN Chang-Zhou, ZHANG Xiao-Gang, ZHANG Luo-Jiang, XU Ke.5-Sulfosalicylic Acid-Assisted Hydrothermal Synthesis and Supercapacitive Properties of Co-Ni Layered Double Hydroxides[J]. Acta Phys. -Chim. Sin., 2010,26(12): 3175-3180
80. WANG Ming-Yong, WANG Zhi, GUO Zhan-Cheng.NiW Alloys Electrodeposited under Super Gravity Field and Their Anti-Corrosion Properties in Alkaline Solutions[J]. Acta Phys. -Chim. Sin., 2010,26(12): 3163-3168
81. WANG Dan-Li, RUAN Yong-Feng, ZHANG Ling-Cui, YANG Hong-Bo.Preparation by Electrodeposition and Characterization of ZnO Nanowire Arrays[J]. Acta Phys. -Chim. Sin., 2010,26(12): 3369-3372
82. ZHANG Xiao-Bo, CHEN Ming-Hai, ZHANG Xiao-Gang, LI Qing-Wen.Preparation of Porous Carbon Nanofibers by Electrospinning and Their Electrochemical Capacitive Behavior[J]. Acta Phys. -Chim. Sin., 2010,26(12): 3169-3174
83. WU Wei-Gang, YANG Fang-Zu, LUO Ming-Hui, TIAN Zhong-Qun, ZHOU Shao-Min.Electrodeposition of Copper in a Citrate Bath and Its Application to a Micro-Electro-Mechanical System[J]. Acta Phys. -Chim. Sin., 2010,26(10): 2625-2632
84. SONG Li-Jun, MENG Hui-Min.Electrodeposition of Nanocrystalline Nickel Alloys and Their Hydrogen Evolution in Seawater[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2375-2380
85. TIAN Ying, YAN Jing-Wang, LIU Xiao-Xue, XUE Rong, YI Bao-Lian.Electrochemical Capacitance of Composites with MnOx Loaded on the Surface of Activated Carbon Electrodes[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2151-2157
86. GUO Yuan-Yuan, WANG Ming, MAO Xiao-Bo, JIANG Yue-Xiu, WANG Chen, YANG Yan-Lian.Growth Mechanism for Controlled Synthesis of Metal Nanotube and Nanowire Arrays Using Anodic Aluminum Oxide Templates[J]. Acta Phys. -Chim. Sin., 2010,26(07): 2037-2043
87. LI Li-Min, LIU En-Hui, LI Jian, YANG Yan-Jing, SHEN Hai-Jie, HUANG Zheng-Zheng, XIANG Xiao-Xia.Polyaniline-Based Carbon for a Supercapacitor Electrode[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1521-1526
88. JI Qian-Qian, GUO Pei-Zhi, ZHAO Xiu-Song.Preparation of Chitosan-Based Porous Carbons and Their Application as Electrode Materials for Supercapacitors[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1254-1258
89. CHANG Yu-Qing, HUANG Ling, SUN Shi-Gang.Electrodeposition and Electrochemical Properties of Ternary Sn-Co-Zn Alloy Electrodes as Anodes for Lithium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2010,26(03): 561-566
90. LIANG Shan, XUE Qun-Ji, CUI Yu-Hong, ZHAO Zhan-Fen.Patterning of TiO2 Thin Films Prepared from Aqueous Solutions[J]. Acta Phys. -Chim. Sin., 2010,26(02): 502-506
91. ZANG Yang, HAO Xiao-Gang, WANG Zhong-De, ZHANG Zhong-Lin, LIU Shi-Bin.Copolymerization and Capacitive Performance of Composite Carbon Nanotubes/Polyaniline/Nickel Hexacyanoferrate Films[J]. Acta Phys. -Chim. Sin., 2010,26(02): 291-298
92. ZHOU Bao-Ping, YU Gang, OUYANG Yue-Jun, SI Wei-Wei, QIAO Li-Jie.Electrodeposition of Pd-Ag Alloy Nanoparticle Chains on Carbon Fibers and Their Hydrogen Sensing Properties[J]. Acta Phys. -Chim. Sin., 2010,26(01): 237-243
93. LI Juan, MO Xiao-Liang, SUN Da-Lin, CHEN Guo-Rong.Preparation of CuInS2 Thin Films by One-Step Electrodeposition[J]. Acta Phys. -Chim. Sin., 2009,25(12): 2445-2449
94. PANG Xu, MA Zheng-Qing, ZUO Lie.Sn Doped MnO2 Electrode Material for Supercapacitors[J]. Acta Phys. -Chim. Sin., 2009,25(12): 2433-2437
95. FU Qing-Bin, GAO Bo, SU Ling-Hao, YUAN Chang-Zhou, LU Xiang-Jun, ZHANG Xiao-Gang.Preparation of Polypyrrole/Benzenesulfonic Functionalized Multi-Walled Carbon Nanotubes Induced by Hydrogen Bonding and Their Electrochemical Behavior[J]. Acta Phys. -Chim. Sin., 2009,25(11): 2199-2204
96. SUN Zhe, LIU Kai-Yu, ZHANG Hai-Feng, LI Ao-Sheng, XU Xiao-Cun.Study on Meso-C/MnO2 Asymmetric Supercapacitors[J]. Acta Phys. -Chim. Sin., 2009,25(10): 1991-1997
97. WANG Yan-Kun, ZHANG Jian-Min, LAN Meng.Temperature Effects on ZnO Film Electrodeposition[J]. Acta Phys. -Chim. Sin., 2009,25(10): 1998-2004
98. CAO Yin-Liang, WANG Feng, LIU Jing-Jun, WANG Jian-Jun, ZHANG Liang-Hu, QIN Shi-Yong.Electrochemical Preparation and Electrocatalytic Mechanisms of Ni-S Active Cathode for Hydrogen Evolution[J]. Acta Phys. -Chim. Sin., 2009,25(10): 1979-1984
99. JIANG Dong-Dong, FU Yan-Bao, MA Xiao-Hua.Fabrication and Characterization of Tin Nanorod Electrodes for Lithium Ion Rechargeable Batteries[J]. Acta Phys. -Chim. Sin., 2009,25(08): 1481-1484
100. WANG Ming-Yong, WANG Zhi, GUO Zhan-Cheng.Regularity and Mechanism of Pb Electrodeposition Intensified by Super Gravity Field[J]. Acta Phys. -Chim. Sin., 2009,25(05): 883-889
101. YANG Fang-Zu, HUANG Ling, XU Shu-Kai, ZHOU Shao-Min.Preparation, Heat Treatment and Corrosion Behavior of Amorphous Ni-W/ZrO2 Composite Coating[J]. Acta Phys. -Chim. Sin., 2009,25(05): 864-868
102. YANG Hong-Yan, GUO Pan-Pan, LI Wei-Shan.Electrodeposition Preparation and Activity of CO-Resistant Catalyst Pt-HxWO3 for Methanol Oxidation[J]. Acta Phys. -Chim. Sin., 2009,25(04): 719-723
103. LI Ning, GAO Cheng-Hui, YANG Su-Zhen.Crystallization Kinetics of Electrodeposited Amorphous/Nanocrystalline Ni81.32Mo18.68 Alloy Coating[J]. Acta Phys. -Chim. Sin., 2009,25(04): 735-740
104. JIANG Qi, ZHAO Xiao-Feng, HUANG Bin, DU Bing, ZHAO Yong.Effect of the Activated Carbon Reactivation on Its Electrochemical Capacitance[J]. Acta Phys. -Chim. Sin., 2009,25(04): 757-761
105. DU Bing, JIANG Qi, ZHAO Xiao-Feng, LIN Sun-Zhong, MU Pei-Shan, ZHAO Yong.Preparation of PPy/CNTs Composite Based on the Electrostatic Absorption Effect[J]. Acta Phys. -Chim. Sin., 2009,25(03): 513-518
106. CHEN Li; ZHANG Xiao-Gang; YUAN Chang-Zhou; CHEN Sheng-Yao.Electrochemical Properties of Poly(3,4-ethylenedioxythiophene)/Manganese Oxide Synthesized by Interfacial Polymerization[J]. Acta Phys. -Chim. Sin., 2009,25(02): 304-308
107. GAO Qiang; LIU Ya-Fei; HU Zhong-Hua; ZHENG Xiang-Wei; WEN Zu-Biao.Electrochemical Properties of Manganese Oxide Surface-Modified Activated Carbon Electrode Materials[J]. Acta Phys. -Chim. Sin., 2009,25(02): 229-236
108. WANG Tao, HE Jian-Ping, ZHANG Chuan-Xiang, ZHOU Jian-Hua, GUO Yun-Xia, CHEN Xiu, DI Zhi-Yong, SUN Dun, WANG Dao-Jun.Preparation and Electrochemical Properties of Ordered Mesoporous C/NiO Composites[J]. Acta Phys. -Chim. Sin., 2008,24(12): 2314-2320
109. YANG Pei-Xia; AN Mao-Zhong; SU Cai-Na; WANG Fu-Ping.Electrodeposition Behaviors of Pure Cobalt in Ionic Liquid[J]. Acta Phys. -Chim. Sin., 2008,24(11): 2032-2036
110. JIANG Qi; ZHANG Qian; DU Bing; ZHAO Xiao-Feng; ZHAO Yong.Preparation and Electrochemical Properties of CNTs-PANI Composite Material via Finite Field Polymerization[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1719-1723
111. LIU Ya-Fei; HU Zhong-Hua; XU Kun; ZHENG Xiang-Wei; GAO Qiang.Surface Modification and Performance of Activated Carbon Electrode Material[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1143-1148
112. SHI Yan-Hua; MENG Hui-Min; SUN Dong-Bai; YU Hong-Ying; FU Hua-Rong.Manganese Oxide Coating Electrodes Prepared by Pulse Anodic Electrodeposition[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1199-1206
113. GAO Li-Xia; WANG Li-Na; QI Tao; LI Yu-Ping; CHU Jing-Long; QU Jing-Kui.Electrodeposition of Aluminium from AlCl3/Et3NHCl Ionic Liquids[J]. Acta Phys. -Chim. Sin., 2008,24(06): 939-944
114. AO Jian-Ping; SUN Guo-Zhong; YAN Li; KANG Feng; YANG Liang; HE Qing; ZHOU Zhi-Qiang; LI Feng-Yan; SUN Yun.Properties of One-Step Electrodeposited Cu(In1-x, Gax)Se2 Thin Films[J]. Acta Phys. -Chim. Sin., 2008,24(06): 1073-1079
115. ZENG Wen-Wen; HUANG Ke-Long; YANG You-Ping; LIU Su-Qin; LIU Ren-Sheng.Solvothermal Synthesis and Capacitance Performance of Co3O4 with Different Morphologies[J]. Acta Phys. -Chim. Sin., 2008,24(02): 263-268
116. YANG Jing; LIU Ya-Fei; CHEN Xiao-Mei; HU Zhong-Hua; ZHAO Guo-Hua.Carbon Electrode Material with High Densities of Energy and Power[J]. Acta Phys. -Chim. Sin., 2008,24(01): 13-19
117. YU Jun-Sheng; SUO Fan; LI Wei-Zhi; LIN Hui; LI Lu; JIANG Ya-Dong.Influence of Electrode Materials on the Performance of NPB/Alq3 Organic Electroluminescent Devices[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1821-1826
118. MA Xu; YAO Su-Wei; ZHANG Wei-Guo; WANG Hong-Zhi.Structure and Corrosion Behavior of Electrodeposited Fe-W-ZrO2 Nano-composite Coatings[J]. Acta Phys. -Chim. Sin., 2007,23(10): 1617-1621
119. YANG Jian-Jun; HUANG Jun-Jie; JIANG Zhi-Yu.Supercapacitance of MnO2 Thin Film Electrodes Prepared Using Jet Printing Method[J]. Acta Phys. -Chim. Sin., 2007,23(09): 1365-1369
120. WANG Jie; XU You-Long; SUN Xiao-Fei; XIAO Fang; MAO Sheng-Chun.Capacitance Properties of Porous Polypyrrole Thick Films Prepared Electrochemically by Multi-step Polymerization[J]. Acta Phys. -Chim. Sin., 2007,23(06): 877-882
121. ZENG Wei; ZHOU Hai-Hui; YING Xiao-Fang; ZENG Qing-Liang; HU Wei-Ya; KUANG Ya-Fei.Electrodeposition of Gold Nanoparticles Coatings from Electrode/ReverseMicroemulsion System[J]. Acta Phys. -Chim. Sin., 2007,23(05): 769-773
122. LIU Yong; WEI Zi-Dong; CHEN Si-Guo; FENG Yong-Chao; YIN Guang-Zhi; SUN Cai-Xin.PEMFC Electrodes Platinized by Modulated Pulse Current Electrodeposition[J]. Acta Phys. -Chim. Sin., 2007,23(04): 521-525
123. YAO Su-Wei; JIANG Ying; ZHANG Wei-Guo.Electrochemical Preparation and Giant Magnetoresistance Effect of Spin-valve Multilayers[J]. Acta Phys. -Chim. Sin., 2007,23(04): 493-498
124. MA Liang; MA Jie; LIU Hui.Composite Electrodeposition of CoNiP-BaFe12O19Magnetic Thin Film[J]. Acta Phys. -Chim. Sin., 2007,23(04): 590-594
125. WANG Jie;XU You-Long;CHEN Xi;DU Xian-Feng;LI Xi-Fei.Effect of Doping Ions on Electrochemical Capacitance Properties of Polypyrrole Films[J]. Acta Phys. -Chim. Sin., 2007,23(03): 299-304
126. HUANG Ling;JIANG Hong-Hong;KE Fu-Sheng;FAN Xiao-Yong;ZHUANG Quan-Chao;YANG Fang-Zu;SUN Shi-Gang.Structure and Properties of Three-dimensional Reticular Sn-Co Alloy Electrodes as Anode Material for Lithium Batteries[J]. Acta Phys. -Chim. Sin., 2006,22(12): 1537-1541
127. PENG Xie-Lan;XIE Qing-Ji;KANG Qing;YAO Shou-Zhuo .EQCM Study on the Electrodeposition of Hydroxides in Hydrated Perchlorate + Organic Solvent Systems[J]. Acta Phys. -Chim. Sin., 2006,22(11): 1361-1366
128. BAI Shuo;YANG Ling-Lu;ZHANG Mao-Feng;YANG Zhao-Hui;ZHANG Zhi-Feng;CAO Wei-Xiao.Patterned Ag Film with Superhydrophobic Properties[J]. Acta Phys. -Chim. Sin., 2006,22(10): 1296-1299
129. ZHANG Wei-guo;LI Wei-Xiang;ZHANG Lu;YAO Su-Wei .Electrodeposition of Cu/Ni Multilayered Nanowires Ordered Arrays by Dual Bath Technique[J]. Acta Phys. -Chim. Sin., 2006,22(08): 977-980
130. GU Min; XIAN Xiao-Hong.The Preparation of Copper Electrodeposits with (110) Lattice Plane Fully Preferred Orientation[J]. Acta Phys. -Chim. Sin., 2006,22(03): 378-382
131. YAO Su-wei; WU Hai-xia; WANG Hong-zhi; ZHANG Wei-guo.Electrodeposition of Cu-Co Granular Films on Semiconductor Si Substrate and Their GMR Effect[J]. Acta Phys. -Chim. Sin., 2005,21(08): 915-919
132. LI Hua; XU Cai-ling; ZHAO Guang-yu; LI Hu-lin.Preparation and Magnetic Properties of Amorphous Co-Pt Alloy Nanowire Arrays[J]. Acta Phys. -Chim. Sin., 2005,21(06): 641-645
133. CHEN Zhi-gang; TANG Yi-wen; ZHANG Li-sha; CHEN Zheng-hua; JIA Zhi-jie.Electrochemical Deposition and Characterization of Zinc Oxide Thin Films[J]. Acta Phys. -Chim. Sin., 2005,21(06): 612-615
134. FENG Shao-bin; SHANG Shi-bo; BAO Xiang; FENG Li-ting; ZHANG Jing-wei; LI Zong-hui.Study of Potential Activation Phenomenon and Initial Process of the Metal Electrodeposition[J]. Acta Phys. -Chim. Sin., 2005,21(05): 463-467
135. XIAO Xue-Zhang; CHEN Chang-Pin; WANG Xin-Hua; CHEN Li-Xin; WANG Li; GAO Lin-Hui.Microstructure and Electrochemical Properties of Amorphous Mg-Fe-Ni Hydrogen Storage Electrode Material[J]. Acta Phys. -Chim. Sin., 2005,21(05): 565-568
136. YANG Hong-Sheng; ZHOU Xiao; ZHANG Qing-Wu.Electrochemical Performances of Supercapacitor with Polyaniline Particles with Hierarchy as Active Electrode Material[J]. Acta Phys. -Chim. Sin., 2005,21(04): 414-418
137. Yang Fang-Zu;Ma Zhao-Hai;Huang Ling;Xu Shu-Kai;Zhou Shao-Min.Electrodeposition, Structure and Properties of an Amorphous Ni-W-B/ZrO2 Composite Coating[J]. Acta Phys. -Chim. Sin., 2004,20(12): 1411-1416
138. Chen Hong;Chen Jin-Song;Zhou Hai-Hui;Jiao Shu-Qiang;Chen Jin-Hua;Kuang Ya-Fei.The Application of Nano-fibrous Polyaniline in Electrochemical Capacitor[J]. Acta Phys. -Chim. Sin., 2004,20(06): 593-597
139. Yang Fang-Zu;Huang Ling;Xu Shu-Kai;Zhou Shao-Min.Studies on the Electrodeposition Behaviors of Palladium by the Actions of Additive[J]. Acta Phys. -Chim. Sin., 2004,20(05): 463-467
140. Su Yu-Zhi;Guo Shi-Heng;Xiao Yi-Zhi;Xiao Min;Yang Qi-Qin.Electrode Kinetics of 2,2’-diaminophenyloxydisulfide[J]. Acta Phys. -Chim. Sin., 2004,20(05): 518-523
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142. Liu Xian-Ming;Zhang Yi-He;Zhang Xiao-Gang;Fu Shao-Yun.The Supercapacitive Properties of Ni-Ru Oxide Composites[J]. Acta Phys. -Chim. Sin., 2004,20(04): 417-420
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144. Jia Chong;Jin Chuan-Gui;Liu Wei-Feng;Cai Wei-Li;Yao Lian-Zeng;Li Xiao-Guang.Fabrication of Sb Single-crystal Nanowire Arrays[J]. Acta Phys. -Chim. Sin., 2004,20(03): 240-243
145. Zhou Hai-Hui;Jiao Shu-Qiang;Chen Jin-Hua;Wei Wan-Zhi;Kuang Ya-Fei.Electrocatalytic Oxidation of Methanol on Nano-fibular Polyaniline Electrode Modified with Pt Microparticles[J]. Acta Phys. -Chim. Sin., 2004,20(01): 9-14
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147. Zhuang Xin-Guo;Yang Yu-Sheng;Ji You-Ju;Yang Dong-Ping;Tang Zhi-Yuan.The Influence of Porous Structure of Activated Carbons Used as Supercapacitor Electrode Materials on Its Properties[J]. Acta Phys. -Chim. Sin., 2003,19(08): 689-694
148. Li Gao-Ren;Tong Ye-Xiang;Liu Guan-Kun.Study on Electrodeposition of Er-Bi Alloy Films in Organic Bath[J]. Acta Phys. -Chim. Sin., 2003,19(07): 630-634
149. Wang Xiao-Feng;Wang Da-Zhi;Liang Ji.Carbon Nanotube Capacitor Materials Loaded with Different Amounts of Ruthenium Oxide[J]. Acta Phys. -Chim. Sin., 2003,19(06): 509-513
150. Zhang Bao-Hong;Zhang Na.Research on Nanophase MnO2 for Electrochemical Supercapacitor[J]. Acta Phys. -Chim. Sin., 2003,19(03): 286-288
151. Xu Jin-Xia;Huang Xin-Min;Qian Li-Hua.Structure and Properties of Ni-Al2O3 Nanochannel Array System by Direct Current Electro-deposition[J]. Acta Phys. -Chim. Sin., 2003,19(03): 265-267
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153. Gu Min;Yang Fang-Zu;Huang Ling;Yao Shi-Bing;Zhou Shao-Min.The Formation of Copper Electrodeposits with Highly Preferred Orientation and Their Surface Morphology[J]. Acta Phys. -Chim. Sin., 2002,18(11): 973-978
154. Wang Hong-Zhi;Yao Su-Wei;Xing Dong-Mei;Zhang Wei-Guo.Preparation, Characterization and the Study of the Thermal Strain of Ni-W Gradient Deposits with Nanostructure[J]. Acta Phys. -Chim. Sin., 2002,18(11): 1029-1032
155. Yao Su-Wei;Chi Guang-Jun;Cui Lan;Fan Jun;Zhang Wei-Guo;Wang Hong-Zhi.Preparation and Characterization of Fe Nanowire Arrays in Porous Anodic Aluminum[J]. Acta Phys. -Chim. Sin., 2002,18(10): 930-933
156. Wang Jian-Chao;He Feng-Rong;Liu Guan-Kun;Tong Ye-Xiang.Electrochemical Preparation of Y-Mg-Co Alloy Film from Dimethylformamide Bath[J]. Acta Phys. -Chim. Sin., 2002,18(08): 732-736
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158. Huang Ling;Zhang Rui;Gu Min;Yang Fang-Zu;Xu Shu-Kai;Zhou Shao-Min.Effects of Nicotinic Acid on Copper Electrodeposition in Acid Sulphate[J]. Acta Phys. -Chim. Sin., 2002,18(07): 665-668
159. Chi Guang-Jun;Yao Su-Wei;Fan Jun;Zhang Wei-Guo;Wang Hong-Zhi.Electrochemically Assembled Silver Nanowire Arrays and Its Structural Characterization[J]. Acta Phys. -Chim. Sin., 2002,18(06): 532-535
160. Zhao Li-Li;Wang Rong-Shu;Niu Wen-Tai;Li Xiang.Synthesis of γ-MnO2 Nano Powder Used for SieveMembrane Reactor[J]. Acta Phys. -Chim. Sin., 2002,18(03): 197-200
161. Dong Jun;Shi Hong-Yun;Deng Jie;Zhang Yun-Qian.Preparation of Amerphous Alloys of Nickel with Lanthanum,Cerium by Electrodeposition and Crystallization Kinetics[J]. Acta Phys. -Chim. Sin., 2001,17(11): 1053-1056
162. Zhang Li;Ren Yan-Jie;Cai Sheng-Min.Photoelectrochromism of Dyesensitized Nanoporous TiO2 Film Combined with Electrodeposited MoO3 Film[J]. Acta Phys. -Chim. Sin., 2001,17(09): 817-819
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