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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2012,Vol.28>> Issue(02)>> 450-456     doi: 10.3866/PKU.WHXB201112141         中文摘要
CATALYSIS AND SURFACE SCIENCE
Hydrogen Evolution by Photocatalytic Steam Reforming of Methane over Pt/TiO2
LI Cao-Long1,2, CHEN Wei1, YUAN Jian1, SHANGGUAN Wen-Feng1
1. Research Center for Combustion and Environment Technology, Shanghai Jiao Tong University, Shanghai 200240, P. R. China;
2. Department of Inorganic Chemistry of Basic Courses, China Pharmaceutical University, Nanjing 211169, P. R. China
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Photocatalytic reaction of CH4 gas with H2O vapor over Pt/TiO2 at around room temperature (ca 323 K) was examined in a flow reactor. H2 and CO2 were the main products, and only trace amounts of C2H6, C2H4, and CO were observed. After an induction period, the molar ratio of H2 to CO2 in the outlet gas became close to 1.7. Thus, the main reaction is suggested to be: CH4+2H2O(g)→4H2+CO2, which can be referred to as photocatalytic steam reforming of methane (PSRM). The reaction would be promoted by photoexcited electrons and holes, which were generated by band gap photoexcitation of the TiO2 photocatalyst. In addition, the effects of reaction parameters, such as molar ratio of CH4 to H2O, total flow rate, noble-metal cocatalysts, wavelength of irradiating light, amounts of catalysts, and recycling efficiency of the p-Pt/TiO2 photocatalyst via light deposition of preformed Pt nanoparticles on P25, on the hydrogen evolution were investigated.

Keywords: Photocatalytic reforming   Hydrogen   CH4   Steam   TiO2  
Received: 2011-08-05 Accepted: 2011-12-06 Publication Date (Web): 2011-12-14
Corresponding Authors: SHANGGUAN Wen-Feng Email: shangguan@sjtu.edu.cn

Fund: The project was supported by the National Natural Science Foundation of China (20973110) and National Key Basic Research Program of China (973) (2009CB220000).

Cite this article: LI Cao-Long, CHEN Wei, YUAN Jian, SHANGGUAN Wen-Feng. Hydrogen Evolution by Photocatalytic Steam Reforming of Methane over Pt/TiO2[J]. Acta Phys. -Chim. Sin., 2012,28 (02): 450-456.    doi: 10.3866/PKU.WHXB201112141
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79. ZHANG Sheng-Han, LIANG Ke-Xin, TAN Yu.Preparation of TiO2 Nanotube Arrays with Different Cerium Mixing Morphology and Their Photoelectrochemical Response in Visible Light[J]. Acta Phys. -Chim. Sin., 2011,27(11): 2726-2732
80. ZHAO Liu-Jie, RAN Jing-Yu, WU Sheng.Thermodynamic Study of the Humidity Ratio for Methane Reforming at Low Temperature in a Micro-Combustor[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2027-2034
81. YUAN Wen-Hui, LI Bao-Qing, LI Li.Superior Graphene for Hydrogen Adsorption Prepared by the Improved Liquid Oxidation-Reduction Method[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2244-2250
82. LI Di, CHEN Hong-Chong, LI Jin-Hua, ZHOU Bao-Xue, CAI Wei-Min.Photoelectrocatalytic Performance and Reaction Mechanism of Different Organics upon Adsorption on a TiO2 Nanotube Array Electrode[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2153-2159
83. PENG Xuan, ZHANG Qin-Xue, CHENG Xuan, CAO Da-Peng.Adsorption and Separation of CO2/CH4/N2 Binary Mixtures in an Ordered Mesoporous Carbon Material CMK-3[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2065-2071
84. LU Sheng-Yong, HUANG Yi-Long, WANG Qiu-Lin, LI Xiao-Dong, YAN Jian-Hua.Photocatalytic Degradation of Gaseous 1,2-Dichlorobenzene over TiO2/AC Photocatalysts[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2191-2199
85. LI Xue-Fei, ZHAO Yun, JIAO Qing-Ze, LI Han-Sheng, WU Hong-Yu, LIU Hong-Bo, CUI Wen-Jia.Preparation of One-Dimensional Titanate Nanomaterials Using Different Titania Sources[J]. Acta Phys. -Chim. Sin., 2011,27(08): 1996-2000
86. XIA Wen-Sheng, CHANG Gang, HOU Yu-Hui, WENG Wei-Zheng, WAN Hui-Lin.Influence of Ni Chemical States on the Partial Oxidation Mechanism of Methane: An Energetics Analysis[J]. Acta Phys. -Chim. Sin., 2011,27(07): 1567-1573
87. LIANG Jian-Ming, ZHANG Ri-Guang, ZHAO Qiang, DONG Jin-Xiang, WANG Bao-Jun, LI Jin-Ping.Hydrogen Adsorption on Zeolite Na-MAZ and Li-MAZ Clusters[J]. Acta Phys. -Chim. Sin., 2011,27(07): 1647-1653
88. ZHAO Xing, ZHUANG Quan-Chao, QIU Xiang-Yun, XU Shou-Dong, SHI Yue-Li, CUI Yong-Li.Electrochemical Performance of Cr2O3/TiO2 Composite Material for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2011,27(07): 1666-1672
89. QIU Wei, REN Cheng-Jun, GONG Mao-Chu, HOU Yun-Ze, CHEN Yao-Qiang.Structure, Surface Properties and Photocatalytic Activity of TiO2 and TiO2/SiO2 Catalysts Prepared at Different pH Values[J]. Acta Phys. -Chim. Sin., 2011,27(06): 1487-1492
90. YUN Hong, LIN Chang-Jian, DU Rong-Gui.Anticorrosion Properties of Nano Anatase TiO2 Films Derived from Sol-Gel and Hydrothermal Crystallization[J]. Acta Phys. -Chim. Sin., 2011,27(05): 1122-1127
91. ZHANG Hui-Min, HU Rui-Sheng, HU Jia-Nan, ZHANG Yu-Long.Preparation and Catalytic Activities of La2CoAlO6 for Methane Combustion[J]. Acta Phys. -Chim. Sin., 2011,27(05): 1169-1175
92. SU Ya-Ling, LI Yi, DU Ying-Xun, LEI Le-Cheng.Visible-Light-Driven Catalytic Properties and First-Principles Study of Fluorine-Doped TiO2 Nanotubes[J]. Acta Phys. -Chim. Sin., 2011,27(04): 939-945
93. SONG Lei, YU Feng, WU Li-Xia, ZHOU Xiao-Guo, LIU Shi-Lin.Anionic Production Pathways Involved in the Reaction between OH- and CH2ClF[J]. Acta Phys. -Chim. Sin., 2011,27(04): 801-807
94. CHEN Dong-Po, ZHANG Xiao-Dan, WEI Chang-Chun, LIU Cai-Chi, ZHAO Ying.Effect of Blocking Layers Prepared by the Hydrolysis of TiCl4 Solution on the Photovoltaic Performance of a Dye-Sensitized Solar Cell[J]. Acta Phys. -Chim. Sin., 2011,27(02): 425-431
95. LUO Ying, CUI Xiao-Li, XIE Jing-Ying.Preparation and Visible Light Photoelectrochemical Response of TiO2-MoO3 Composite Nanotube Thin Films[J]. Acta Phys. -Chim. Sin., 2011,27(01): 135-142
96. CHEN Hua-Rong, CHANG Ran-Ran, LI Li, YUAN Wen-Hui.High Performance NaA Zeolite Membrane for Hydrogen Separation Synthesized on an Organic-Functionalized α-Al2O3 Ceramic Hollow Fiber Surface[J]. Acta Phys. -Chim. Sin., 2011,27(01): 241-247
97. ZHANG Zhi-Yu, SANG Li-Xia, SUN Biao, ZHANG Xiao-Min, MA Chong-Fang.Kinetics and Electrochemical Impedance Properties of TiO2 Nanotube Array Photoelectrode[J]. Acta Phys. -Chim. Sin., 2010,26(11): 2935-2940
98. ZHANG Xiao-Ru, LIN Yan-Hong, ZHANG Jian-Fu, HE Dong-Qing, WANG De-Jun.Photoinduced Charge Carrier Properties and Photocatalytic Activity of N-Doped TiO2 Nanocatalysts[J]. Acta Phys. -Chim. Sin., 2010,26(10): 2733-2738
99. WU Li-Xia, YU Feng, LIU Jing, DAI Jing-Hua, ZHOU Xiao-Guo, LIU Shi-Lin.Ab initioMolecular Dynamics Investigation on the Production Channels for the Reaction of O- with CH3F[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2331-2336
100. ZHU Yan-Feng, DU Rong-Gui, LI Jing, QI Hai-Qing, LIN Chang-Jian.Photogenerated Cathodic Protection Properties of a TiO2 Nanowire FilmPrepared by a Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2349-2353
101. CHAO Wen-Liu, WAN Yong, WANG Yun-Xia, LIU Chang-Song.Tribological Properties of Cu-Doped TiO2 Films[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2317-2322
102. HUANG Yong-Xia, LAI Yue-Kun, LIN, Long-Xiang, SUN Lan, LIN Chang-Jian.Electrochemical Construction and Biological Performance of Micropatterned CaP Films[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2057-2060
103. WANG Luo-Xin, XU Jie, ZOU Han-Tao, YI Chang-Hai.Effect of Chirality and Size on the Thermal Decomposition of Nitromethane Confined inside Single-Walled Carbon Nanotube[J]. Acta Phys. -Chim. Sin., 2010,26(03): 721-726
104. LEI Ze, ZHU Qing-Shan, HAN Min-Fang.Fabrication and Performance of Direct Methane SOFC with a Cu-CeO2-Based Anode[J]. Acta Phys. -Chim. Sin., 2010,26(03): 583-588
105. MA Chun-An, LIU Ting, CHEN Li-Tao.CO and H Adsorption on Pt/WC(0001) Surface[J]. Acta Phys. -Chim. Sin., 2010,26(01): 155-162
106. BAI Mei-Gui, TAO Xu-Mei, WU Qing-You, HUANG Zhi-Jun, LI Yu-Liang, YIN Yong-Xiang, DAI Xiao-Yan.Effect of Different Feeding Modes on CO2 Reforming of CH4 by Thermal Plasma[J]. Acta Phys. -Chim. Sin., 2009,25(12): 2455-2460
107. LI Mei-Fen, ZENG Fan-Gui, SUN Bei-Lei, QI Fu-Hui.Evolution Kinetics of Hydrogen Generation from Low Rank Coal Pyrolysis and Its Relation to the First Coalification Jump[J]. Acta Phys. -Chim. Sin., 2009,25(12): 2597-2603
108. DU Xiao-Ming, WU Er-Dong.Modeling the Supercritical Adsorption of Hydrogen on A-and X-Type Zeolites with a Lattice Density Function[J]. Acta Phys. -Chim. Sin., 2009,25(09): 1823-1828
109. ZHANG Chang-Hua, ZHANG Yan, ZHANG Song, ZHANG Bing.Photodissociation Dynamics of Chloroiodomethane in the A-Band[J]. Acta Phys. -Chim. Sin., 2009,25(08): 1708-1712
110. ZENG Fan-Gui, JIA Jian-Bo.Reaction Types and Kinetics of Methane Generation from Huolinhe Lignite Pyrolysis by TG/MS Experiment and Quantum Chemical Calculations[J]. Acta Phys. -Chim. Sin., 2009,25(06): 1117-1124
111. CHEN Wei, DONG Xin-Fa, CHEN Zhi-Shan, CHEN Sheng-Zhou, LIN Wei-Ming.Effect of Fe3+ Doping on Photocatalytic Activity of K2La2Ti3O10 for Water Decomposition to Hydrogen under Visible Light[J]. Acta Phys. -Chim. Sin., 2009,25(06): 1107-1110
112. DU Xiao-Ming, WU Er-Dong.Behavior of Adsorbed Hydrogen Molecules on Zeolites[J]. Acta Phys. -Chim. Sin., 2009,25(03): 549-554
113. WAN Li-Hua, YA Ke-Feng, LI Xiao-Sen, FAN Shuan-Shi.Molecular Dynamics Simulation of Methane Hydrate Dissociation Process in the Presence of Thermodynamic Inhibitor[J]. Acta Phys. -Chim. Sin., 2009,25(03): 486-494
114. XU Jun-Ke; LI Zhao-Jing; WANG Ji-Hui; ZHOU Wei; MA Jian-Xin.Characterization and Analysis of Carbon Deposited on the Surface of Ni/Al2O3 Catalyst for Methane Dry Reforming[J]. Acta Phys. -Chim. Sin., 2009,25(02): 253-260
115. CHEN Shan-Jun; DAI Wei; LUO Jiang-Shan; TANG Yong-Jian; WANG Chao-Yang; SUN Wei-Guo.Simulation of Methane Adsorption in AFS Molecular Sieves[J]. Acta Phys. -Chim. Sin., 2009,25(02): 285-290
116. ZHANG Nuo-Wei, HUANG Chuan-Jing, KUANG Fei-Ping, GAO Xiao-Xiao, WENG Wei-Zheng, WAN Hui-Lin.Effect of a Mg Promoter on the Structure and Catalytic Performance of a Co/Mg/HZSM-5 Catalyst for the Partial Oxidation of Methane to Syngas[J]. Acta Phys. -Chim. Sin., 2008,24(12): 2165-2171
117. XIAO Li-Hua, SUN Kun-Peng, XU Xian-Lun.Catalytic Combustion of Methane over CeO2-MOx (M=La3+, Ca2+) Solid Solution Promoted Pd/γ-Al2O3 Catalysts[J]. Acta Phys. -Chim. Sin., 2008,24(11): 2108-2113
118. ZENG Yu-Yao; ZHANG Bing-Jian.Designed Metal-Organic Frameworks Based on MOF-5 and Their Methane Adsorption Calculation by Grand Canonical Monte
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119. WANG Bin-Bin; QIU Rong; JIANG Yong.Effects of Hydrogen Enhancement in LPG/Air Premixed Flame[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1137-1142
120. GUO Liang; WU Zhan-Song.Mechanism of Methane’s Adsorption on Nanometer Active Carbon at Supercritical State[J]. Acta Phys. -Chim. Sin., 2008,24(05): 737-742
121. GENG Chun-Yu; DING Li-Ying; HAN Qing-Zhen; WEN Hao.Influence of Gas Molecule on Stability of Methane Hydrate[J]. Acta Phys. -Chim. Sin., 2008,24(04): 595-600
122. REN Xiu-Bin; LI Huan-Ying; GUO Xiang-Yun.Oscillatory Behavior during the Partial Oxidation of Methane[J]. Acta Phys. -Chim. Sin., 2008,24(02): 197-200
123. ZHANG Ya-Yuan; JIANG Zheng; ZHANG Shi-Chao; ZHU Qing-Shan.Catalytic Performance of La0.8Sr0.2FeMn1.5Al9.5O19-δ Hexaaluminate-typed Aerosol Catalysts[J]. Acta Phys. -Chim. Sin., 2008,24(02): 211-216
124. MA Chun-An; WANG Xiao-Juan; LI Guo-Hua; LI Mei-Chao; CHEN Song.Electroreduction Characteristics of Nitromethane in Ionic Liquid BMImBF4[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1719-1722
125. JIANG Yong; CHU Wei; JIANG Cheng-Fa; WANG Yao-Hong.A DFT Study of Pdn(n=1-7) Clusters and Their Interactions with CH4 Molecule[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1723-1727
126. SHEN Jian-Dong; ZHANG Shi-Cheng; LIAN Jin-Jun; KONG Ling-Dong; CHEN Jian-Min.Benz[a]anthracene Heterogeneous Photochemical Reaction on the Surface of TiO2 Particles[J]. Acta Phys. -Chim. Sin., 2007,23(10): 1531-1536
127. SUN Lan; ZUO Juan; LAI Yue-Kun; NIE Cha-Geng; LIN Chang-Jian.Electrical Transport Properties of Individual TiO2 Nanowire in One Dimension[J]. Acta Phys. -Chim. Sin., 2007,23(10): 1603-1606
128. YUE Qiao-Hong; SHAO Xiao-Hong; CAO Da-Peng.Separation of Hydrogen and Carbon Dioxide in Activated Mesocarbon Microbeads with High Specific Surface[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1080-1084
129. DU Xiao-Ming; WU Er-Dong.Application of the Adsorption Potential Theory to Hydrogen Adsorption on Zeolites above Critical Temperature[J]. Acta Phys. -Chim. Sin., 2007,23(06): 813-819
130. ZHANG Xiao-Fei; HU Rui-Sheng; GAO Guan-Jun; MENG He; SU Hai-Quan.Influence of Two Complexants on Structure and Performance of Ce-Sn-O Complex Oxides[J]. Acta Phys. -Chim. Sin., 2007,23(05): 659-663
131. FANG Shu-Mei; OU Yan; LIN Jing-Dong; LIAO Dai-Wei.Preparation of Cu/Sr3Ti2O7 and Its Photocatalytic Activity of Watersplitting for Hydrogen Evolution[J]. Acta Phys. -Chim. Sin., 2007,23(04): 601-604
132. CAO Chen-Zhong;ZENG Rong-Jin.Effect of Electronegativity and Polarizability on the C 1s Core Ionization Energies of Halomethanes[J]. Acta Phys. -Chim. Sin., 2006,22(09): 1085-1089
133. HOU Si-Cong;LIU Ling-Tao;KOU Yuan.Li-ZnO/La2O3 Catalyst for the Oxidation Coupling of Methane at Low Temperature[J]. Acta Phys. -Chim. Sin., 2006,22(08): 1040-1042
134. WANG Da-wang; MA Teng-cai; CUI Jin-hua.Methane Coupling in Atmospheric Pressure Glow Discharge Plasma with a Rotary Helix Electrode[J]. Acta Phys. -Chim. Sin., 2005,21(11): 1291-1294
135. DAI Wen-xin; WANG Xu-xu; FU Xian-zhi; LIU Ping; LIN Hua-xiang.Effect of Halides on Photo-induced Hydrophilicity over TiO2 Films[J]. Acta Phys. -Chim. Sin., 2005,21(11): 1274-1279
136. HUA Nan-ping; WU Zun-yi; DU Yu-kou; ZOU Zhi-gang; YANG Ping.Titanium Dioxide Nanoparticles Codoped with Pt and N for Photodegradation of Cl3CCOOH[J]. Acta Phys. -Chim. Sin., 2005,21(10): 1081-1085
137. TANG Zi-long ; MI Jia; ZHANG Zhong-tai; ZHOU Zhi-gang.Effect of Sm, Eu and Gd on Nb- doped TiO2 Varistors[J]. Acta Phys. -Chim. Sin., 2005,21(10): 1122-1126
138. SHI Jing-ying; LENG Wen-hua; CHENG Xiao-fang; ZHANG Jian-qing; CAO Chu-nan.Photocatalytic Oxidation of Methyl Red by TiO2 in a Photoelectrochemical Cell[J]. Acta Phys. -Chim. Sin., 2005,21(09): 971-976
139. XIONG Yu-hua; LI Feng-yi.Degradation of Polyethylene Film by Fe3+/TiO2 Photocatalyst[J]. Acta Phys. -Chim. Sin., 2005,21(06): 607-611
140. LI Yong-Xin; GUO Yu-Hua; JI Yong-Qiang.Catalytic Activity of M/(MgO)y(CeO2)1-y (M=Ni, Co, Cu) Catalysts for Methane Combustion[J]. Acta Phys. -Chim. Sin., 2005,21(05): 468-473
141. SHEN Guang-Xia; CHEN Yi-Cong; LIN Chang-Jian.Preparation of Nano TiO2-V2O5 Composite Coating and Its Functions in Corrosion Protection of Metals[J]. Acta Phys. -Chim. Sin., 2005,21(05): 485-489
142. WU Feng-Qing; REN Hui; ZOU Bo; WANG Zhu-Yi; ZHANG Tong; ZOU Le-Hui; XU Bao-Kun.Preparation of TiO2 Nanocrystalline and Its Sensitive Property to TMA[J]. Acta Phys. -Chim. Sin., 2005,21(05): 556-559
143. JING Li-Qiang; FU Hong-Gang; WANG De-Jun; WEI Xiao; SUN Jia-Zhong.Surface Photoinduced Charge Separation and Photocatalytic Activity of Sn Doped TiO2 Nanoparticles[J]. Acta Phys. -Chim. Sin., 2005,21(04): 378-382
144. BAO Xing-Wang;ZHANG Jin-Long;LIANG Xue-Hai;HUANG Jia-Zhen;ZHANG Li-Zhong.Preparation of TiO2 Thin Films at Low Temperature and Characterization of Their Properties[J]. Acta Phys. -Chim. Sin., 2005,21(01): 69-73
145. Jiang Zheng;Hou Hong-Xia;Hao Zheng-Ping;Kang Shou-Fang;Li Jin-Jun;Hu Chun.Effects of La Incorporation in Ba1xLaxFeAl11O19δ on the Performance of Methane Catalytic Combustion[J]. Acta Phys. -Chim. Sin., 2004,20(11): 1313-1319
146. Wang Cao;Kong Fan-Ao.Dissociation of Polyatomic Molecules in the Intense Femtosecond Laser Field[J]. Acta Phys. -Chim. Sin., 2004,20(08S): 1055-1062
147. Guo Jia-Hao;He Xiao-Ying;Guo Min;Cai Sheng-Min;Chen Xiu-Ying;Peng Xiao-Jun.Photoelectrochemical Studies of the TiO2 Nanocrystalline Electrode Sensitized by Novel Cyanine Dye[J]. Acta Phys. -Chim. Sin., 2004,20(08): 849-853
148. Cao Jiang-Lin;Leng Wen-Hua;Zhang Jian-Qing;Cao Chu-Nan.Adsorption Behavior and Photooxidation Kinetics of OH- at TiO2 Thin Film Electrodes[J]. Acta Phys. -Chim. Sin., 2004,20(07): 735-739
149. Su Yue-Feng;Wu Feng;Chen Chao-Feng.Preparation of Li4Ti5O12 from Nanocrystalline TiO2 and It’s Lithiation Performance[J]. Acta Phys. -Chim. Sin., 2004,20(07): 707-711
150. Wu Yu-Qi;Lü Gong-Xuan;Li Shu-Ben.Hydrogen Production by Pt/TiO2 Anaerobic Photocatalytic Reforming Degradation of Aqueous Monoethanolamine[J]. Acta Phys. -Chim. Sin., 2004,20(07): 755-758
151. Liu Shou-Xin;Sun Cheng-Lin.Influence of Silver Deposition on the Transfer of Photogenerated Electrons for TiO2 Photocatalyst[J]. Acta Phys. -Chim. Sin., 2004,20(06): 621-625
152. Yun Hong;Chen Jian-Hua;Zhang Hui;Lin Jing-Dong;Chen Hong-Bo;Lin Chang-Jian.The Effects of ZrO2 on Cu-ZnO-ZrO2 Catalysts for Hydrogen Generation by Steam Reforming of Methanol[J]. Acta Phys. -Chim. Sin., 2004,20(05): 550-553
153. Cui Jin-Hua;Xu Gen-Hui;Liu Chang-Jun.Novel Plasma Reactor with Rotary Multi-tip Electrode Used in CH4 Coupling[J]. Acta Phys. -Chim. Sin., 2004,20(05): 557-560
154. Li Ling-Xia;Wu Xia-Wan;Wang Hong-Ru;Zhang Zhi-Ping;Yu Hao-Ming.Analysis on Quantitative Relationship between Dielectric Properties and Phase Structure of High Frequency Dielectric System[J]. Acta Phys. -Chim. Sin., 2004,20(04): 396-399
155. Chu Dao-Bao;Wang Feng-Wu;Wei Yi-Jun;Yao Wen-Li;Li Xiao-Hua.Electrocatalytic Activities and Preparation of Nanocrystalline TiO2 -Pt Modified Electrode[J]. Acta Phys. -Chim. Sin., 2004,20(02): 182-185
156. Chen Ji-Xiang;Qiu Ye-Jun;Zhang Ji-Yan;Su Wan-Hua.Influence of La2O3 and CeO2 Promoters on Physico-chemical Properties and Catalytic Performance of Ni/MgO Catalyst in Methane Reforming with Carbon Dioxide[J]. Acta Phys. -Chim. Sin., 2004,20(01): 76-80
157. Zhang Li;Liu Hong-Guo;Kang Shi-Zhao;Zhang Ren-Jie;Mou Ying-Di;Qian Dong-Jin;Feng Xu-Sheng.The Fabrication of New Luminescent Thin Films of Europium Complex/TiO2/AA by Langmuir-Blodgett Technique[J]. Acta Phys. -Chim. Sin., 2003,19(12): 1146-1149
158. Tang Xiao-Ping;Wang Su-Fan;Gao Li-Rong;Wang Cao;Kong Fan-Ao.Dissociation of Methane in Intense Femtosecond Laser Field[J]. Acta Phys. -Chim. Sin., 2003,19(07): 661-665
159. Yao Qiao-Hong;Shan Lu;Li Fu-You;Yin Dong-Dong;Huang Chun-Hui.The Photoelectrochemical Properties of Four Hemicyanine Derivatives on Nanocrystalline TiO2 Electrode[J]. Acta Phys. -Chim. Sin., 2003,19(07): 635-640
160. Piao Ling-Yu;Li Yong-Dan.Structure of Carbon Nanotubes from Decomposition of Methane on an Aerogel Catalyst[J]. Acta Phys. -Chim. Sin., 2003,19(04): 347-351
161. Zhou Chang-Jun;Lin Wei;Zhu Yue-Xiang;Xie You-Chang.Sulphur Poisoning Mechanism of SnO2 Based Catalysts for Methane Combustion[J]. Acta Phys. -Chim. Sin., 2003,19(03): 246-250
162. Wang Jin-Zhong;Zhao Yan;Zhang Cai-Bei.Synthesis of Ordered Mesoporous TiO2 on a Composite Surfactant Template[J]. Acta Phys. -Chim. Sin., 2003,19(03): 251-255
163. Zheng Qing-Rong;Gu An-Zhong;Lin Wen-Sheng;Li Ming;Lu Xue-Sheng.Theoretical Study on the Adsorbed Hydrogen Molecules on Multi-Walled Carbon Nanotubes[J]. Acta Phys. -Chim. Sin., 2003,19(02): 139-143
164. Zhang Min;Jin Zhen-Sheng;Wang Shou-Bin;Zhang Shun-Li;Zhang Zhi-Jun.The Photocatalytic Enhancement Effect of CO on Pd/TiO2[J]. Acta Phys. -Chim. Sin., 2003,19(02): 100-104
165. Zhang Xin-Rong;Shi Peng-Fei.Catalytic Production of Hydrogen from Steam Reforming of Methanol on CeO2 Promoted Cu/Al2O3 Catalysts[J]. Acta Phys. -Chim. Sin., 2003,19(01): 85-89
166. Wang Bin;Gao Fei;He Bin;Zhang Dong-Bai;Cheng Hu-Min;Ma Ji-Ming;Qi Li-Min.Optic Property of CdS/TiO2 Composite Nanoparticle Prepared in the Reversed Microemulsion[J]. Acta Phys. -Chim. Sin., 2003,19(01): 21-24
167. Ling Lan;Wang Xu-Xu;Weng Hao;Yang Qing;Fu Xian-Zhi.Modification of CoMo/TiO2-Al2O3 Catalyst by Gas Phase Fluorination[J]. Acta Phys. -Chim. Sin., 2003,19(01): 70-74
168. Cui Xiao-Li;Jiang Zhi-Yu.Electrochemical Behavior of ITO/TiO2 Electrode under UV Illumination[J]. Acta Phys. -Chim. Sin., 2002,18(11): 1014-1017
169. Wang Jun-Wei;Xu Jin-Guang;Tian Zhi-Jian;Xu Yun-Peng;Xu Zhu-Sheng;Lin Li-Wu.Effect of Introduction of Ba, Mn on Thermal Stability and Catalytic Activity to Methane Combustion of Al2O3[J]. Acta Phys. -Chim. Sin., 2002,18(11): 1018-1022
170. Yan Zhen;Kou Yuan.Homogeneous Partial Oxidation of Methane Catalyzed by NOx under Oxidizing Conditions[J]. Acta Phys. -Chim. Sin., 2002,18(11): 1048-1051
171. Zhou Ling-Ping;Li Wei;Tao Ke-Yi;Li He-Xuan;Li Xuan-Wen.The Stability with Time-on-Stream of NaBr-Promoted KY Zeolite Catalyst for the Oxidative Methylation of Toluene with Methane[J]. Acta Phys. -Chim. Sin., 2002,18(10): 916-919
172. Sun Zhen-Fan;Li Yu-Guang.Surface Structural Morphology of TiO2 Nano-Films[J]. Acta Phys. -Chim. Sin., 2002,18(10): 896-900
173. Zhang Wen-Hua;Peng Jiang-Jie;Ma Yun-Sheng;Hao Li-Qing;Zhuang Shu-Xian.Catalytic Reduction of SO2 by CO on Sulfided CoMo/ Al2O3-TiO2 Catalysts[J]. Acta Phys. -Chim. Sin., 2002,18(10): 901-906
174. Zou Ji-Jun;Li Yang;Zhang Yue-Ping;Liu Chang-Jun.Product Distribution of Conversions of Methane and Carbon Dioxide Using Dielectric Barrier Discharge[J]. Acta Phys. -Chim. Sin., 2002,18(08): 759-763
175. Ji Yong-Qiang;Feng Wen-Lin;Hao Mao-Rong;Li Hui-Ying.The Reaction Path and Varitional Rate Constant of the Reaction CH3+CH3NO2→CH4+CH2NO2[J]. Acta Phys. -Chim. Sin., 2002,18(08): 721-726
176. Zhang Xian-Ren;Wang Wen-Chuan.Molecular Simulation on Adsorption of Methane in Mesopore MCM-41[J]. Acta Phys. -Chim. Sin., 2002,18(08): 680-685
177. Zhao Zhuan-Qing;Yao Su-Wei;Zhang Wei-Guo;Gong Zheng-Lie.Preparation and Photoelectrochemical Performance of Photoelectrode of TiO2 Film on Nickel[J]. Acta Phys. -Chim. Sin., 2002,18(05): 473-476
178. Zhao Wen-Kuan;Fang You-Ling.Synthesis of Photocatalytic Activity TiO2 Thin Films at LowTemperature[J]. Acta Phys. -Chim. Sin., 2002,18(04): 368-371
179. Cui Jin-Hua;Xu Gen-Hui;Han Sen.Eliminating Coke Formed in CH4 Coupling under Plasma via Pure H2 Discharge in the System[J]. Acta Phys. -Chim. Sin., 2002,18(03): 276-278
180. Yin Feng;Lin Yuan;Lin Rui-Feng;Xiao Xu-Rui.Photocatalytic Mechanism Studies of TiO2 Particulate Suspension by IntensityModulation Photocurrent Spectroscopy[J]. Acta Phys. -Chim. Sin., 2002,18(01): 21-25
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182. Cao Da-Peng;Wang Wen-Chuan;Shen Zhi-Gang;Chen Jian-Feng.Determination of Optimum Pressure for Supercritical Methane Adsorbed in Nano-material[J]. Acta Phys. -Chim. Sin., 2001,17(10): 940-943
183. Xiao Xu-Rui;Zhang Jing-Bo;Lin Yuan;Yin Feng;Li Xue-Ping.Study of the Kinetics of Nanocrystalline Semiconductor Thin Film Electrode Processes by Intensity Modulated Photocurrent Spectroscopy[J]. Acta Phys. -Chim. Sin., 2001,17(10): 918-923
184. Yang Yong-Lai;Xu Heng-Yong;Li Wen-Zhao.Study on Carbon Deposition of CH4,C2H6 and C2H4 Cracking over Ni-based Catalysts[J]. Acta Phys. -Chim. Sin., 2001,17(09): 773-775
185. Zhou Chang-Jun;Zhu Yue-Xiang;Xie You-Chang.Catalytic Combustion of Methane over Tin Dioxide Supported Silver Catalysts[J]. Acta Phys. -Chim. Sin., 2001,17(09): 850-854
186. Li Liao-Sha;Sui Zhi-Tong.Physical Chemistry Behavior of Enrichment Selectivity of TiO2 in Perovskite[J]. Acta Phys. -Chim. Sin., 2001,17(09): 845-849
187. Zhou Jian;Wang Wen-Chuan.Gibbs Ensemble Monte Carlo Simulation of Adsorption Equilibrium of Methane[J]. Acta Phys. -Chim. Sin., 2001,17(08): 723-727
188. Yan Qian-Gu;Luo Chun-Rong;Weng Wei-Zheng;Yang Le-Fu;Wan Hui-Lin;Wu Ting-Hua.Activation of Methane over Ni/TiO2 Catalyst[J]. Acta Phys. -Chim. Sin., 2001,17(08): 733-738
189. Xi Jing-Yu;Lv Gong-Xuan;Wang Zhi-Fei.Partial Oxidation of Methanol to Hydrogen over Cu/Zn and Cu/Zn/Ni Catalysts[J]. Acta Phys. -Chim. Sin., 2001,17(07): 655-658
190. Zhang Zhao-Liang;Ma Jun;Yang Xi-Yao.High Effective deSOx-deNOx Integrated Catalysts[J]. Acta Phys. -Chim. Sin., 2001,17(06): 481-483
191. Zhou Xing-Fu;Chu Dao-Bao;Han Ai-Jie;Gu Jia-Shan;Lin Chang-Jian;Tian Zhong-Qun;Tan Jian-Guang.Electrochemical Dissolution of Pure Titanium and Direct Hydrolysis for Preparation of Nanocrystalline TiO2[J]. Acta Phys. -Chim. Sin., 2001,17(04): 367-371
192. Zhang Yu-Hong;Xiong Guo-Xing;Yang Wei-Shen;Fu Xian-Zhi.Preparation of MxOy-TiO2 Photocatalysts by Sol-gel Method[J]. Acta Phys. -Chim. Sin., 2001,17(03): 273-277
193. Liu Ping;Zhou Ting-Yun;Lin Hua-Xiang;Fu Xian-Zhi.Coupling Effect for TiO2/SnO2 Compound Semiconductor Photocatalyst[J]. Acta Phys. -Chim. Sin., 2001,17(03): 265-270
194. Yu Jia-Guo;Zhao Xiu-Jian;Chen Wen-Mei;Lin Li;Zhang Ai-Li.Photocatalytic Activity and Hydrophilic Property of TiO2/SiO2 Composite Nanometer Thin Films[J]. Acta Phys. -Chim. Sin., 2001,17(03): 261-264
195. Ji Ya-Ying;Li Wen-Zhao;Xu Heng-Yong;Chen Yan-Xin.Study on the Ignition Process for the Catalytic Partial Oxidation of Methane to Synthesis Gas by MS-TPSR Technique[J]. Acta Phys. -Chim. Sin., 2001,17(03): 201-205
196. Gao En-Qin;Zhang Li;Yang Mai-Zhi;Cai Sheng-Min.Preparation of TiO2 Nanoparticles by Hydrothermal Method and its Application for Photoelectrochemical Cell[J]. Acta Phys. -Chim. Sin., 2001,17(02): 177-180
197. Yan Xiu-Ru;Li Xiao-Hong;Huo Ming-Liang;Guo Wei-Wei;Gong Yong-Jin.Preparation and Photocatalytic Properties of Nanometer SnO2@TiO2[J]. Acta Phys. -Chim. Sin., 2001,17(01): 23-27
198. Su Wen-Yue;Fu Xian-Zhi;Wei Ke-Mei.Effect of Sulfation on Structure and Photocatalytic Performance of TiO2[J]. Acta Phys. -Chim. Sin., 2001,17(01): 28-31
199. Zhu Ai-Min, Zhang Xiu-Ling, Gong Wei-Min, Zhang Bao-An.Study on Coupling of Methane under Pulse Corona Plasma in the Presence of Oxygen[J]. Acta Phys. -Chim. Sin., 2000,16(09): 839-843
200. Li Jian-Chang, Xue Zeng-Quan, Zhang Hao, Zeng Yan, Liu Wei-Min, Wu Quan-De.Chiral Fractal Patterns of TCNQ Thin Films Grown by Vacuum Evaporation[J]. Acta Phys. -Chim. Sin., 2000,16(07): 579-582
201. Chen Hong-Shan, Niu Jian-Zhong, Xia Chun-Gu, Li Shu-Ben.Raman Spectroscopy Characterization of Na-W-Mn/SiO2 Catalyst for Oxidative Coupling of Methane[J]. Acta Phys. -Chim. Sin., 2000,16(06): 543-546
202. Li Jian-Chang, Song Yan-Lin, Xue Zeng-Quan, Liu Wei-Min, Jiang Lei, Zhu Dao-Ben.Microstructure and Electric Properties of Polyaniline-TCNQ Complex Thin Film Grown by Vacuum Evaporation[J]. Acta Phys. -Chim. Sin., 2000,16(04): 289-293
203. Li Chun-Yi, Yu Chang-Chun, Shen Shi-Kong.The Main Origin of CO2 in Partial Oxidation of Methane to syngas over a Ni/Al2O3 Catalyst[J]. Acta Phys. -Chim. Sin., 2000,16(02): 97-100
204. Zhu Yong-Fa, Zhang Li, Gao Chong, Yao Wen-Qing, Cao Li-Li.The Preparation of Nanosized Anatase TiO2 Powder by Using TiCl4 a Precursor[J]. Acta Phys. -Chim. Sin., 1999,15(09): 784-788
205. Jin Rong-Chao, Chen Yan-Xin, Cui Wei, Li Wen-Zhao, Yu Chun-Ying, Jiang Yi.Mechanism of Catalytic Partial Oxidation of Methane to Synthesis Gas on Nickel Catalyst[J]. Acta Phys. -Chim. Sin., 1999,15(04): 313-318
206. Liu Yan-Fang, Zhao Min, Shen Shi-Gang, Gao Jun-Gang.Curing Kinetics of Tetrabromo-bisphenol-a Epoxy Resin with Diaminodiphenyl Methane[J]. Acta Phys. -Chim. Sin., 1998,14(10): 927-931
207. Jin Rong-Chao, Chen Yan-Xin, Li Wen-Zhao, Ji Ya-Ying, Qin Yong-Sheng, Jiang Yi.Ni/α-Al2O3 Catalyst for the Partial Oxidation of Methane to Syngas[J]. Acta Phys. -Chim. Sin., 1998,14(08): 737-741
208. Fan Xiao-Wei, Zhou Shao-Jie, Zhang Qing-Xiang, Deng Jing-Kang, Zheng Yan-You, Gao Nai-Fei, Chen Xue-Jun.Accurate Study of Valence Orbitals of Methane by Electron Momentum Spectroscopy[J]. Acta Phys. -Chim. Sin., 1998,14(06): 573-576
209. Zeng Jin-Long, Xiong Zhi-Tao, Lin Guo-Dong, Yu La-Jia, Zhang Hong-Bin.Spectroscopic Characterization of Mo/HZSM-5-based Catalysts for Dehydro-aromatization of Methane[J]. Acta Phys. -Chim. Sin., 1998,14(05): 394-400
210. Dong Guo-Li, Gao Yin-Ben, Chen Song-Ying.Effect of Different Drying Methods on the Properties of TiO2 Particles[J]. Acta Phys. -Chim. Sin., 1998,14(02): 142-146
211. Xiao Zhong-Dang, Huang Dan, Gu Jian-Hua, Lu Zu-Hong.X-ray Photoelectron Spectroscopy Study of the Deposition of TiO2 Thin Films on Self-assembly Monolayer[J]. Acta Phys. -Chim. Sin., 1998,14(01): 57-62
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213. Liu Wei-,Xu Yi-De,Li Li-Yun,Hu Hong-Bing.Study Mo/HZSM-5 Catalysts by NMR[J]. Acta Phys. -Chim. Sin., 1997,13(08): 693-699
214. Zhang Gui-Qiu,Sha Guo-He,Xu Ji-Jun,Knott W.Proch D.Abnormal Pressure Effects of H2 Three-photon Resonant Enhanced Ionization Spectroscopy[J]. Acta Phys. -Chim. Sin., 1997,13(07): 617-620
215. Tian Yi-Ling,Xiao Yan-Fan,Zhu Hong-Xu,Dong Xi-Jing,Ren Xiao-Wen,Zhang Feng-Cai.Interfacial Tensions between Water and Non-polar Fluids at High Pressures and High Temperatures[J]. Acta Phys. -Chim. Sin., 1997,13(01): 89-95
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217. Chu Yan-Lai,Li Shu-Ben,Gong Hua,Chen Zheng-Shi.Active Phase and Reaction Mechanism of Methane Partial Oxidation on Ni-Cu-Al2O3 Catalysts[J]. Acta Phys. -Chim. Sin., 1996,12(05): 429-435
218. Luo Sheng-Cheng,Gui Lin-Lin,Tang You-Qi.The Characterisation of the Adsorption of H2S on MoO3/TiO2-Al2O3 by XPS[J]. Acta Phys. -Chim. Sin., 1996,12(04): 341-345
219. Luo Sheng-Cheng,Gui Lin-Lin,Tang You-Qi.The Comparative Study on TiO2-Al2O3 Composites[J]. Acta Phys. -Chim. Sin., 1996,12(01): 7-11
220. Fu Xian-Zhi,Huang Hui-Zhong,Zhu Lin,Luo Sheng-Cheng,Gui Lin-Lin.Investigation of Sulfidation Processes for Hydrotreating Catalysts by[J]. Acta Phys. -Chim. Sin., 1995,11(12): 1071-1076
221. Yu Lin,Xu Yi-De,Guo Xie-Xian.A FT-IR Study on the Interaction of CH4 and O2 with the Surface of SrO-La2O3/CaO Catalysts[J]. Acta Phys. -Chim. Sin., 1995,11(10): 902-906
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228. Zhao Zhen, Yuan Song-Yue, Yu Zuo-Long.Role of Lithium in Multicomponent Oxide Catalysts for Oxidative Coupling of Methane[J]. Acta Phys. -Chim. Sin., 1994,10(07): 616-622
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230. Zhao Zhen, Yuan Song-Yue, Yu Zuo-Long.Study of Methane Oxidative Coupling over Ti-La-Li Mixed Oxides[J]. Acta Phys. -Chim. Sin., 1994,10(04): 324-329
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232. Li Can, Zhang Hui, Wang Kai-Li, Xin Qin.FT-IR Emission Spectroscopic Studies of Surface Structure of V2O5/TiO2 Catalyst[J]. Acta Phys. -Chim. Sin., 1994,10(01): 33-37
233. Luo Xiao-Ming; Han Qiao-Feng; Chen Yi; Han Shi-Ying; Jin Tong-Zheng; Sui Yun-Xia.The Study of Adsorbed Oxygen Species on the Surface of a Series of Na2SnO3 Catalysts by epr Experiments[J]. Acta Phys. -Chim. Sin., 1993,9(06): 746-751
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235. Ye Dai-Qi; Liang Hong; Huang Zhong-Tao.Study on the Interaction Between the Active Phase and Support on V2O5/TiO2 Catalyst[J]. Acta Phys. -Chim. Sin., 1993,9(04): 501-508
236. Zhao Bi-Ying; Xu Xian-Ping; Ma Hua-Rong; Gao Jin-Ming; Wang Rong-Qiu; Sun Dong-Hong; Tang You-Qi.A New Way to Prepare Some Supported Catalysts With Highly Specific Surfaces[J]. Acta Phys. -Chim. Sin., 1993,9(01): 8-12
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240. Wei Zhao-Bin; Wei Cheng-Dong; Xin Qin.Raman Spectroscopic Study of MoO3/TiO2-Al2O3 Catalyst[J]. Acta Phys. -Chim. Sin., 1992,8(02): 261-265
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242. Guo Jing-Zhong; Gu Yue-Shu; Liu Chuan-Pu; Li Bao-Zhong; Yin Yong-Jia; Cai Ji-Ye; Cao De-Zhao.Study on the Structure Defect of Electrodeposited Tin Using Positron Annihilation Lifetime Spectroscopy[J]. Acta Phys. -Chim. Sin., 1991,7(02): 211-214
243. Gong Hua; Jiang Yong-Ji; Wang Yi; Chen Ming-Zhi; Zheng Guo-Kang.Excess Volumes for (Tetrachlorloromethane+Lewis Bases) and for (Trichloromethane+Lewis Bases)[J]. Acta Phys. -Chim. Sin., 1991,7(01): 49-56
244. LU Yang.Recent Progress in Facet Effect of TiO2 Photocatalysts[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
245. XU Juan, LIU Jia-Qin, LI Jing-Wei, WANG Yan, LV Jun, WU Yu-Cheng.Controlled Synthesis and Supercapacitive Performance of Heterostructured MnO2/H-TiO2 Nanotube Arrays[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
246. NIE Wang-Xin, ZOU Xiu-Jing, WANG Xue-Guang, DING Wei-Zhong, LU Xiong-Gang.Preparation of Highly-Dispersed Ni-Ce-Zr Oxides over Mesoporous γ-Alumina and Their Catalytic Properties for CO2 Methanation[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
247. ZHOU Li, LIU Huan-Huan, YANG Yu-Lin, QIANG Liang-Sheng.SILAR Prepared TiO2/CdS/Co-Pi Water Oxidation Photoanode and Its Performance[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
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