ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2012,Vol.28>> Issue(04)>> 871-876     doi: 10.3866/PKU.WHXB201202013         中文摘要
Highly Active Pd-Co3O4/MWCNTs Catalysts for Methanol Electrocatalytic Oxidation
NIE Su-Lian, ZHAO Yan-Chun, FAN Jie-Wen, TIAN Jian-Niao, NING Zhen, LI Xiao-Xiao
Key Laboratory for the Chemistry and Molecular Engineering of Medicinal Resources, Ministry of Education of China, College of Chemistry and Chemical Engineering, Guangxi Normal University, Guilin 541004, Guangxi Province, P. R. China
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Nano-flocculent-Co3O4 modified multi-walled carbon nanotubes supported Pd nanoparticles (Pd-Co3O4/MWCNTs) with uniform dimensions were prepared by a facile hydrothermal method using Co(NO3)3·6H2O as the cobalt source, polyethylene glycol (PEG) 20000 as a surface active agent, and H2PdCl4 as the Pd precursor. The catalysts were characterized by scanning electron microscopy, transmission electron microscopy, and X-ray powder diffraction. The Pd nanoparticles had a face-centered cubic crystal structure and were well dispersed on the external walls of the Co3O4/MWCNTs. The catalytic activity was studied by cyclic voltammetry and chronoamperometry toward methanol oxidation. The Pd-Co3O4/MWCNT catalysts had a large electrochemically active area, good electrocatalytic performance, and stability toward methanol oxidation in alkaline media. All the results suggest that Co3O4 will improve the electrocatalytic activity in direct methanol fuel cells.

Keywords: Direct methanol fuel cell   Co3O4   Hydrothermal method   Pd   Multi-walled carbon nanotubes   Electrocatalytic oxidation  
Received: 2011-10-19 Accepted: 2012-01-10 Publication Date (Web): 2012-02-01
Corresponding Authors: ZHAO Yan-Chun Email:

Fund: The project was supported by the Guangxi Natural Science Foundation, China (2010GXNSFF013001, 0728043) and National Natural Science Foundation of China (21163002).

Cite this article: NIE Su-Lian, ZHAO Yan-Chun, FAN Jie-Wen, TIAN Jian-Niao, NING Zhen, LI Xiao-Xiao. Highly Active Pd-Co3O4/MWCNTs Catalysts for Methanol Electrocatalytic Oxidation[J]. Acta Phys. -Chim. Sin., 2012,28 (04): 871-876.    doi: 10.3866/PKU.WHXB201202013
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68. JIANG Yong; CHU Wei; JIANG Cheng-Fa; WANG Yao-Hong.A DFT Study of Pdn(n=1-7) Clusters and Their Interactions with CH4 Molecule[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1723-1727
69. JIN Ling-Yun; LU Ji-Qing; LUO Meng-Fei; XIE Guan-Qun; HE Mai.CeO2-Y2O3 Washcoat and Supported Pd Catalysts for the Combustion of Volatile Organic Compounds (VOCs)[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1691-1695
70. ZHAO Qing; ZHAI Guang-Jie; ZAERA Francisco.Conversion of Alcohol Oxidation on Ni(100) by Fluorine[J]. Acta Phys. -Chim. Sin., 2007,23(09): 1447-1450
71. FU Jian-Liang; ZHANG Xing-Wang; LEI Le-Cheng.Fe-modified Multi-walled Carbon Nanotube Electrode for Production of Hydrogen Peroxide[J]. Acta Phys. -Chim. Sin., 2007,23(08): 1157-1162
72. YANG Su-Dong; ZHANG Xiao-Gang; HUANG Jian-Shu; SUN Jing-Yu.Pd-Ni/MWCNT Electrocatalysts for Ethylene Glycol Electro-oxidation in Alkaline Medium[J]. Acta Phys. -Chim. Sin., 2007,23(08): 1224-1228
73. DENG Hui-Ning; WANG Yu-Xin.Preparation and Properties of Proton Conducting Composite Membranes from Sulfonated Poly(phthalazinone ether keton) and Phosphotungstic Acid[J]. Acta Phys. -Chim. Sin., 2007,23(08): 1235-1240
74. ZHENG Hai-Tao; LI Yong-Liang; LIANG Jian-Ying; SHEN Pei-Kang.Methanol Oxidation on Pd-based Electrocatalysts[J]. Acta Phys. -Chim. Sin., 2007,23(07): 993-996
75. LI Lan-Lan; WEI Zi-Dong; YAN Can; LUO Yi-Hui; YIN Guang-Zhi; SUN Cai-Xin.Methanol Oxidation on a Pt ElectrodeModified by Underpotential Deposition of Ru[J]. Acta Phys. -Chim. Sin., 2007,23(05): 723-727
76. SUN Xi-Yuan; KONG Fan-Jie; JIANG Gang; ZHU Zheng-He.Thermodynamics of Water Adsorbed on Palladium Surface[J]. Acta Phys. -Chim. Sin., 2007,23(05): 651-654
77. WU Wei; CAO Jie-Ming; CHEN Yu; LU Tian-Hong.Preparation of High-alloying Pt-Ru/CMK-3 Catalysts in THF-H2O-EtOH Ternary Solution System[J]. Acta Phys. -Chim. Sin., 2007,23(04): 559-564
78. DENG Hui-Ning;WANG Yu-Xin .Sulfonated Poly(phthalazinones) Membranes For Direct Methanol Fuel Cell[J]. Acta Phys. -Chim. Sin., 2007,23(02): 187-191
79. WU Jin;DU Lin;Li Gui-Ying;LIANG Bin-Yong;QIN Song;HU Chang-Wei .Study on the Photoelectrochemical degradation of Reactive Brilliant Red K-2BP on RuOx-PdO/Ti electrode[J]. Acta Phys. -Chim. Sin., 2007,23(02): 268-273
80. HUANG Mian-Yan;CHEN Hua-Yan;GUO Jian-Zhao;WANG Zhi-Tao;XU Li;WANG Yu-Xin.Methanol Resistant Poly(Ether Sulfone)/Sulfonated Poly(Ether Ether Ketone) Blend Proton Exchange Membrane for DMFC[J]. Acta Phys. -Chim. Sin., 2007,23(01): 44-49
81. LI Quan;LI De-Hua;SHENG Yong;ZHU Zheng-He.Structure and Stability of PdYn±(n=0, 1, 2, 3) Molecular Ions[J]. Acta Phys. -Chim. Sin., 2006,22(12): 1516-1519
82. ZHAO Qing;ZHANG Hui-Min;ZAERA Francisco .Adsorption and Thermal Decomposition of 2-Iodoethanolon Ni(100)-Intermediates of Oxidation of Hydrocarbons: Hydroxyalkyls and Oxametallacycles[J]. Acta Phys. -Chim. Sin., 2006,22(11): 1353-1360
83. BIAN Cheng-Xiang;XU Xue-Cheng;YU Wei;CHEN Yi-Wei;CHENG Rong-Ming;SHI Yan;LI Xiang-Mei;JIN Sheng-Song.Study on Conductive Mechanism of Composites―Sulfonated Polyphenylacetylene / Multiwalled Carbon Nanotubes[J]. Acta Phys. -Chim. Sin., 2006,22(10): 1185-1190
84. ZHAO Qing;ZHANG Hui-Min;ZAERA Francisco.Chemical Thermal Decomposition of 2-iodoethanol on Ni(100)[J]. Acta Phys. -Chim. Sin., 2006,22(09): 1043-1046
85. CHEN Zhe;YAN You-Wei .Combustion Synthesis and Luminescent Properties of blue-emitting Nanocrystalline Phosphor for PDP Application[J]. Acta Phys. -Chim. Sin., 2006,22(08): 1030-1033
86. ZHU Yu;JIANG Gang;FANG Fang;YU Gui-Feng;ZHU Zheng-He.Structure and Potential Energy Function of PdN and PdN2 Molecules*[J]. Acta Phys. -Chim. Sin., 2006,22(05): 538-541
87. ZHANG Zeng-Fu; LUO Guo-Hua; FAN Zhuang-Jun; XIANG Rong; ZHOU Li; WEI Fei.Complex Permittivity and Permeability Spectra of Different Kinds of Carbon Nanotubes[J]. Acta Phys. -Chim. Sin., 2006,22(03): 296-300
88. YANG Bo; YU Gang; HUANG Jun.Electrocatalytic Reductive Dechlorination of 2,4,5-PCB in Aqueous Solution by Palladium-modified Titanium Mesh as Cathode[J]. Acta Phys. -Chim. Sin., 2006,22(03): 306-311
89. CHEN Ling; WANG Xin-dong; GUO Min.The Effect of NdOx as Co-catalyst for the Electro-oxidation of Methanol on PtRu/C[J]. Acta Phys. -Chim. Sin., 2006,22(02): 141-145
90. ZHU Yu;JIANG Gang;YU Gui-Feng;ZHU Zheng-He;WANG He-Yi;FU Yi-Bei.Adsorption Behavior of N2 on Pd Surface[J]. Acta Phys. -Chim. Sin., 2005,21(12): 1343-1346
91. TANG Jing; PETRI Marc; KIBLER Ludwig A.; KOLB Dieter M..ECSTM Tip-induced Nanostructuring of Ordered Pd Clusters Array[J]. Acta Phys. -Chim. Sin., 2005,21(11): 1303-1306
92. LI Juan; FANG Zheng-ping; WANG Jian-guo; GU Aijuan; TONG Li-fang; LIU Fu.Microstructure Transformation of Multi-walled Carbon Nanotubes during Diamine Grafting Process[J]. Acta Phys. -Chim. Sin., 2005,21(11): 1244-1248
93. WANG Zhen-bo; YIN Ge-ping; SHI Peng-fei.The Influence of Three Groups of Pt-Ru/C Catalyst’s Precursors on Its Performance for Direct Methanol Fuel Cell[J]. Acta Phys. -Chim. Sin., 2005,21(10): 1156-1160
94. PENG Jing; ZHU Yi-cai; ZHAI Mao-lin; QIAO JIN-liang; WEIG en-shuan.Influence of OH Radicals on the Radiation Effect of Polydimethylsiloxane Latex[J]. Acta Phys. -Chim. Sin., 2005,21(08): 873-877
95. HE Qin; ZHOU Li-xin.Theoretical Study on the Interaction of Platinum Compounds with DNA Base Pairs[J]. Acta Phys. -Chim. Sin., 2005,21(08): 846-851
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97. TANG Tian-di; CHEN Jiu-ling; LI Yong-dan.Treatment of the Carbon Nanofiber Surfaces in Mixed Concentrated HNO3-H2SO4 and the Catalytic Activity of Supported Pd-Pt for Naphthalene Hydrogenation[J]. Acta Phys. -Chim. Sin., 2005,21(07): 730-734
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