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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2012,Vol.28>> Issue(08)>> 1978-1984     doi: 10.3866/PKU.WHXB201205172         中文摘要
CATALYSIS AND SURFACE SCIENCE
Visible Light Photocatalytic Properties of Bi3.25La0.75Ti3O12 Nanowires
LIN Xue1,2, Lü Peng1, GUAN Qing-Feng1, LI Hai-Bo3, LI Hong-Ji2, CAI Jie1, ZOU Yang1
1. School of Materials Science and Engineering, Jiangsu University, Zhenjiang 212013, Jiangsu Porvnce, P. R. China;
2. College of Chemistry, Key Laboratory of Preparation and Application Environmentally Friendly Materials of the Ministry of Education, Jilin Normal University, Siping 136000, Jilin Porvnce, P. R. China;
3. College of Physics, Jilin Normal University, Siping 136000, Jilin Porvnce, P. R. China
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Lanthanum-doped bismuth titanate (Bi3.25La0.75Ti3O12, BLT) nanowires were synthesized by a one-step hydrothermal process and their optical and photocatalytic properties were investigated. Their crystal structure and microstructures were characterized using X-ray diffraction (XRD), transmission electron microscopy (TEM), and high-resolution transmission electron microscopy (HRTEM). The BLT nanowires obtained are single-phase with an average diameter of 25 nm. The room temperature photoluminescence (PL) spectrum reveals two visible emission peaks at 400 and 596 nm, which are assigned to excitonic and surface-defect emissions, respectively. The UV-visible diffuse reflectance spectrum (UV-Vis DRS) reveals that the band gap of BLT nanowires is 2.07 eV. The prepared BLT nanowires are stable and exhibit higher photocatalytic activities in the degradation of methyl orange (MO) under visible light irradiation (λ >420 nm) compared with commercial P25 TiO2, traditional N-doped TiO2 (N-TiO2), and pure bismuth titanate (Bi4Ti3O12, BIT). The high photocatalytic performance of BLT photocatalysts is attributed to the strong visible light absorption and the recombination restraint of the e-/h+ pairs resulting from the presence of La3+ ions.



Keywords: Bismuth titanate   Lanthanum doping   Nanowire   Hydrothermal synthesis   Photocatalytic degradation   Visible light irradiation  
Received: 2012-04-09 Accepted: 2012-05-17 Publication Date (Web): 2012-05-17
Corresponding Authors: GUAN Qing-Feng Email: guanqf@ujs.edu.cn

Fund: The project was supported by the Key Laboratory of Preparation and Application Environmentally Friendly Materials of the Ministry of Education of China.

Cite this article: LIN Xue, Lü Peng, GUAN Qing-Feng, LI Hai-Bo, LI Hong-Ji, CAI Jie, ZOU Yang. Visible Light Photocatalytic Properties of Bi3.25La0.75Ti3O12 Nanowires[J]. Acta Phys. -Chim. Sin., 2012,28 (08): 1978-1984.    doi: 10.3866/PKU.WHXB201205172

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61. HOU Jun-Wei, SONG Bo, ZHANG Zhi-Hua, WANG Wen-Jun, WU Rong, SUN Yan-Fei, ZHENG Yu-Feng, DING Peng, JIAN Ji-Kang.Synthesis of Highly-Crystallized Ternary Cd1-xZnxS Nanowires by Chemical Vapor Deposition[J]. Acta Phys. -Chim. Sin., 2009,25(04): 724-728
62. LI Hai-Yan; JIAO Jun.Alignment Behavior and Field Emission Properties of Cadmium Sulfide Nanowires Synthesized via a Bismuth Triiodide Sheet-Assisted Solution-Phase Method[J]. Acta Phys. -Chim. Sin., 2009,25(03): 401-405
63. XUE Cheng-Shan; ZHANG Dong-Dong; ZHUANG Hui-Zhao; HUANG Ying-Long; WANG Zou-Ping; WANG Ying.Structure and Characterization of Mg-Doped GaN Nanowires[J]. Acta Phys. -Chim. Sin., 2009,25(01): 113-115
64. LI Kui-Ying; GUO Jing; LIU Tong; ZHOU Bing-Jing; LI Yue.Electron Structure and Energy Transformation Mechanism of the Surface of Porous Nanocrystalline TiO2 Doped with La[J]. Acta Phys. -Chim. Sin., 2008,24(11): 2096-2101
65. YAO Hui-Jun; MO Dan; DUAN Jing-Lai; CHEN Yan-Feng; ZHANG Ling; LIU Jie; HOU Ming-Dong; SUN You-Mei.Preparation and Optical Properties of Gold Nanowire Arrays[J]. Acta Phys. -Chim. Sin., 2008,24(10): 1922-1926
66. ZHANG Zhi-Jun; WANG Fa-Zhan; LIU Bo; YUAN Si-Cong.Structural and Photoluminescent Properties of Ternary Zn1-xCdxO Bramble-like Nanostructures[J]. Acta Phys. -Chim. Sin., 2008,24(10): 1912-1916
67. HAN Yi; LI Wei; ZHANG Ming-Hui; TAO Ke-Yi.Synthesis and Magnetic Property of Fe-B Amorphous Alloy Nanowires by Inducing DC Magnetic Field[J]. Acta Phys. -Chim. Sin., 2008,24(06): 927-931
68. ZHENG Kai-Bo; LI Jing-Lei; SHEN Hao-Ting; SUN Da-Lin; CHEN Guo-Rong.Gas Sensing Properties of Single ZnO Nanowire at Room Temperature[J]. Acta Phys. -Chim. Sin., 2008,24(06): 1080-1084
69. FU Xiao-Feng; ZOU Hua-Min; ZHOU Li; ZHOU Zhang-Kai; YU Xue-Feng; HAO Zhong-Hua.Growth Mechanism of Penta-twinned Ag Nanowires Synthesized by Polyol Process[J]. Acta Phys. -Chim. Sin., 2008,24(05): 781-787
70. WEI Qiang, LI Meng-Ke, YANG Zhi, CAO Lu, ZHANG Wei, LIANG Hong-Wei.Fabrication and Optical Properties of Aligned Zn1-xMgxO Nanowire Arrays[J]. Acta Phys. -Chim. Sin., 2008,24(05): 793-798
71. DENG Zhan-Qiang; QI Jun-Jie; ZHANG Yue; LIAO Qing-Liang; HUANG Yun-Hua; CAO Jia-Wei.Synthesis, Structure and Growth Mechanism of ZnS Nanowires with High Aspect Ratio[J]. Acta Phys. -Chim. Sin., 2008,24(02): 193-196
72. GAI Hong-De; WU You-Shi; WU Li-Li; SHI Yuan-Chang; JING Min; ZOU Ke.PVA-Assisted Synthesis and Characterization of CdS Nanowires[J]. Acta Phys. -Chim. Sin., 2008,24(01): 157-160
73. WANG Feng; HAO Ya-Juan; JIN Guo-Qiang; GUO Xiang-Yun.Effects of the Reaction Conditions in Preparation of Si3N4 Nanowires[J]. Acta Phys. -Chim. Sin., 2007,23(10): 1503-1507
74. SUN Lan; ZUO Juan; LAI Yue-Kun; NIE Cha-Geng; LIN Chang-Jian.Electrical Transport Properties of Individual TiO2 Nanowire in One Dimension[J]. Acta Phys. -Chim. Sin., 2007,23(10): 1603-1606
75. YAO Su-Wei; SONG Zhen-Xing; WANG Hong-Zhi.Fabrication and Magnetic Properties of Co/Cu Multilayer Nanowire Arrays[J]. Acta Phys. -Chim. Sin., 2007,23(08): 1306-1310
76. ZHOU Guo-Rong; LI Bei-Qi; GENG Hao-Ran; TENG Xin-Ying; CHEN Guang-Li.Freezing Process of Al Nanowires by Molecular Dynamics Simulation[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1071-1074
77. YAO Hui-Jun; LIU Jie; DUAN Jing-Lai; HOU Ming-Dong; SUN You-Mei; MO Dan; CHEN Yan-Feng; XUE Zhi-Hao.Preparation of Silver Nanowires in Ion-trackMembranes[J]. Acta Phys. -Chim. Sin., 2007,23(04): 489-492
78. ZOU Xing-Quan;WU Ping;LI Qiang;XIAO Tan
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79. LI Jing-Yi;SIQIN Gao-Wa;LIU Li-Na.Photocatalytic Degradation of Organic Pollutants on TiO2/Bentonite[J]. Acta Phys. -Chim. Sin., 2007,23(01): 16-20
80. PAN Guang-Hu;ZHANG Qi-Feng;ZHANG Jun-Yan;WU Jin-Lei .Luminescence Properties of As-doping ZnO Nanowires[J]. Acta Phys. -Chim. Sin., 2006,22(11): 1431-1434
81. PAN Guo-Wei.Silicon Nanowires Produced by SiO-Au Method[J]. Acta Phys. -Chim. Sin., 2006,22(09): 1147-1150
82. FENG Chun-Bo;DU Zhi-Ping;Zhao Yong-Hong;TAI Xiu-Mei;LI Qiu-Xiao .Photocatalytic Activity of Au Modified Nano-TiO2 for NPE-10 Degradation[J]. Acta Phys. -Chim. Sin., 2006,22(08): 953-957
83. ZHANG Wei-guo;LI Wei-Xiang;ZHANG Lu;YAO Su-Wei .Electrodeposition of Cu/Ni Multilayered Nanowires Ordered Arrays by Dual Bath Technique[J]. Acta Phys. -Chim. Sin., 2006,22(08): 977-980
84. LIU Ling; ZHAO Yao-Min; YANG Jie; ZHAO Chong-Jun; JIANG Zhi-Yu.Photoeletrochemical Behavior of Polypyrrole Nanofiber Array Electrodes[J]. Acta Phys. -Chim. Sin., 2006,22(03): 261-264
85. MIAO Jian-ying; ZHAO Li-fang; LIU Zong-huai.Hydrothermal Synthesis and Characterization of Layered Zinc Benzoate Hydroxide Compound[J]. Acta Phys. -Chim. Sin., 2006,22(02): 193-197
86. REN Xin; HUANG Xin-min; ZHANG Hu-hai.Fabrication of Ni-P Nanowire and Nanotube Ordered Arrays by Electroless Deposition[J]. Acta Phys. -Chim. Sin., 2006,22(01): 102-105
87. ZHANG Lu; YAO Su-wei; ZHANG Wei-guo; WANG Hong-zhi.Preparation and Formation Mechanism of Alumina Nanowires[J]. Acta Phys. -Chim. Sin., 2005,21(11): 1254-1258
88. HUA Nan-ping; WU Zun-yi; DU Yu-kou; ZOU Zhi-gang; YANG Ping.Titanium Dioxide Nanoparticles Codoped with Pt and N for Photodegradation of Cl3CCOOH[J]. Acta Phys. -Chim. Sin., 2005,21(10): 1081-1085
89. YUAN Juan; XIAO Yao-kun; YU Gang; HU Bo-nian; YE Li-yuan.Pd-Ni Nanowires Prepared by Electrochemical Step-edge Decoration[J]. Acta Phys. -Chim. Sin., 2005,21(06): 602-606
90. XIONG Yu-hua; LI Feng-yi.Degradation of Polyethylene Film by Fe3+/TiO2 Photocatalyst[J]. Acta Phys. -Chim. Sin., 2005,21(06): 607-611
91. LI Hua; XU Cai-ling; ZHAO Guang-yu; LI Hu-lin.Preparation and Magnetic Properties of Amorphous Co-Pt Alloy Nanowire Arrays[J]. Acta Phys. -Chim. Sin., 2005,21(06): 641-645
92. CAI Cheng-Dong; ZHOU Jian-Zhang; QI Li; XI Yan-Yan; LAN Bi-Bo; WU Ling-Ling; LIN Zhong-Hua.Conductance of a Single Conducting Polyaniline Nanowire[J]. Acta Phys. -Chim. Sin., 2005,21(04): 343-346
93. QIAO Jun-Juan;MENG Xiang-Min;ZHANG Xiao-Hong;WU Shi-Kang.Nano-wire Preparation of Small Molecular Organic Compound in Solution[J]. Acta Phys. -Chim. Sin., 2005,21(01): 106-109
94. Zhou Jian-Zhang; Dong Ping; Cai Cheng-Dong; Lin Zhong-Hua.Chemically Modified AAO Template and Application to PANI Nanowires Synthesis[J]. Acta Phys. -Chim. Sin., 2004,20(11): 1287-1291
95. Su Wen-Yue;Zhang Yong;Wang Xu-Xu;Fu Xian-Zhi.Reaction Pathway of Photocatalytic Degradation of Methyl-tert-butyl Ether in Water[J]. Acta Phys. -Chim. Sin., 2004,20(10): 1211-1215
96. Jia Chong;Jin Chuan-Gui;Liu Wei-Feng;Cai Wei-Li;Yao Lian-Zeng;Li Xiao-Guang.Fabrication of Sb Single-crystal Nanowire Arrays[J]. Acta Phys. -Chim. Sin., 2004,20(03): 240-243
97. Han Shi-Tong;Xi Hai-Ling;Fu Xian-Zhi;Wang Xu-Xu;Ding Zheng-Xin;Lin Zhi-Cong;Su Wen-Yue.Study on the Photocatalytic Degradation of a Simulate Agent (2-CEES) of Mustard Gas[J]. Acta Phys. -Chim. Sin., 2004,20(03): 296-301
98. Wei Jin-Quan;Jiang Bin;Li Yan-Hui;Wu De-Hai.Preparation and Structure of Boron Carbide Nanowires[J]. Acta Phys. -Chim. Sin., 2004,20(03): 256-259
99. Liu Lei;Zhang Gao-Yong;Dong Jin-Xiang.Effects of Different Templating Agent on the Structure of Silica MCM-41 Mesoporous Molecular Sieves[J]. Acta Phys. -Chim. Sin., 2004,20(01): 65-69
100. Nie Qiu-Lin;Yuan Qiu-Li;Xu Zhu-De;Chen Wei-Xiang.Study on the Morphology Control of CdS Nanocrystals Synthesized by Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2003,19(12): 1138-1142
101. Li Zeng-He;Yin Chen;Wang Ru-Ji;Wang Ping;Guo Hong-You.Synthesis and Crystal Structure of an Inorganic-Organic Hybrid CompoundCo(μ2-bpy)V2O6 (bpy=4,4’-bipyridine)[J]. Acta Phys. -Chim. Sin., 2003,19(12): 1133-1137
102. Tian Ye;He Yu;Zhu Yong-Fa;Wang Wei.Hydrothermal Synthesis of MoS2 and Its Lubricating Properties[J]. Acta Phys. -Chim. Sin., 2003,19(11): 1044-1048
103. Jiang Guo-Wei;Yao Lian-Zeng;Jin Chuan-Gui;He Ting;Lin Qing;Cai Wei-Li;Li Xiao-Guang;Yao Zhen.Templated Synthesis and Magnetic Properties of Fe-Co-Ni Ternary Alloy Nanowires[J]. Acta Phys. -Chim. Sin., 2003,19(07): 597-600
104. Zhu Li-Xia;Yue Tao;Gao Shi-Yang;Xia Shu-Ping.Hydrothermal Crystal Growth of Mg(OH)2•2MgSO4•2H2O[J]. Acta Phys. -Chim. Sin., 2003,19(03): 212-215
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106. Yao Su-Wei;Chi Guang-Jun;Cui Lan;Fan Jun;Zhang Wei-Guo;Wang Hong-Zhi.Preparation and Characterization of Fe Nanowire Arrays in Porous Anodic Aluminum[J]. Acta Phys. -Chim. Sin., 2002,18(10): 930-933
107. Wang Yin-Hai;Xu Yan-Qi;Cai Wei-Li;Mo Ji-Mei.A New Method to Prepare CdS Nanowire Arrays[J]. Acta Phys. -Chim. Sin., 2002,18(10): 943-946
108. Chi Guang-Jun;Yao Su-Wei;Fan Jun;Zhang Wei-Guo;Wang Hong-Zhi.Electrochemically Assembled Silver Nanowire Arrays and Its Structural Characterization[J]. Acta Phys. -Chim. Sin., 2002,18(06): 532-535
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