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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2012,Vol.28>> Issue(09)>> 2135-2140     doi: 10.3866/PKU.WHXB201206271         中文摘要
CATALYSIS AND SURFACE SCIENCE
Oxidative Dehydrogenation of Propane to Propylene over Mesoporous Alumina Supported Ni-Co Oxide Catalysts
SUN Yi-Fei, LI Guang-Chao, PAN Xin-Di, HUANG Chuan-Jing, WENG Wei-Zheng, WAN Hui-Lin
State Key Laboratory of Physical Chemistry of Solid Surfaces, National Engineering Laboratory for Green Chemical Productions of Alcohols, Ethers and Esters, Department of Chemistry, College of Chemistry and Chemical Engineering, Xiamen University, Xiamen 361005, Fujian Province, P. R. China
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A series of mesoporous alumina supported nickel oxide, cobalt oxide, and bimetallic nickelcobalt oxide catalysts were synthesized by a one-pot method, using nonionic triblock copolymer as a template and aluminum isopropoxide as the source of aluminum. For comparison, an additional supported Ni-Co oxide catalyst was prepared by impregnation, using mesoporous alumina as the support. The catalysts were tested for the oxidative dehydrogenation of propane, and their structure and properties were characterized by N2 adsorption-desorption, high-resolution transmission electron microscopy (HRTEM), powder X-ray diffraction (XRD), temperature-programmed H2 reduction (H2-TPR), and laser Raman spectroscopy (LRS). All samples synthesized by the one-pot method had large surface area, highly ordered mesoporous structure, and highly dispersed supported oxide species. However, in the sample prepared by impregnation, the mesostructure of the carrier was destroyed with the formation of Co3O4 phase. Among the catalysts studied, the mesoporous alumina supported Ni-Co oxide catalyst from one-pot synthesis showed the best catalytic performance for propane oxidation to propylene. On this catalyst a 10.3% propylene yield was obtained at 450 ° C, C3H8:O2:N2 molar ratio of 1:1:4, and gas hourly space velocity (GHSV) of 10000 mL·h-1·g-1. This result was much higher than the yield of 2.4% obtained from the catalyst prepared by impregnation. Combining the results of characterization and catalytic reaction, the relationship between structure and performance of the catalysts was discussed. The large difference observed in catalytic performance between catalysts prepared by one-pot and impregnation methods was attributed to their different structures, including textural structure, and dispersion of the supported metal oxide species.



Keywords: Propane   Propylene   Oxidative dehydrogenation   Ni-Co oxide catalyst   Mesoporous alumina   One-pot method  
Received: 2012-04-18 Accepted: 2012-06-26 Publication Date (Web): 2012-06-27
Corresponding Authors: HUANG Chuan-Jing, WAN Hui-Lin Email: huangcj@xmu.edu.cn; hlwan@xmu.edu.cn

Fund: The project was supported by the National Key Basic Research Program of China (973) (2010CB732303), National Natural Science Foundation of China (21173173, 21073148, 21033006), Program for Innovative Research Team of the Ministry of Education of China (IRT1036), National Foundation for Fostering Talents of Basic Science, China (J1030415), and Key Scientific Project of Fujian Province, China (2009HZ0002-1).

Cite this article: SUN Yi-Fei, LI Guang-Chao, PAN Xin-Di, HUANG Chuan-Jing, WENG Wei-Zheng, WAN Hui-Lin. Oxidative Dehydrogenation of Propane to Propylene over Mesoporous Alumina Supported Ni-Co Oxide Catalysts[J]. Acta Phys. -Chim. Sin., 2012,28 (09): 2135-2140.    doi: 10.3866/PKU.WHXB201206271

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68. CHEN Zhi-Ping; GAO Bao-Jiao; YANG Xiao-Feng.Adsorption Mechanism of Bilirubin on Aminated Crosslinking Microspheres of PGMA[J]. Acta Phys. -Chim. Sin., 2008,24(08): 1417-1424
69. HUANG Li-Hua; YANG Li-Li; XU Bo-Lian; FAN Yi-Ning.Catalytic Properties of PtSn/Al2O3/MCM-41 Catalysts for Propane Dehydrogenation[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1297-1301
70. XUAN Wei-Min; ZOU Fang; CHEN Lei-Qi; FANG Xue-Ming; LIAN Wei; ZHANG Hui.Mechanism of Absolute Asymmetric Synthesis and Solid-State CD Spectroscopy of BPOB[J]. Acta Phys. -Chim. Sin., 2008,24(06): 955-960
71. LI Jin-Huan; KANG Wan-Li; YAN Wen-Hua; GUO Yi-Hang; GAO Hong-Feng; LIU Zhong-He.Preparation of Eu3+ Doped Titania Nanocrystals and Photocatalytic Degradation Partially Hydrolyzed Polyacrylamide[J]. Acta Phys. -Chim. Sin., 2008,24(06): 1030-1034
72. PEI Su-Peng; ZHANG Bin; JIAO Kun; BAO Ren-Lie; YUE Bin; HE He-Yong.Nanostructured CoMoO4 Supported on Mesoporous SBA-15 for Catalytic Oxidative Dehydrogenation of Propane to Propene[J]. Acta Phys. -Chim. Sin., 2008,24(04): 561-564
73. WANG Fang-Ping; DU Xin-Zhen; WANG Chun; DONG Xiao-Li; CHEN Hui.Synthesis, Characterization and Micellization of Poly(acrylic acid)-g-Octylphenyl Polyoxylethylene Ether[J]. Acta Phys. -Chim. Sin., 2008,24(02): 350-354
74. WANG Jian; GAO Bao-Jiao; GUO Hao-Peng.Adsorption Mechanism of Grafting Particle PMAA/SiO2 for Pirimicarb in Water Medium[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1905-1911
75. ZHANG Lan; ZHANG Shi-Chao.Preparation and Characterization of Poly(acrylonitrile-methoxy polyethylene glycol (350) monoacrylate-lithium acrylate)[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1943-1947
76. YAO Jia; WANG Qing; TONG Da-Jun; LI Hao-Ran.Self-aggregation Behavior of PEG-b-PDMAEMA Copolymers with Different Block Ratios in Aqueous Solution[J]. Acta Phys. -Chim. Sin., 2007,23(10): 1612-1616
77. HE Yi-Ming; YI Xiao-Dong; HUANG Chuan-Jing; YING Fang; ZHANG Xiao-Bing; WENG Wei-Zheng; WAN Hui-Lin.Role of Te on Selective Oxidation of Propane to Acrolein over MoBiTeO/SiO2 Catalysts[J]. Acta Phys. -Chim. Sin., 2007,23(06): 851-855
78. PENG Shun-Jin; ZHAO Lei; WU Li-Min.Surface Properties of Fluorinated Acrylate Polymers Latex Films[J]. Acta Phys. -Chim. Sin., 2007,23(04): 531-536
79. HAO Zhi-Xian;LIU Hui;GUO Bin;LI Hong;ZHANG Jia-Wei;GAN Li-Hua;XU Zi-Jie;CHEN Long-Wu.Sol-Gel Synthesis of Alumina Using Inorganic Salt Precursor[J]. Acta Phys. -Chim. Sin., 2007,23(03): 289-294
80. JIANG Li-Ding;GAO Bao-Jiao;LI Gang.Interaction between Cationic Gemini Surfactant with Hydrophobically Associatied Polyacrylamide of a New Family[J]. Acta Phys. -Chim. Sin., 2007,23(03): 337-342
81. LI Cui-Ping;ZHAO Rui-Hong;GUO Fen;CHEN Jian-Feng.Preparation and Characterization of Ni Catalysts Supported on Organized Mesoporous Alumina[J]. Acta Phys. -Chim. Sin., 2007,23(02): 157-161
82. JIA Long;XU Yong-Fu;GE Mao-Fa;DU Lin;WANG Geng-Chen;ZHUANG Guo-Shun.Kinetic Study of the Gas-phase Ozonolysis of Propylene[J]. Acta Phys. -Chim. Sin., 2006,22(10): 1260-1265
83. JIN Guo-Jie;GUO Yang-Long;LIU Xiao-Hui;YAO Wei;GUO Yun;WANG Yun-Song;YUAN Fang;LU Guan-Zhong.In situ FT-IR Study on the Direct Gas Phase Epoxidation of Propylene over Ag-MoO3 Catalyst[J]. Acta Phys. -Chim. Sin., 2006,22(07): 809-814
84. ZHANG Yi-Wei;ZHOU Yu-Ming;QIU An-Ding;WANG Yu;XU Yi;WU Pei-Cheng.Effect of Na Addition on Catalytic Performance of PtSn/ZSM-5 Catalyst for Propane Dehydrogenation[J]. Acta Phys. -Chim. Sin., 2006,22(06): 672-678
85. YU Ya-Ming;WANG Zhong-Hua;GAO Bao-Jiao;WANG Rui-Xin.Effect of Micellization Behavior of Surface Active Monomer NaAMC14S on Copolymerization Process[J]. Acta Phys. -Chim. Sin., 2006,22(04): 496-501
86. GAN Zhi-ping; GUAN Jian-guo.Chemical Self-assembly Route to Fabricate Hollow Barium Ferrite Submicrospheres[J]. Acta Phys. -Chim. Sin., 2006,22(02): 189-192
87. FENG Jia-Chun; DUAN Yu; JIAO Ying; ZHANG Xiu-Ju; CHEN Ming-Cai.Effect of Lanthanum Complex on Isothermal Crystallization Kinetics of Isotatic Polypropylene[J]. Acta Phys. -Chim. Sin., 2005,21(12): 1431-1435
88. LIU Li-cheng; LI Hui-quan; CAI Wei-quan; ZHANG Yi.Synthesis, Characterization and Catalytic Activity of Mesoporous Cr-MSU-1[J]. Acta Phys. -Chim. Sin., 2005,21(11): 1311-1314
89. TANG Ding-guo; LIU Jian-hong; CI Yun-xiang; QI Lu.Preparation and Performances of a Novel Gel Polymer Electrolyte[J]. Acta Phys. -Chim. Sin., 2005,21(11): 1263-1268
90. LIU Wan-qiang; WANG Xue-ye; LI Xin-fang; LONG Qing-ping; WEN Xiao-hong; LI Jianjun.Quantum Chemistry-ANN Methods Study on Tg of Polyacrylates[J]. Acta Phys. -Chim. Sin., 2005,21(06): 596-601
91. ZHANG Wen-yu; DONG Qing-nian; ZHAO Ning; WEI Wei; SUN Yu-han.The Reaction Mechanism for the Synthesis of 1-methoxy-2-propanol on MgO Catalyst[J]. Acta Phys. -Chim. Sin., 2005,21(06): 653-657
92. ZHANG Kai; FU Qiang; HUANG Yu-hong; ZHOU De-hui.Study on Acrylonitrile Graft Copolymerization on Surfaces of Polystyrene Microspheres[J]. Acta Phys. -Chim. Sin., 2005,21(06): 673-676
93. Zhao Feng;Du Yu-Kou;Li Xing-Chang;Tang Ji-An;Yang Ping.Study on Viscoelastic Properties of Partially Hydrolyzed Polyacrylamide Solution[J]. Acta Phys. -Chim. Sin., 2004,20(11): 1385-1388
94. Zhang Ying;Fang Yu;Lin Shu-Yu;Liu Jing;Yang Juan-Ling.Preparation of Spherical Nano-structured PMAA/CdS Composites by a Microgel Template Method[J]. Acta Phys. -Chim. Sin., 2004,20(08S): 897-901
95. Chen Ming-An;Zhang Xin-Ming;Xie Xuan.Interphase Analysis of Adhesion Bonded Aluminum Sheet/polypropylene and Maleic Anhydride Grafted Polypropylene by XPS[J]. Acta Phys. -Chim. Sin., 2004,20(08): 882-886
96. Wang Zheng-Wu;Li Ying;Li Gan-Zuo;Gu Ming-Yan.Surface Activity and Micellization of LSmn in Aqueous Solution[J]. Acta Phys. -Chim. Sin., 2004,20(08): 816-820
97. Bian Feng-Ling;Liu Ming-Zhu;Sheng Fen-Ling.A Study of Solution Properties of Poly(N-isopropylacrylamide) and Poly(N,N-diethylacrylamide) in Mixed Solvent of Water-Methanol[J]. Acta Phys. -Chim. Sin., 2004,20(04): 337-343
98. Xu Xiao-Ping;Andreas Hüther;Gerd Maurer.Correlation and Prediction of Swelling Behavior of N-isopropyl- acrylamide Based Hydrogels in Aqueous Solution of Acetone[J]. Acta Phys. -Chim. Sin., 2004,20(03): 244-250
99. Lin Mei-Qin;Sun Ai-Jun;Dong Zhao-Xia;Tang Ya-Lin;Li Ming-Yuan;Wu Zhao-Liang.Study on Properties of the Linked Polymer Solution with Low Polymer Concentration[J]. Acta Phys. -Chim. Sin., 2004,20(03): 285-289
100. Yi Xiao-Dong;Lin Hong;He Yi-Ming;Huang Chuan-Jing;Weng Wei-Zheng;Wan Hui-Lin.Selective Oxidation of Propane over Mo-V-Zr-O Catalysts[J]. Acta Phys. -Chim. Sin., 2004,20(03): 309-312
101. Dong Xiang-Ting;He Ying;Yan Jing-Hui;Xue Bo-Fei;Feng Xiu-Li;Hong Guang-Yan.Preparation and Characterization of Nanosized AgBr/PMMA Photochromic Hybrid Material[J]. Acta Phys. -Chim. Sin., 2003,19(12): 1159-1162
102. Chen Hong;Han Li-Juan;Xu Peng;Luo Ping-Ya.The Thickening Mechanism Study of Hydrophobically Modified Polyacrylamide[J]. Acta Phys. -Chim. Sin., 2003,19(11): 1020-1024
103. Zhang Xin;Wan Hui-Lin;Weng Wei-Zheng;Yang Le-Fu;Yi Xiao-Dong.Role of Ce on Selective Oxidation of Propane to Acrolein over Ce-Ag-Mo-P-O Catalysts[J]. Acta Phys. -Chim. Sin., 2003,19(06): 492-497
104. Zhang Sheng-Mao;Zhang Zhi-Jun;Dang Hong-Xin;Liu Wei-Min;Xue Qun-Ji.Preparation and Characterization of TiO2/Poly(butyl acrylate) Nanocomposite Film[J]. Acta Phys. -Chim. Sin., 2003,19(02): 171-173
105. Zhang Xin;Wan Hui-Lin;Weng Wei-Zheng;Yi Xiao-Dong.The Effect of MoO3 in Ag-Mo-P-O Catalysts on Oxidative Dehydrogenation of Propane[J]. Acta Phys. -Chim. Sin., 2002,18(10): 878-883
106. Bian Feng-Ling;Liu Ming-Zhu.The Temperature Dependence of the Viscosity of Poly (N,N-diethylacrylamide) Solutions[J]. Acta Phys. -Chim. Sin., 2002,18(09): 776-780
107. Pu Min;Wang Hai-Xia;Feng Xiao;Wu Dong;Sun Yu-Han.Research on the Rotation Rearrangement of C=C Double Bond of 3-Hydroxy Acrolein by Density Function Theory[J]. Acta Phys. -Chim. Sin., 2002,18(06): 522-526
108. Wang Zhan-Liang;Tang Zhi-Yuan;Geng Xin;Xue Jian-Jun.Research on Novel PMMAbased Gel Electrolyte for Lithium Ion Battery[J]. Acta Phys. -Chim. Sin., 2002,18(03): 272-275
109. Zhao-Ri Ge-Tu;Li Wen-Zhao;Yu Chun-Ying;Xu Heng-Yong;Kieffer,Roger.Propane Oxidative Dehydrogenation on Molybdenum Doped LaVO4 Catalyst[J]. Acta Phys. -Chim. Sin., 2002,18(01): 1-4
110. Yin Yi-Qing;Fang Yu;Hu Dao-Dao;Gao Gai-Ling.Fluorescence Properties of N-vinylcarbazole Labeled Methacrylic Acid-Acenaphthylene Copolymers[J]. Acta Phys. -Chim. Sin., 2001,17(09): 776-780
111. Xie Jian-Chun;Luo Hong-Peng;Zhu Li-Li;Zhou Li;Li Chong-Xi;Xu Xiao-Jie.Extracting Active Compounds from Herbs Using Molecular Imprinting Technology[J]. Acta Phys. -Chim. Sin., 2001,17(07): 582-585
112. Tao Yue-Wu;Zhong Shun-He.Laser Stimulated Isobutane Selective Oxidation Reaction on the Surface of Li and Bi Mixed Phosphate[J]. Acta Phys. -Chim. Sin., 2001,17(04): 356-360
113. Lu An-Hui;Li Wen-Cui;Zheng Jing-Tang.Preparation of PANbased Molecular Sieve ACF and Study of Surface Structure by XPS[J]. Acta Phys. -Chim. Sin., 2001,17(03): 216-221
114. Zhang Tian-Li;Yan Ji-Min;Kong Fan-Ao.Quasiclassical Trajectory Study of Reaction of Chlorine Substituting the Primary Hydrogen of Propane[J]. Acta Phys. -Chim. Sin., 2001,17(02): 119-122
115. Zhao Ri-GeTu, Ge Qing-Jie, Li Wen-Zhao, Yu Chun-Ying, Jia Mei-Lin, Xu Heng-Yong.In Situ Electrical Conductivity Study of Ni-V-O Catalysts Used in Oxidative Dehydrogenation of Propane[J]. Acta Phys. -Chim. Sin., 2000,16(09): 798-803
116. Liu Fu-Yi, Li Cheng-Xiang, Gao Hui, Sheng Liu-Si, Zhang Yun-Wu.Photoionization of Epichlorohydrin by Synchrotron Radiation[J]. Acta Phys. -Chim. Sin., 2000,16(08): 758-763
117. Liu Shou-Xin, Fang Yu, Hu Dao-Dao, Lv Hong-Wang.Complexation between Poly(methacrylic acid) and Cationically Modified Polyacrylamide[J]. Acta Phys. -Chim. Sin., 2000,16(03): 214-220
118. Zhang Wen-Min, Wu Qi, Wei Tao, Liu Zhan-Hua.Preparation of High Content Surfactant-free Narrowly Distributed Macromolecule Nanoparticle Latex[J]. Acta Phys. -Chim. Sin., 2000,16(02): 116-120
119. Dai Le-Rong, Su Xiao-Yan, Chen Hui-Ying, Wu Pei-Qiang.Lyotropic Liquid Crystal of Poly(Sodium Sulfoalky Methacrylate)[J]. Acta Phys. -Chim. Sin., 1999,15(12): 1060-1063
120. Zhang Tian-Li, Xu Li-Jin, Yan Ji-Min, Kong Fan-Ao.A Quasiclassical Trajectory Study for Reaction of Chlorine with Propane[J]. Acta Phys. -Chim. Sin., 1999,15(11): 1045-1048
121. Cao Wan-Qiang, Li Jing-De.Effect of Polarization Cooling in Polypropylene[J]. Acta Phys. -Chim. Sin., 1999,15(10): 943-947
122. Chen Ming-Shu, Weng Wei-Zheng, Wan Hui-Lin.Mechanism of Propane and iso-butane Oxidehydrogenation on VMgO Catalyst[J]. Acta Phys. -Chim. Sin., 1999,15(10): 938-942
123. Liu Fu-Yi, Sheng Liu-Si, Qi Fei, Wu Guo-Hua, Gao Hui, Zhou Wei-Dong, Zhang Yun-Wu.Photoionization/Dissociation Channels and Mechanism of 1,2-Propylene Oxide[J]. Acta Phys. -Chim. Sin., 1999,15(09): 845-849
124. Zhai Mu-Heng, Zhang Wen-Min, Sheng En-Hong, Fu Zhong, Zhang Feng.Preparation of Monodispersed Macromolecule Microspheres by Microwve Irradiation and Research on the Mechanism of Its Formation[J]. Acta Phys. -Chim. Sin., 1999,15(08): 747-751
125. Chen Tong, Li Wen-Zhao, Yu Chun-Ying.Investigation of the Interaction between NiO and Support,γ-Al2O3,for Oxidative Dehydrogenation of Ethane[J]. Acta Phys. -Chim. Sin., 1999,15(07): 613-618
126. He Li-Zhen, Chen Guang-Ju, Liu Ruo-Zhang.Investigation of the Thermal Reaction of Propene Forming Methylcyclopentane[J]. Acta Phys. -Chim. Sin., 1999,15(04): 308-312
127. Chen Li-Tao, Chen Guang-Ju, Fu Xiao-Yuan.AM1 Studies of Two Pathways of Vinylacetylene React with Nitric Oxide[J]. Acta Phys. -Chim. Sin., 1998,14(11): 1001-1006
128. Tang Yong-Zheng, Tang Ye-Cang, Luo Shi-Zhong, Fu Zhong, Zhang Wen-Min.Microwave Preparation of Narrowly Distributed Surfactant-free Macromolecular Nanospheres[J]. Acta Phys. -Chim. Sin., 1998,14(07): 620-623
129. Zeng Jin-Long, Xiong Zhi-Tao, Lin Guo-Dong, Yu La-Jia, Zhang Hong-Bin.Spectroscopic Characterization of Mo/HZSM-5-based Catalysts for Dehydro-aromatization of Methane[J]. Acta Phys. -Chim. Sin., 1998,14(05): 394-400
130. Hu Hai-Quan, Liu Cheng-Bu.Mechanism of the Isomerization of Difluorosilacyclopropene[J]. Acta Phys. -Chim. Sin., 1998,14(04): 349-352
131. Wang Xin-Ping, Zhang Jia-Yun, Tang Ji-An, Jiang Long.Interfacial Rheology Investigation of Polyacrylamide-Surfactant Interactions[J]. Acta Phys. -Chim. Sin., 1998,14(01): 88-92
132. Qian Ying,Wang Yan,Feng Wen-Lin,Liu Ruo-Zhuang.Theoretical Calculation on the Canonical Rate Constants for the Addition Reaction of 1,3-cyclohexa-diene with Propylene[J]. Acta Phys. -Chim. Sin., 1997,13(12): 1084-1089
133. Zhang Yu,Wu Fan-Xin,Zhang Hong-Bin,Lin Guo-Dong,Yuan You-Z.Hydroformylation of Propene over Carbon Nanotubes-Supported Rh-Catalyst[J]. Acta Phys. -Chim. Sin., 1997,13(12): 1057-1060
134. Cao Wan-Qiang,Wang Yong,Liu Jun-Diao,Xiao Zhong-Mo,Li Jing-De.The Frozen and Thermally Stimulated Polarization in Polymer[J]. Acta Phys. -Chim. Sin., 1997,13(10): 921-924
135. Jiang Kui-Yang,Zhang Jun,Gui Lin-Lin.Synthesis and Characterization of PMMA-ZrO2(SiO2,TiO2,Al2O3) Organic-Inorganic Hybrid Materials[J]. Acta Phys. -Chim. Sin., 1997,13(05): 407-412
136. Guan Jian-Guo,Zhao Su-Ling,Xie Hong-Quan.The Temperature and Electric Field Dependence of Properties for Hydrous Electrorheological Fluid-Lithium Polymethacrylate[J]. Acta Phys. -Chim. Sin., 1997,13(03): 242-246
137. Cao Wan-Qiang,Wang Yong,Li Jing-De.Thermally Stimulated Current of Polypropylene in Equilibrium and Non-equilibrium State[J]. Acta Phys. -Chim. Sin., 1996,12(12): 1090-1093
138. Shao Guo-Quan,Fang Wei-Hai,Chen Guang-Ju,Liu Ruo-Zhuang.Theoretical Study on Decarbonylation Reaction of Acrolein and Its Derivatives in Their Electronic Ground States[J]. Acta Phys. -Chim. Sin., 1996,12(09): 830-835
139. Cheng Mo-Jie,Yang Ya-Shu.Effect of High Temperature Water Steaming on the Active Centers of ZnHZSM-5[J]. Acta Phys. -Chim. Sin., 1996,12(08): 721-726
140. Zhang Jun,Luo Sheng-Cheng,Gui Lin-Lin,Tang You-Qi.Synthesisi and Characterization of New PMMA-TiO2 Organic-Lnorganic Hybrid Glasses[J]. Acta Phys. -Chim. Sin., 1996,12(04): 289-292
141. Cao Rong,Hou Zhen-Shan,Zhao Hong,He Di-Jing,Chen Wen-Hai.Propane Aromatization over Pt-Ga/HZSM-5 Catalyst[J]. Acta Phys. -Chim. Sin., 1996,12(02): 114-118
142. Liu Mu-Xin.Xu Gui-Ying.Li Gan-Zuo.Mao Hong-Zhi.Li Fang.The Transient Interfacial Tension between Oleic Acid-sodium Oleate Aqueous Solution and Crude Oil[J]. Acta Phys. -Chim. Sin., 1995,11(11): 1040-1043
143. Zhang Bang-Hua, Li Chuan-Gang, Song Mou-Dao, Zhou Qing-Ye, Hao Guang-Jie, Zhang Ying.Study on the Miscibility of PVC/PBD-b-PMMA Blends[J]. Acta Phys. -Chim. Sin., 1995,11(09): 807-811
144. Cheng Mo-Jie,Wang Jiang-Mai,Yang Ya-Shu,Li Can.The Study of Propane Aromatization over ZnHZSM-5:Activation of Propane[J]. Acta Phys. -Chim. Sin., 1995,11(08): 724-729
145. Xu Gui-Ying, Su Hong-Mei, Li Gan-Zuo, Liu Mu-Xin, Li Fang, Mao Hong-Zhi.The Interaction between Polyacrylamide and Mixed Surfactants[J]. Acta Phys. -Chim. Sin., 1994,10(10): 909-914
146. She Li-Qin, Zhu Gao-Zhong, Wen Rui-Wu, Zhang Chang-Jun, Li Xuan-Wen, Liu Xing-Yun.Formation and Characterization of Ga Active Site in GaZSM-5 Zeolite[J]. Acta Phys. -Chim. Sin., 1994,10(07): 628-634
147. Xie Zhi-Ming; Gao Pian; Li Zhuo-Mei.Study on the Stability of Soap-free Water-Solubilized Polyacrylic Colloidal Dispersions[J]. Acta Phys. -Chim. Sin., 1994,10(05): 438-443
148. She Li-Qin, Wang Duo-Cai, Li Xuan-Wen, Liu Xing-Yun, Han Ming.The States of Zinc in ZnZSM-5 Zeolites and their Catalysis[J]. Acta Phys. -Chim. Sin., 1994,10(03): 247-253
149. Huang Wei-Jun, Chen Su-Ming, Tan Fu, Yang Zhen-Xiang.Study on Thermodynamic Characteristics of Cinnamic Acid Derivatives[J]. Acta Phys. -Chim. Sin., 1994,10(02): 151-153
150. Yang Li-Ying, Chen Shu, Xu Wen-Qing, Li Guo-Ying, YIN Yuan-Gen.Identification of γ-Fe2O3 in Ferrite-ferric Oxide Catalysts Using Second Derivative IR Spectra[J]. Acta Phys. -Chim. Sin., 1994,10(02): 164-167
151. Ji Yong-Qiang, Fu Xiao-Yuan.Theoretical Study on the Thermal Decomposition of 2-nitropropene[J]. Acta Phys. -Chim. Sin., 1994,10(01): 22-25
152. Fang Wei-Hai; Fang De-Cai; Liu Ruo-Zhuang.AM1 Study of the Photodecarboxylation Reaction of Acrylic acid in the Gas Phase[J]. Acta Phys. -Chim. Sin., 1993,9(06): 788-790
153. Luo Yun-Xia; Yang Hong; Yu Bin; Ding Meng-Xian; Jiang Bing-Zheng.The Effect of Mobility of Molecules on Radiation-induced Chain Scission and Racemization of iso-Poly(Methyl Methacrylate)[J]. Acta Phys. -Chim. Sin., 1993,9(05): 604-609
154. Fang Wei-Hai; Fang De-Cai; Liu Ruo-Zhuang.Theoretical Study of Pyrolysis Mechanisms of Acrylic acid in the Gas Phase[J]. Acta Phys. -Chim. Sin., 1993,9(05): 630-634
155. Liao Jian-Hui; Liu Li-Zhi; Wang Guo-Ying; Jiang Bing-Zheng.The Compatibility and Crystallization of the Mixtures of Poly (Tetrahydrofuran-b-methyl methacrylate) Diblock Copolymer with Polyvinyl Chloride Homopolymer[J]. Acta Phys. -Chim. Sin., 1993,9(05): 657-662
156. Zhang Qing-Da; Li Zhuo-Mei.Study on the Dissociation of A New Cationic Polyacrylamide[J]. Acta Phys. -Chim. Sin., 1993,9(05): 679-683
157. Xu Gui-Ying; Gu Ying-Hui; Zeng Li-Rong; Zhu He-Ping; Mao Hong-Zhi.Study of the Interaction Between Polyacrylamide and Sodium Dodecyl Sulfonate by Viscosity Method[J]. Acta Phys. -Chim. Sin., 1992,8(03): 352-357
158. Song Mo; Liang Hao-Jun; Chen Yi-Yi; Jiang Bing-Zheng.Investigation of Phase Separation Behavior in Poly (Methyl Methacrylate)/Poly (Styrene-CO-Acrylonitrile) Mixtures With Pulsed Nuclear Magnetic Resonance[J]. Acta Phys. -Chim. Sin., 1991,7(05): 513-517
159. Bai Tong-Chun; Wang Jian-Ji; Liu Wen-Bin; Lu Jin-Suo.Study on the Salt Effect in Nonaqueous Solutions by Gas Liquid Chromatography——For Nonelectrolyte Solute (Hydrocarbons,Aromatic Hydrocarbons,Chloro-Hydrocarbons,Ketones) in Salt (Nal, NaSCN, KSCN) and Propy-Lene Carbonate Solutions[J]. Acta Phys. -Chim. Sin., 1991,7(04): 480-484
160. Du Qi-Shi; Du Lei.The H-F Force Method to Describe the MO'S Bonding Property[J]. Acta Phys. -Chim. Sin., 1991,7(02): 140-145
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