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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2013,Vol.29>> Issue(01)>> 95-101     doi: 10.3866/PKU.WHXB201209272         中文摘要
ELECTROCHEMISTRY AND NEW ENERGY
Preparation and Characterization of Core-Shell Co@Pt/C Catalysts for Fuel Cell
CAO Chun-Hui1,2, LIN Rui1,2, ZHAO Tian-Tian1,2, HUANG Zhen1,2, MA Jian-Xin1,2
1 Clean Energy Automotive Engineering Center, Tongji University, Shanghai 201804, P. R. China;
2 School of Automotive Studies, Tongji University, Shanghai 201804, P. R. China
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Co@Pt/C core-shell catalysts have been synthesized by a two-step chemical reduction method, followed by heat treatment in a H2 and N2 mixture. High resolution transmission electron microscopy (HR-TEM) and X-ray photoelectron spectroscopy (XPS) techniques were used to characterize the catalyst microstructure and morphology. The results indicate that the core-shell structure of Co rich in core and Pt rich in shell is formed and the nano-particles are highly dispersed on the surface of the carbon support. Heat treatment affects the structure and morphology of the catalysts. The electrocatalytic performance, kinetic characteristics of O2 reduction reaction (ORR), and durability of the catalysts were measured by cyclic voltammetry (CV) and linear sweep voltammetry (LSV) techniques. It was found that the formation of the core-shell structure is favorable for improving the performance and utilization of Pt. The Co@Pt/C catalyst mechanism proceeds by an approximately four-electron pathway in acid solution, through which molecular oxygen is directly reduced to water. Compared with alloy catalysts, the formation of the core-shell structure obviously improves the catalyst durability.



Keywords: Fuel cell   Core-shell structure Co@Pt/C catalyst   Electrochemical performance   Reaction kinetic   Durability  
Received: 2012-07-11 Accepted: 2012-09-26 Publication Date (Web): 2012-09-27
Corresponding Authors: Email: ruilin@tongji.edu.cn; jxma@tongji.edu.cn

Fund: The project was supported by the National Natural Science Foundation of China (21276199), Program for Young Excellent Talents in Tongji University, China (2006KJ022), Shanghai Leading Academic Discipline Project, China (B303), and Energy Saving and Environmental Protection Automobile Innovation“111 Project”(B08019).

Cite this article: CAO Chun-Hui, LIN Rui, ZHAO Tian-Tian, HUANG Zhen, MA Jian-Xin. Preparation and Characterization of Core-Shell Co@Pt/C Catalysts for Fuel Cell[J]. Acta Phys. -Chim. Sin., 2013,29 (01): 95-101.    doi: 10.3866/PKU.WHXB201209272

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69. ZHANG Xiao-Yan, SUN Ming-Xuan, SUN Yu-Jun, LI Jing, SONG Peng, SUN Tong, CUI Xiao-Li.Photoelectrochemical Properties of Graphene Oxide Thin Film Electrodes[J]. Acta Phys. -Chim. Sin., 2011,27(12): 2831-2835
70. LI Qing-Wu, WEI Zi-Dong, CHEN Si-Guo, QI Xue-Qiang, LIU Xiao, DING Wei, MAYu.PtSnCo/C Anode Catalyst for Methanol Oxidation[J]. Acta Phys. -Chim. Sin., 2011,27(12): 2857-2862
71. LIU Li, TIAN Fang-Hua, WANG Xian-You, ZHOU Meng.Electrochemical Behavior of LiV3O8 in Aqueous Li2SO4 Solution[J]. Acta Phys. -Chim. Sin., 2011,27(11): 2600-2604
72. DANG Dai, GAO Hai-Li, PENG Liang-Jin, SU Yun-Lan, LIAO Shi-Jun, WANG Ye.Preparation of High Performance Core-Shell PdRu@Pt/CNT Electrocatalyst[J]. Acta Phys. -Chim. Sin., 2011,27(10): 2379-2384
73. XU Li, QIAO Jin-Li, DING Lei, HU Long-Yu, LIU Ling-Ling, WANG Hai-Jiang.Electrocatalytic Activity of CoPy/C Catalyst for the Oxygen Reduction Reaction in Alkaline Electrolyte[J]. Acta Phys. -Chim. Sin., 2011,27(10): 2251-2254
74. FU Rong, ZHENG Jun-Sheng, WANG Xi-Zhao, MA Jian-Xin.Effect of the Reduction Heat-Treatment Condition on the Performance of Pt-Fe/C Alloy Catalyst[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2141-2147
75. YAN Hui, ZHANG Huan, ZHANG Ding, ZHU Zhi, QI Lu.Hydrothermal Synthesis of Spherical Li4Ti5O12 as Anode Material for High Power Lithium-Ion Secondary Battery[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2118-2122
76. PENG Tian-You, KE Ding-Ning, ZENG Peng, ZHANG Xiao-Hu, FAN Ke.Preparation and Photoelectrochemical Performance of BiVO4 Film Electrode[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2160-2166
77. WANG Xi-Zhao, FU Rong, ZHENG Jun-Sheng, Ma Jian-Xin.Platinum Nanoparticles Supported on Carbon Nanofibers as Anode Electrocatalysts for Proton Exchange Membrane Fuel Cells[J]. Acta Phys. -Chim. Sin., 2011,27(08): 1875-1880
78. WEN Sheng, GONG Chun-Li, TSAI Fang-Chang, YEH Jen-Taut.Properties of SPES/AlOOH Composite Proton Exchange Membranes[J]. Acta Phys. -Chim. Sin., 2011,27(08): 1886-1892
79. ZHANG Min, LI Jing-Jian, PAN Mu, XU Dong-Sheng.Catalytic Performance of Pt Nanowire Arrays for Oxygen Reduction[J]. Acta Phys. -Chim. Sin., 2011,27(07): 1685-1688
80. HUANG Ying-Heng, TONG Zhang-Fa, WEI Teng-You, LI Bin.Reaction Kinetics of the Intermediate in Synthesis of LiCoPO4 by Solid-State Reaction[J]. Acta Phys. -Chim. Sin., 2011,27(06): 1325-1334
81. LI Yun-Xia, WEI Zi-Dong, ZHAO Qiao-Ling, DING Wei, ZHANG Qian, CHEN Si-Guo.Preparation of Pt/Graphene Catalyst and Its Catalytic Performance for Oxygen Reduction[J]. Acta Phys. -Chim. Sin., 2011,27(04): 858-862
82. LIU Chun-Yan, XU Bin, TANG Ya-Wen, CAO Gao-Ping, YANG Yu-Sheng, LU Tian-Hong.Electrocatalytic Performance of Pd Catalyst Supported on Macropore Carbon for Oxidation of Formic Acid[J]. Acta Phys. -Chim. Sin., 2011,27(03): 604-608
83. AN Ting, ZHAO Feng-Qi, YI Jian-Hua, FAN Xue-Zhong, GAO Hong-Xu, HAO Hai-Xia, WANG Xiao-Hong, HU Rong-Zu, PEI Qing.Preparation, Characterization, Decomposition Mechanism and Non-Isothermal Decomposition Reaction Kinetics of the Super Thermite Al/CuO Precursor[J]. Acta Phys. -Chim. Sin., 2011,27(02): 281-288
84. WANG Xi-Zhao, ZHENG Jun-Sheng, FU Rong, MA Jian-Xin.Pulse-Microwave Assisted Chemical Reduction Synthesis of Pt/C Catalyst and Its Electrocatalytic Oxygen Reduction Activity[J]. Acta Phys. -Chim. Sin., 2011,27(01): 85-90
85. ZHAO Yan-Chun, ZHAN Lu, TIAN Jian-Niao, NIE Su-Lian, NING Zhen.N-Doped Amorphous Carbon Supported Pd Catalysts for Methanol Electrocatalytic Oxidation[J]. Acta Phys. -Chim. Sin., 2011,27(01): 91-96
86. DENG An-Qiang, FAN Jing-Bo, QIAN Ke-Nong, LUO Yong-Chun.Effect of Heat Treatment on the Structure and Properties of La4MgNi19 Hydrogen Storage Electrode Alloys[J]. Acta Phys. -Chim. Sin., 2011,27(01): 103-107
87. ZHANG Lei-Yong, HE Shui-Jian, CHEN Shui-Liang, GUO Qiao-Hui, HOU Hao-Qing.Preparation and Electrochemical Properties of Polyaniline/Carbon Nanofiber Composite Materials[J]. Acta Phys. -Chim. Sin., 2010,26(12): 3181-3186
88. LI Huan-Zhi, TANG Ya-Wen, LU Tian-Hong.Effect of NH4+ on the Electrocatalytic Performance of Carbon Supported Pd Catalyst for Formic Acid Oxidation[J]. Acta Phys. -Chim. Sin., 2010,26(12): 3199-3202
89. GAO Hai-Li, LIAO Shi-Jun, ZENG Jian-Huang, LIANG Zhen-Xing, XIE Yi-Chun.Preparation and Characterization of Platinum-Decorated Ru/C Catalyst with High Performance and Superior Poison Tolerance[J]. Acta Phys. -Chim. Sin., 2010,26(12): 3193-3198
90. ZHANG Qiao-Bao, FENG Zeng-Fang, HAN Nan-Nan, LIN Ling-Ling, ZHOU Jian-Zhang, LIN Zhong-Hua.Preparation and Photoeletrochemical Performance of CdS Quantum Dot Sensitized ZnO Nanorod Array Electrodes[J]. Acta Phys. -Chim. Sin., 2010,26(11): 2927-2934
91. GONG Chun-Li, ZHOU Yi, YAN Li-Cheng, WEN Sheng, ZHENG Gen-Wen.Properties of SPES/PWA/SiO2 Composite Proton Exchange Membranes[J]. Acta Phys. -Chim. Sin., 2010,26(11): 2967-2974
92. LUO Yong-Chun, ZHANG Tie-Jun, WANG Duo, KANG Long.Influence of Ball-Milling on Hydrogen Storage and Electrochemical Properties of (Ti Cr)0.497V0.42Fe0.083/30%(w) (LaRMg)(NiCoAl)3.5 Alloy Electrodes[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2397-2404
93. YANG Su-Xia, LI Yuan, LIU Zhi-Ping, YANG Shu-Qin, HAN Shu-Min.Effect of Partial Substitution of Cu by Fe on the Phase Structure and Electrochemical Property of Low-Co AB5 Type Hydrogen Storage Alloys[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2144-2150
94. ZHAO Yan-Chun, LAN Huang-Xian, DENG Bin-Bin, TIAN Jian-Niao, YANG Xiu-Lin, WANG Feng-Yang.Electrocatalytic Oxidation of Methanol with Poly Functionalized Multiwalled Carbon Nanotubes Supported Pt Catalysts[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2255-2260
95. TANG Yu-Bao, LIU Jiang.Fueling Solid Oxide Fuel Cells with Activated Carbon[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1191-1194
96. AN Xiao-Sha, CHEN De-Jun, ZHOU Zhi-You, WANG Qiang, FAN You-Jun, SUN Shi-Gang.Rare Earth Eu Doped PtRu/C Catalysts and Their Properties for Methanol Electrooxidation[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1207-1213
97. ZONG Wei-Zheng, ZHU Yong-Fa.Preparation of Single-Chamber Solid Oxide Fuel Cell by Co-Pressing and Direct Forming Process[J]. Acta Phys. -Chim. Sin., 2010,26(04): 827-832
98. WU Yan-Ni, LIAO Shi-Jun.Shortened Carbon Nanotubes as Supports to Prepare High-Performance Pt/SCNT and PtRu/SCNT Catalysts for Fuel Cells[J]. Acta Phys. -Chim. Sin., 2010,26(03): 669-674
99. LEI Ze, ZHU Qing-Shan, HAN Min-Fang.Fabrication and Performance of Direct Methane SOFC with a Cu-CeO2-Based Anode[J]. Acta Phys. -Chim. Sin., 2010,26(03): 583-588
100. LIANG Peng, XU Hong-Feng, LIU Ming, LU Lu, FU Jie.Electrochemical Performance Testing and Characterization of Silver-Plated and Graphite-Coated 316L Stainless Steel Bipolar Plates[J]. Acta Phys. -Chim. Sin., 2010,26(03): 595-600
101. JIANG Lei, HUANG Hui, WANG Chun-Tao, ZHANG Wen-Kui, GAN Yong-Ping, TAO Xin-Yong.Photoelectrochromic Properties of TiO2-xNx/NiO Bilayer Thin Films[J]. Acta Phys. -Chim. Sin., 2010,26(02): 299-303
102. GAO Yin-Yi, CAO Dian-Xue, WANG Gui-Ling, YIN Cui-Lei.Catalytic Behavior of NiCo2O4 for H2O2 Electroreduction in Alkaline Medium[J]. Acta Phys. -Chim. Sin., 2010,26(01): 29-33
103. WANG Wei-Kun, ZHANG Yong-Yong, WANG An-Bang, YU Zhong-Bao, HAN Min-Fang, YANG Yu-Sheng.Electrochemical Performance of 1,4,5,8-Tetrahydroxy-9,10-anthraquinone as Cathode Material in Lithium Batteries[J]. Acta Phys. -Chim. Sin., 2010,26(01): 47-50
104. LU Hua-Quan, WU Feng, SU Yue-Feng, LI Ning, CHEN Shi, BAO Li-Ying.Electrochemical Performance of LiNi0.5Mn0.5O2 as Cathode Material for Lithium-Ion Batteries Prepared by Oxalate Co-Precipitation Method[J]. Acta Phys. -Chim. Sin., 2010,26(01): 51-56
105. YANG Gai-Xiu, CHEN Ting-Ting, TANG Ya-Wen, LU Tian-Hong.Electrocatalytic Performance of Silicotungstic Acid Modified Carbon Supported Pd Catalyst for Oxidation of Fomic Acid[J]. Acta Phys. -Chim. Sin., 2009,25(12): 2450-2454
106. SUN Zhe, LIU Kai-Yu, ZHANG Hai-Feng, LI Ao-Sheng, XU Xiao-Cun.Study on Meso-C/MnO2 Asymmetric Supercapacitors[J]. Acta Phys. -Chim. Sin., 2009,25(10): 1991-1997
107. FANG Xiang, SHEN Pei-Kang.Mechanism of Ethanol Electrooxidation on Pd Electrode[J]. Acta Phys. -Chim. Sin., 2009,25(09): 1933-1938
108. SU Zhi, XU Mao-Wen, YE Shi-Hai, WANG Yong-Long.Doping of Layered LiMnO2 as Cathode Materials for Lithium-Ion Batteries and Their Electrochemical Properties[J]. Acta Phys. -Chim. Sin., 2009,25(06): 1232-1238
109. FAN You-Jun, ZHEN Chun-Hua, CHEN Sheng-Pei, SUN Shi-Gang.Effect of Specific Adsorption of Anions and Surface Structure of Pt(111) Electrode on Kinetics of Dissociative Adsorption of Ethylene Glycol[J]. Acta Phys. -Chim. Sin., 2009,25(05): 999-1003
110. GAO Hong-Quan, LAI Yan-Qing, ZHANG Zhi-An, LIU Ye-Xiang.Electrochemical Behaviors of New Lithium Salt LiBC2O4F2 in EC+DMC Solvents[J]. Acta Phys. -Chim. Sin., 2009,25(05): 905-910
111. WANG Jian-She, GUO Xun, SONG Cheng-Ying, WANG Liu-Cheng, ZHAO Jian-Hong, QIU Xin-Ping.Promoting Methanol Electro-Oxidation through Fabricating Pore Structure in Pt/CNTs Catalyst Layer by Dissolving Away Premixed La2O3 Particles[J]. Acta Phys. -Chim. Sin., 2009,25(04): 767-772
112. DU Bing, JIANG Qi, ZHAO Xiao-Feng, LIN Sun-Zhong, MU Pei-Shan, ZHAO Yong.Preparation of PPy/CNTs Composite Based on the Electrostatic Absorption Effect[J]. Acta Phys. -Chim. Sin., 2009,25(03): 513-518
113. ZHENG Gen-Wen, GONG Chun-Li, WEN Sheng, ZHOU Huan-Bo, XIE Xiao-Lin.Preparation and Properties of Sulfonated Poly(ether sulfone)/Boron Phosphate Composite Proton Exchange Membranes[J]. Acta Phys. -Chim. Sin., 2009,25(03): 575-582
114. JIA Yan-Min; LIU Fei-Ye; XIAO Xue-Zhang; HANG Zhou-Ming; LEI Yong-Quan; CHEN Li-Xin.Microstructure and Electrochemical Properties of V2.1TiNi0.4Zr0.06Cu0.03M0.10 (M=Cr, Co, Fe, Nb, Ta) Hydrogen Storage Alloys[J]. Acta Phys. -Chim. Sin., 2009,25(02): 247-252
115. KE Xi; CUI Guo-Feng; SHEN Pei-Kang.Stability of Pd-Fe Alloy Catalysts[J]. Acta Phys. -Chim. Sin., 2009,25(02): 213-217
116. ZHANG Heng, ZHAO Feng-Qi, YI Jian-Hua, ZHANG Xiao-Hong, HU Rong-Zu, XU Si-Yu, REN Xiao-Ning.Preparation, Thermal Behavior and Non-isothermal Decomposition Reaction Kinetics of Zr(3-NO2-PHT)2·2H2O[J]. Acta Phys. -Chim. Sin., 2008,24(12): 2263-2267
117. ZHANG Wei; CUI Xiao-Li; JIANG Zhi-Yu.Effect of Composite Modes on Photoelectrochemical Properties of MWCNTs/TiO2 Nanocomposite Films[J]. Acta Phys. -Chim. Sin., 2008,24(11): 1975-1980
118. LIU Fei-Ye; CHEN Li-Xin; LI Lu; JIA Yan-Min; LEI Yong-Quan.Microstructure and Electrochemical Properties of V2.1TiNi0.4Zr0.06Cux (x=0-0.12) Hydrogen Storage Alloys[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1694-1698
119. JIANG Qi; ZHANG Qian; DU Bing; ZHAO Xiao-Feng; ZHAO Yong.Preparation and Electrochemical Properties of CNTs-PANI Composite Material via Finite Field Polymerization[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1719-1723
120. XU Si-Yu; ZHAO Feng-Qi; YI Jian-Hua; HU Rong-Zu; GAO Hong-Xu; LI Shang-Wen; HAO Hai-Xia; PEI Qing.Thermal Behavior and Non-Isothermal Decomposition Reaction Kinetics of Composite Modified Double Base Propellant Containing CL-20[J]. Acta Phys. -Chim. Sin., 2008,24(08): 1371-1377
121. WEN Qing; LIU Zhi-Min; CHEN Ye; LI Kai-Feng; ZHU Ning-Zheng.Electrochemical Performance of Microbial Fuel Cell with Air-Cathode[J]. Acta Phys. -Chim. Sin., 2008,24(06): 1063-1067
122. WANG Lin; CHEN Shun-Quan; LIU Yuan.NiO/LaMnO3 Catalysts for Steam Reforming of Ethanol[J]. Acta Phys. -Chim. Sin., 2008,24(05): 849-854
123. ZHENG Gen-Wen; GONG Chun-Li; WEN Sheng; XIE Xiao-Lin.Preparation and Performances of Sulfonated Poly(ether imide) and Poly (ether sulfone) Blends for Proton Exchange Membrane[J]. Acta Phys. -Chim. Sin., 2008,24(05): 855-860
124. FAN Mao-Song; LEI Xiang-Li; WU Ning-Ning; QI Lu.Electrochemical Performance of LiMn2O4 Power Battery[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 36-39
125. YI Jian-Hua; ZHAO Feng-Qi; XU Si-Yu; GAO Hong-Xu; HU Rong-Zu; HAO Hai-Xia; PEI Qing; GAO Yin.Nonisothermal Thermal Decomposition Reaction Kinetics of Double-base Propellant Catalyzed with Lanthanum Citrate[J]. Acta Phys. -Chim. Sin., 2007,23(09): 1316-1320
126. DENG Hui-Ning; WANG Yu-Xin.Preparation and Properties of Proton Conducting Composite Membranes from Sulfonated Poly(phthalazinone ether keton) and Phosphotungstic Acid[J]. Acta Phys. -Chim. Sin., 2007,23(08): 1235-1240
127. ZHENG Hai-Tao; LI Yong-Liang; LIANG Jian-Ying; SHEN Pei-Kang.Methanol Oxidation on Pd-based Electrocatalysts[J]. Acta Phys. -Chim. Sin., 2007,23(07): 993-996
128. WEI Ying-Jin; LI Xu; WANG Chun-Zhong; ZHAN Shi-Ying; CHEN Gang.Preparation and Electrochemical Properties of Cu Doped V2O5[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1090-1094
129. MA Guo-Xian; ZHONG Hui; LU Tian-Hong; XIA Yong-Yao.Direct Electrochemistry and Immobilization of Glucose Oxidase on Carbon Black[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1053-1058
130. LIU Su-Qin; GONG Ben-Li; HUANG Ke-Long; ZHANG Ge; LI Shi-Cai.Effect of Calcination Temperature on the Compositions and Electrochemical Performance of Products in the Synthesis of LiFePO4[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1117-1122
131. FENG Rui-Xiang; CAO Yu-Liang; AI Xin-Ping; YANG Han-Xi.AgNi Alloy Used as Anodic Catalyst for Direct Borohydride Fuel Cells[J]. Acta Phys. -Chim. Sin., 2007,23(06): 932-934
132. WU Wei; CAO Jie-Ming; CHEN Yu; LU Tian-Hong.Preparation of High-alloying Pt-Ru/CMK-3 Catalysts in THF-H2O-EtOH Ternary Solution System[J]. Acta Phys. -Chim. Sin., 2007,23(04): 559-564
133. HE Qiong; WANG Shi-Zhong.Effects of the Concentration of LSGMC5 on the Performance of Ni-Fe Composite Anodes for Dimethyl Ether Fuel Cells[J]. Acta Phys. -Chim. Sin., 2007,23(04): 473-478
134. DENG Hui-Ning;WANG Yu-Xin .Sulfonated Poly(phthalazinones) Membranes For Direct Methanol Fuel Cell[J]. Acta Phys. -Chim. Sin., 2007,23(02): 187-191
135. LEI Ze;ZHU Qing-Shan .Solution Combustion Synthesis and Characterization of Nanocrystalline La0.6Sr0.4Co0.2Fe0.8O3-δ Cathode Powders[J]. Acta Phys. -Chim. Sin., 2007,23(02): 232-236
136. HUANG Mian-Yan;CHEN Hua-Yan;GUO Jian-Zhao;WANG Zhi-Tao;XU Li;WANG Yu-Xin.Methanol Resistant Poly(Ether Sulfone)/Sulfonated Poly(Ether Ether Ketone) Blend Proton Exchange Membrane for DMFC[J]. Acta Phys. -Chim. Sin., 2007,23(01): 44-49
137. CAI Yu-Fen;LIU Jun-Min;LIAO Shi-Jun.Preparation, Characterization and Electrocatalytic Properties of Promoted PtMoSi/C Catalysts[J]. Acta Phys. -Chim. Sin., 2007,23(01): 92-97
138. SHEN Pei-Kang;WANG Sheng-Long;HU Zhi-Yi;LI Yong-Liang;ZENG Rong;HUANG Yue-Qiang.Hydrogen Production by Alcohol Electrolysis[J]. Acta Phys. -Chim. Sin., 2007,23(01): 107-110
139. TIAN Juan;ZHENG Dan;ZHANG Xi-Gui;ZHANG Bao-Hong;XIA Bao-Jia;YANG Hui.Preparation of Pt Nanoparticle Modified Porous Silicon Electrode and Its Electrocatalytic Performance[J]. Acta Phys. -Chim. Sin., 2007,23(01): 68-72
140. TANG Zhi-Yuan;YU Ming-Yuan;XUE Jian-Jun;GAO Fei;CUI Yan;LI Liang-Dong.Electrochemical Properties and Synthesis of LiNi0.01Co0.01Mn1.98O4 by SAC Route for Lithium Secondary Battery[J]. Acta Phys. -Chim. Sin., 2007,23(01): 134-138
141. HUANG Ling;JIANG Hong-Hong;KE Fu-Sheng;FAN Xiao-Yong;ZHUANG Quan-Chao;YANG Fang-Zu;SUN Shi-Gang.Structure and Properties of Three-dimensional Reticular Sn-Co Alloy Electrodes as Anode Material for Lithium Batteries[J]. Acta Phys. -Chim. Sin., 2006,22(12): 1537-1541
142. XIE Jian;ZHAO Xin-Bing;YU Hong-Ming;QI Hao;CAO Gao-Shao;TU Jiang-Ping .Preparation, Characterization and Electrochemical Li-absorption/extraction Behaviors of Nanosized Co-Sn Intermetallic Compounds[J]. Acta Phys. -Chim. Sin., 2006,22(11): 1409-1412
143. LI Chang-Yu;LÜ Zhe;LIU Li-Li;LIU Zhi-Ming;SU Wen-Hui.Preparation and Performance Test of Ni-Fe/SDC Cell Anode[J]. Acta Phys. -Chim. Sin., 2006,22(10): 1181-1184
144. GUO Jin-Yu;ZHANG Jian-Guo;ZHANG Tong-Lai;WU Rui-Feng;YU Wei.Thermal Decomposition Mechanisms of a Three-dimensional Framework Coordination Polymer [Cu(HCOO)2(H2O)2][J]. Acta Phys. -Chim. Sin., 2006,22(10): 1206-1211
145. CHU Dao-Bao;YIN Xiao-Juan;FENG De-Xiang;LIN Hua-Shui;TIAN Zhao-Wu.Electrocatalytic Oxidation of Ethanol on Pt/nanoTiO2-CNT Complex Catalysts[J]. Acta Phys. -Chim. Sin., 2006,22(10): 1238-1242
146. JIA Long;XU Yong-Fu;GE Mao-Fa;DU Lin;WANG Geng-Chen;ZHUANG Guo-Shun.Kinetic Study of the Gas-phase Ozonolysis of Propylene[J]. Acta Phys. -Chim. Sin., 2006,22(10): 1260-1265
147. QU Hong-Bo;LIANG Feng;WEI Zheng-Rong;LI Hai-Yang;ZHANG Bing.Photodissociation Dynamics of n-C7H15Br Molecule by Ion Velocity Imaging[J]. Acta Phys. -Chim. Sin., 2006,22(09): 1106-1110
148. ZOU Yu-Man;WANG Shi-Zhong .Preparation of Sm0.5Sr0.5CoO3-La0.8Sr0.2Ga0.8Mg0.15Co0.05O3 composite cathodes using wet-chemistry method and characterization of their properties[J]. Acta Phys. -Chim. Sin., 2006,22(08): 958-961
149. GAO Jie;WANG Shi-Zhong.Study of Ni Composite Anodes for Dimethyl Ether Fuel Cell[J]. Acta Phys. -Chim. Sin., 2006,22(07): 851-855
150. ZHUANG Da-Gao;ZHAO Xin-Bing;XIE Jian;TU Jian;ZHU Tie-Jun;CAO Gao-Shao.One-step Solid-state Synthesis and Electrochemical Performance of Nb-doped LiFePO4/C[J]. Acta Phys. -Chim. Sin., 2006,22(07): 840-844
151. TANG Ding-Guo;CI Yun-Xiang;QI Lu.Influence of Thermal Initiators on the Electrochemical Performances of Gel Polymer Electrolytes[J]. Acta Phys. -Chim. Sin., 2006,22(07): 826-830
152. CHEN Li-Xin;LI Lu;WANG Xin-Hua;DAI Fa-Bang;ZHENG Fang-Ping;LEI Yong-Quan.Phase Structures and Electrochemical Properties of V2.1TiNi0.4Zrx(x= 0~0.06) Hydrogen Storage Electrode Alloys*[J]. Acta Phys. -Chim. Sin., 2006,22(05): 523-527
153. LI Li;WU Gang;YE Qing;DENG Wei;XU Bo-Qing.Electrochemical Modification of Pt/C Catalyst by Silicomolybdic Acid[J]. Acta Phys. -Chim. Sin., 2006,22(04): 419-423
154. YI Shuang-Ping;ZHANG Hai-Yan;PEI Lei;HU Shou-Le;ZENG Guo-Xun;CHEN Jin.Effect of CNTs Treated at Different Temperatures in Nitrogen Ambient on the Electrochemical Properties of CNTs-LaNi5 Electrodes[J]. Acta Phys. -Chim. Sin., 2006,22(04): 436-440
155. CHEN Ling; WANG Xin-dong; GUO Min.The Effect of NdOx as Co-catalyst for the Electro-oxidation of Methanol on PtRu/C[J]. Acta Phys. -Chim. Sin., 2006,22(02): 141-145
156. CHEN Yong-Hong;WEI Yi-Jun;ZHONG Hong-Hai;GAO Jian-Feng;LIU Xing-Qin;MENG Guang-Yao.Synthesis and Properties of La0.5RE0.3Sr0.2FeO3-δ (RE = Nd, Ce, Sm) System with Two Rare Earths for Cathodes[J]. Acta Phys. -Chim. Sin., 2005,21(12): 1357-1362
157. WANG Zhen-bo; YIN Ge-ping; SHI Peng-fei.The Influence of Three Groups of Pt-Ru/C Catalyst’s Precursors on Its Performance for Direct Methanol Fuel Cell[J]. Acta Phys. -Chim. Sin., 2005,21(10): 1156-1160
158. LI Li; XU Bo-qing.Electrooxidation of CO Adsorbed on PtMo/C Catalyst:Effect of Catalyst Preparation[J]. Acta Phys. -Chim. Sin., 2005,21(10): 1132-1137
159. ZHANG Li-juan; XIA Ding-guo.Electrocatalytic Activity of Ordered Intermetallic PtSb for Ethanol Electrooxidation[J]. Acta Phys. -Chim. Sin., 2005,21(09): 1006-1010
160. LIU Shi-jun; CHEN Qi-yuan; FUNAHASHI Shigenobu.Kinetic Study of the Reactions of Porphyrin with Co(II), Ni(II) and Zn(II) Compounds in Supercritical Carbon Dioxide[J]. Acta Phys. -Chim. Sin., 2005,21(08): 893-897
161. TANG Zhi-yuan; LU Xing-he; ZHANG Na.The Anion-cation Multiple Doping Effect of Spinel Cathode Materials on Electrochemical Speciality[J]. Acta Phys. -Chim. Sin., 2005,21(08): 934-938
162. LIU Chun-ling; WEN Yue-hua; CHENG Jie; GUO Quan-gui; CAO Gao-ping; LIU Lang; YANG Yu-sheng.Influence of Pore Structure of Phenolic Resin Based Activated Carbon Fibers on the Electrochemical Performance of Electrical Double-layer Capacitors[J]. Acta Phys. -Chim. Sin., 2005,21(07): 786-791
163. ZHANG Xue-tong; ZHANG Rong-hua.Kinetics Study of Zeolite in Hydrothermal Solutions[J]. Acta Phys. -Chim. Sin., 2005,21(06): 616-621
164. WU Mei-Yin; WANG Jian-Ming; ZHANG Jian-Qing; CAO Chu-Nan.Structure and Electrochemical Performance of Mn-substituted Nickel Hydroxide[J]. Acta Phys. -Chim. Sin., 2005,21(05): 523-527
165. XIAO Xue-Zhang; CHEN Chang-Pin; WANG Xin-Hua; CHEN Li-Xin; WANG Li; GAO Lin-Hui.Microstructure and Electrochemical Properties of Amorphous Mg-Fe-Ni Hydrogen Storage Electrode Material[J]. Acta Phys. -Chim. Sin., 2005,21(05): 565-568
166. CHEN Yu; TANG Ya-Wen; LIU Chang-Peng; XING Wei; LU Tian-Hong.Research Progress on Proton Exchange Membranes for Direct Methanol Fuel Cell[J]. Acta Phys. -Chim. Sin., 2005,21(04): 458-462
167. TAO Bin-Wu;LIU Jian-Hua;LI Song-Mei;ZHAO Liang.Electrochemical Properties of a V2O5/C Composite in Aqueous Solution Used for Zinc Secondary Battery[J]. Acta Phys. -Chim. Sin., 2005,21(03): 338-342
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170. Chang Xiao-Yan;Wang Zhi-Xing;Li Xin-Hai;Kuang Qiong;Peng Wen-Jie;Guo Hua-Jun;Zhang Yun-He.Synthesis and Performance of LiMnPO4 Used as Cathode Material for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2004,20(10): 1249-1252
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209. XU Han, TONG Ye-Xiang, LI Gao-Ren.Controllable Synthesis of Pd Nanocrystals for Applications in Fuel Cells[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
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