ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2013,Vol.29>> Issue(01)>> 167-175     doi: 10.3866/PKU.WHXB201210291         中文摘要
Core-Shell Nanospheres (HP-Fe2O3@TiO2) with Hierarchical Porous Structures and Photocatalytic Properties
CHEN Fu-Xiao1, FAN Wei-Qiang2, ZHOU Teng-Yun2, HUANG Wei-Hong1
1 School of The Environment, Jiangsu University, Zhenjiang 212013, Jiangsu Province, P. R. China;
2 School of Chemistry and Chemical Engineering, Jiangsu University, Zhenjiang 212013, Jiangsu Province, P. R. China
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Core-shell photocatalysts of hierarchical porous nanospheres (HP-Fe2O3@TiO2) have been designed and prepared using solvothermal and sol-gel methods. Transmission electron microscopy (TEM) images confirm that the obtained samples a hierarchical porous structure, which results from both the macroporous structure of the core (Fe2O3) and the mesoporous structure of the shell (TiO2). X-ray diffraction (XRD), scanning electron microscopy (SEM), high-resolution transmission electron microscopy (HRTEM), X-ray photoelectron spectroscopy (XPS), and nitrogen adsorption-desorption isotherms were employed to characterize the structure and properties of HP-Fe2O3@TiO2 nanospheres. We investigated the photocatalytic degradation (in the presence of H2O2) of methylene blue (MB) irradiated under visible and ultraviolet light. The observed photocatalytic performance of HP-Fe2O3@TiO2 nanospheres is attributed to the synergetic effects of the core-shell structure, which indicates that the TiO2 shell enhances the photocatalytic performance of α-Fe2O3. HP-Fe2O3@TiO2 (1 mL Ti(OC4H9)4 (TBT)) possesses the highest photodegradation reaction constant among all samples under visible light irradiation. Moreover, HP-Fe2O3@TiO2 (4 mL TBT) has an optimal monodisperse morphology and achieves high photocatalytic activity under ultraviolet light irradiation.

Keywords: α-Fe2O3   TiO2   Core-shell nanosphere   Hierarchical porous structure   Photocatalytic property   Methylene blue  
Received: 2012-09-16 Accepted: 2012-10-29 Publication Date (Web): 2012-10-29
Corresponding Authors: Email:

Fund: The project was supported by the National Natural Science Foundation of China (21201085), Natural Science Foundation of Jiangsu Province, China (BK2012294), and Jiangsu University College Student Scientific Research Project, China (Y11A018).

Cite this article: CHEN Fu-Xiao, FAN Wei-Qiang, ZHOU Teng-Yun, HUANG Wei-Hong. Core-Shell Nanospheres (HP-Fe2O3@TiO2) with Hierarchical Porous Structures and Photocatalytic Properties[J]. Acta Phys. -Chim. Sin., 2013,29 (01): 167-175.    doi: 10.3866/PKU.WHXB201210291

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52. ZHENG Hua-Rong, WANG Xiao-Wei, LIN Xia-Hui, GENG Qiang, CHEN Xun, DAI Wen-Xin, WANG Xu-Xu.Promoted Effect of Polyethylene Glycol on the Photo-Induced Hydrophilicity of TiO2 Films[J]. Acta Phys. -Chim. Sin., 2012,28(07): 1764-1770
53. CHANG Meng-Lei, LI Xin-Jun.Fabrication of Nanosheet/Nestlike Nanoarray Hierarchical TiO2 Film for Dye-Sensitized Solar Cell[J]. Acta Phys. -Chim. Sin., 2012,28(06): 1368-1372
54. CONG Yan-Qing, LI Zhe, WANG Qi, ZHANG Yi, XU Qian, FU Fang-Xia.Enhanced Photoeletrocatalytic Activity of TiO2 Nanotube Arrays Modified with Simple Transition Metal Oxides (Fe2O3, CuO, NiO)[J]. Acta Phys. -Chim. Sin., 2012,28(06): 1489-1496
55. CHENG Hui, DONG Jiang-Zhou, CHAO Hui, YAO Jiang-Hong, CAO Ya-An.Infection of Oxygen Vacancy at the TiO2 Surface for Film Electrode Rup2P/TiO2/ITO Photo-Induced Charge Transfer[J]. Acta Phys. -Chim. Sin., 2012,28(04): 850-856
56. LIU Yan-Fang, MA Xin-Guo, YI Xin, ZHU Yong-Fa.Controllable Synthesis and Photocatalytic Performance of Bismuth Phosphate Nanorods[J]. Acta Phys. -Chim. Sin., 2012,28(03): 654-660
57. WU Qi, SU Yu-Feng, SUN Lan, WANG Meng-Ye, WANG Ying-Ying, LIN Chang-Jian.Preparation and Visible Light Photocatalytic Activity of Fe-N Codoped TiO2 Nanotube Arrays[J]. Acta Phys. -Chim. Sin., 2012,28(03): 635-640
58. GAO Xiao-Ya, WEN Wen, SONG Zhi-Ying, ZHANG Ai-Ping, HAO Juan, HUANG Qian.Effects of Rare Earth Ions on the Interaction between Nano TiO2 and Bovine Serum Albumin in the Presence of Ultrasound[J]. Acta Phys. -Chim. Sin., 2012,28(02): 470-478
59. LI Ai-Chang, LI Gui-Hua, ZHENG Yan, FENG Ling-Ling, ZHENG Yan-Jun.Photocatalytic Property and Reaction Mechanism of (Ni-Mo)/TiO2 Nano Thin Film Evaluated with Congo Red[J]. Acta Phys. -Chim. Sin., 2012,28(02): 457-464
60. LI Cao-Long, CHEN Wei, YUAN Jian, SHANGGUAN Wen-Feng.Hydrogen Evolution by Photocatalytic Steam Reforming of Methane over Pt/TiO2[J]. Acta Phys. -Chim. Sin., 2012,28(02): 450-456
61. ZHU Yan-Feng, ZHANG Juan, ZHANG Yi-Yong, DING Min, QI Hai-Qing, DU Rong-Gui, LIN Chang-Jian.Anticorrosion Properties of Modified Nano-TiO2 Films Prepared by Sol-Gel Method[J]. Acta Phys. -Chim. Sin., 2012,28(02): 393-398
62. CHEN Xiao-Yun, LU Dong-Fang, HUANG Jin-Feng, LU Yan-Feng, ZHENG Jian-Qiang.Preparation and Properties of N-F Co-Doped TiO2 Photocatalyst with Wide Range Light Response and Multipore Structure from Ionic Liquid-Water Mixture Solvent[J]. Acta Phys. -Chim. Sin., 2012,28(01): 161-169
63. YANG Xing-Ye, LI Bin, SUN Liang, HUANG Zhi-Wei, CHENG Xiao-Min, ZHANG Tao-Wei, TANG Xing-Fu.Effect of Surface Structure of α-Fe2O3 on the Selective Catalytic Reduction of NO by NH3[J]. Acta Phys. -Chim. Sin., 2012,28(01): 184-188
64. WANG Song, MAO Dong-Sen, GUO Xiao-Ming, LU Guan-Zhong.Dimethyl Ether Synthesis from CO2 Hydrogenation over CuO-TiO2-ZrO2/HZSM-5 Catalysts[J]. Acta Phys. -Chim. Sin., 2011,27(11): 2651-2658
65. ZHANG Sheng-Han, LIANG Ke-Xin, TAN Yu.Preparation of TiO2 Nanotube Arrays with Different Cerium Mixing Morphology and Their Photoelectrochemical Response in Visible Light[J]. Acta Phys. -Chim. Sin., 2011,27(11): 2726-2732
66. LI Di, CHEN Hong-Chong, LI Jin-Hua, ZHOU Bao-Xue, CAI Wei-Min.Photoelectrocatalytic Performance and Reaction Mechanism of Different Organics upon Adsorption on a TiO2 Nanotube Array Electrode[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2153-2159
67. LU Sheng-Yong, HUANG Yi-Long, WANG Qiu-Lin, LI Xiao-Dong, YAN Jian-Hua.Photocatalytic Degradation of Gaseous 1,2-Dichlorobenzene over TiO2/AC Photocatalysts[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2191-2199
68. LI Xue-Fei, ZHAO Yun, JIAO Qing-Ze, LI Han-Sheng, WU Hong-Yu, LIU Hong-Bo, CUI Wen-Jia.Preparation of One-Dimensional Titanate Nanomaterials Using Different Titania Sources[J]. Acta Phys. -Chim. Sin., 2011,27(08): 1996-2000
69. ZHAO Xing, ZHUANG Quan-Chao, QIU Xiang-Yun, XU Shou-Dong, SHI Yue-Li, CUI Yong-Li.Electrochemical Performance of Cr2O3/TiO2 Composite Material for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2011,27(07): 1666-1672
70. QIU Wei, REN Cheng-Jun, GONG Mao-Chu, HOU Yun-Ze, CHEN Yao-Qiang.Structure, Surface Properties and Photocatalytic Activity of TiO2 and TiO2/SiO2 Catalysts Prepared at Different pH Values[J]. Acta Phys. -Chim. Sin., 2011,27(06): 1487-1492
71. YUN Hong, LIN Chang-Jian, DU Rong-Gui.Anticorrosion Properties of Nano Anatase TiO2 Films Derived from Sol-Gel and Hydrothermal Crystallization[J]. Acta Phys. -Chim. Sin., 2011,27(05): 1122-1127
72. SU Ya-Ling, LI Yi, DU Ying-Xun, LEI Le-Cheng.Visible-Light-Driven Catalytic Properties and First-Principles Study of Fluorine-Doped TiO2 Nanotubes[J]. Acta Phys. -Chim. Sin., 2011,27(04): 939-945
73. CHEN Dong-Po, ZHANG Xiao-Dan, WEI Chang-Chun, LIU Cai-Chi, ZHAO Ying.Effect of Blocking Layers Prepared by the Hydrolysis of TiCl4 Solution on the Photovoltaic Performance of a Dye-Sensitized Solar Cell[J]. Acta Phys. -Chim. Sin., 2011,27(02): 425-431
74. LUO Ying, CUI Xiao-Li, XIE Jing-Ying.Preparation and Visible Light Photoelectrochemical Response of TiO2-MoO3 Composite Nanotube Thin Films[J]. Acta Phys. -Chim. Sin., 2011,27(01): 135-142
75. ZHANG Zhi-Yu, SANG Li-Xia, SUN Biao, ZHANG Xiao-Min, MA Chong-Fang.Kinetics and Electrochemical Impedance Properties of TiO2 Nanotube Array Photoelectrode[J]. Acta Phys. -Chim. Sin., 2010,26(11): 2935-2940
76. DENG Lin, QI Zhi-Mei.Study of Competitive Adsorption Behavior of Protein andMethylene Blue by Optical Waveguide Spectroscopy[J]. Acta Phys. -Chim. Sin., 2010,26(10): 2672-2678
77. ZHANG Xiao-Ru, LIN Yan-Hong, ZHANG Jian-Fu, HE Dong-Qing, WANG De-Jun.Photoinduced Charge Carrier Properties and Photocatalytic Activity of N-Doped TiO2 Nanocatalysts[J]. Acta Phys. -Chim. Sin., 2010,26(10): 2733-2738
78. ZHU Yan-Feng, DU Rong-Gui, LI Jing, QI Hai-Qing, LIN Chang-Jian.Photogenerated Cathodic Protection Properties of a TiO2 Nanowire FilmPrepared by a Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2349-2353
79. XU Ping-Chang, LIU Yang, WEI Jian-Hong, XIONG Rui, PAN Chun-Xu, SHI Jing.Solvothermal Preparation of Ag/TiO2 Nanoparticles and Their Photocatalytic Activity[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2261-2266
80. CHAO Wen-Liu, WAN Yong, WANG Yun-Xia, LIU Chang-Song.Tribological Properties of Cu-Doped TiO2 Films[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2317-2322
81. HUANG Yong-Xia, LAI Yue-Kun, LIN, Long-Xiang, SUN Lan, LIN Chang-Jian.Electrochemical Construction and Biological Performance of Micropatterned CaP Films[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2057-2060
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83. CHEN Yu-Juan; HU Zhong-Hua; WANG Xiao-Jing; ZHAO Guo-Hua; LIU Ya-Fei; LIU Wei.Influence of Pore Size and Surface Area of Activated Carbon on the Performance of TiO2/AC Photocatalyst[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1589-1596
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87. HUA Nan-ping; WU Zun-yi; DU Yu-kou; ZOU Zhi-gang; YANG Ping.Titanium Dioxide Nanoparticles Codoped with Pt and N for Photodegradation of Cl3CCOOH[J]. Acta Phys. -Chim. Sin., 2005,21(10): 1081-1085
88. TANG Zi-long ; MI Jia; ZHANG Zhong-tai; ZHOU Zhi-gang.Effect of Sm, Eu and Gd on Nb- doped TiO2 Varistors[J]. Acta Phys. -Chim. Sin., 2005,21(10): 1122-1126
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95. Guo Jia-Hao;He Xiao-Ying;Guo Min;Cai Sheng-Min;Chen Xiu-Ying;Peng Xiao-Jun.Photoelectrochemical Studies of the TiO2 Nanocrystalline Electrode Sensitized by Novel Cyanine Dye[J]. Acta Phys. -Chim. Sin., 2004,20(08): 849-853
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