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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2013,Vol.29>> Issue(05)>> 966-972     doi: 10.3866/PKU.WHXB201302281         中文摘要
ELECTROCHEMISTRY AND NEW ENERGY
Effect of Carbon Aerogel Activation on Electrode Lithium Insertion Performance
LIU Nian-Ping, SHEN Jun, GUAN Da-Yong, LIU Dong, ZHOU Xiao-Wei, LI Ya-Jie
Shanghai Key Laboratory of Special Artificial Microstructure Materials and Technology, Institute of Physical Science and Engineering of Tongji University, Shanghai 200092, P. R. China
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Carbon aerogels have received much recent attention as high-capacity insertion anodes for rechargeable lithium ion batteries. Carbon aerogels were synthesized from resorcinol-formaldehyde with a sodium carbonate catalyst via a sol-gel process, ambient drying, carbonization, and activation. Gaseous CO2-activated carbon aerogels combined the advantages of amorphous and nanoporous structures, with richer porous structures and more lithium insertion points than conventional carbon aerogels. Microporosity analysis indicated a high surface area, and the pore volume effectively retained lithium and its compounds. The mesoporosity allowed the mass transport of Li+ and conferred high ionic conductivity to the electrode. These improvements led to a higher lithium insertion capacity, and the activated carbon aerogel exhibited a specific surface area of 2032 m2·g-1. X-ray diffraction (XRD) and scanning electron microscopy (SEM) revealed an amorphous structure and nanoparticle network skeleton, respectively. Lithium insertion capacities of 3870 and 352 mAh·g-1 were exhibited in the 1st and 50th galvanostatic discharge-charge (50 mA·g-1) cycles, respectively. This corresponded to irreversible capacities of 658 and 333 mAh·g-1, respectively. This work demonstrates the feasibility of CO2 activation for improving lithium insertion performance in carbon aerogels, and provides preparation and optimization procedures for other porous electrode materials.



Keywords: Carbon aerogel   Sol-gel   Gas activation   Amorphous carbon   Lithium ion battery  
Received: 2012-11-12 Accepted: 2013-02-27 Publication Date (Web): 2013-02-28
Corresponding Authors: Email: shenjun67@tongji.edu.cn

Fund: The project was supported by the National Natural Science Foundation of China (51072137, 50802064, 11074189), Key Projects in the National Science & Technology Pillar Program, China (2009BAC62B02), and Shanghai Committee of Science and Technology, China (11nm0501600).

Cite this article: LIU Nian-Ping, SHEN Jun, GUAN Da-Yong, LIU Dong, ZHOU Xiao-Wei, LI Ya-Jie. Effect of Carbon Aerogel Activation on Electrode Lithium Insertion Performance[J]. Acta Phys. -Chim. Sin., 2013,29 (05): 966-972.    doi: 10.3866/PKU.WHXB201302281

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57. GAO Ping, TAN Zhuo, CHENG Fu-Quan, ZHOU Heng-Hui, TAN Song-Ting.Effect of Doping with Ti4+ Ion on the Electrochemical Performance of LiFe0.6Mn0.4PO4/C[J]. Acta Phys. -Chim. Sin., 2012,28(02): 338-342
58. MAO Jing, DAI Ke-Hua, ZHAI Yu-Chun.High Rate Capability and Cycling Stability of Li1.07Mn1.93O4 Nanoflakes Synthesized via Gel-Combustion Method[J]. Acta Phys. -Chim. Sin., 2012,28(02): 349-354
59. XU Zi-Jie, JI Tao, ZHAO Lei, WANG Wei-Yan, YANG Chun-Yan, GAN Li-Hua.Restructured Carbon Aerogels and Their Electrochemical Performances[J]. Acta Phys. -Chim. Sin., 2012,28(02): 361-366
60. ZHU Yan-Feng, ZHANG Juan, ZHANG Yi-Yong, DING Min, QI Hai-Qing, DU Rong-Gui, LIN Chang-Jian.Anticorrosion Properties of Modified Nano-TiO2 Films Prepared by Sol-Gel Method[J]. Acta Phys. -Chim. Sin., 2012,28(02): 393-398
61. GONG Qiang, WANG Hong, LIAO Xiao-Zhen, MA Wei, HE Yu-Shi, MA Zi-Feng.Electrochemical Performance of Vanadium Modified LiFe0.5Mn0.5PO4/C Cathode Materials for Lithium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2012,28(01): 100-104
62. XU Ke, SHEN Lai-Fa, MI Chang-Huan, ZHANG Xiao-Gang.Synthesis and Electrochemical Performance of Graphene Modified LiFePO4 Cathode Materials[J]. Acta Phys. -Chim. Sin., 2012,28(01): 105-110
63. LI Jie-Bin, XU You-Long, XIONG Li-Long, WANG Jing-Ping.Improvement of LiNi1/3Co1/3Mn1/3O2 Cathode Materials by Nano-MgO Doping[J]. Acta Phys. -Chim. Sin., 2011,27(11): 2593-2599
64. YANG Xiao-Wei, HE Yu-Shi, LIAO Xiao-Zhen, MA Zi-Feng.Improved Graphene Film by Reducing Restacking for Lithium Ion Battery Applications[J]. Acta Phys. -Chim. Sin., 2011,27(11): 2583-2586
65. WEI Yi, WANG Li-Juan, YAN Ji, SHA Ou, TANG Zhi-Yuan, MA Li.Calcination Temperature Effects on the Electrochemical Performance of Li2MnSiO4/C Cathode Material for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2011,27(11): 2587-2592
66. LIU Li, TIAN Fang-Hua, WANG Xian-You, ZHOU Meng.Electrochemical Behavior of LiV3O8 in Aqueous Li2SO4 Solution[J]. Acta Phys. -Chim. Sin., 2011,27(11): 2600-2604
67. ZHAO Hao-Chuan, SONG Yang, GUO Xiao-Dong, ZHONG Ben-He, DONG Jing, LIU Heng.Effect of Precursor Ingredient Temperature on the Performance of LiFePO4 by Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2011,27(10): 2347-2352
68. GUO Xing-Zhong, YAN Li-Qing, YANG Hui, LI Jian, LI Chao-Yu, CAI Xiao-Bo.Synthesis of Zirconia Aerogels by Ambient Pressure Drying with Propylene Oxide Addition[J]. Acta Phys. -Chim. Sin., 2011,27(10): 2478-2484
69. XU Shou-Dong, ZHUANG Quan-Chao, SHI Yue-Li, ZHU Ya-Bo, QIU Xiang-Yun, SUN Zhi.Electrochemical Impedance Spectra of Intercalation Compound Electrodes: Models and Theoretical Simulations[J]. Acta Phys. -Chim. Sin., 2011,27(10): 2353-2359
70. NIE Ping, SHEN Lai-Fa, CHEN Lin, SU Xiao-Fei, ZHANG Xiao-Gang, LI Hong-Sen.Sol-Gel Synthesis and Electrochemical Performance of Porous LiMnPO4/MWCNT Composites[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2123-2128
71. CHU Dao-Bao, LI Yan, SONG Qi, ZHOU Ying.Synthesis and Properties of LiFePO4/C Cathode Material with a New Carbon Source[J]. Acta Phys. -Chim. Sin., 2011,27(08): 1863-1867
72. LI You-Ji, CHEN Wei, LI Lei-Yong.Effects of Surface Areas and Adsorption Strength on the Photoactivity and Decomposition Kinetics of Acid Red 27 over TiO2-Coated/Activated Carbon Composites[J]. Acta Phys. -Chim. Sin., 2011,27(07): 1751-1756
73. ZHANG Zi-Yu, HU Zhong-Ai, YANG Yu-Ying, WANG Huan-Wen, CHANG Yan-Qin, CHEN Yan-Li, LEI Zi-Qiang.Ce-Doped Mn3O4 and Its Electrochemical Capacitive Behavior[J]. Acta Phys. -Chim. Sin., 2011,27(07): 1673-1678
74. MAI Li-Qiang, YANG Shuang, HAN Chun-Hua, XU Lin, XU Xu, PI Yu-Qiang.Chemical Lithiation and Electroactivity of Nanomaterials[J]. Acta Phys. -Chim. Sin., 2011,27(07): 1551-1559
75. CHEN Lang, RAO Mu-Min, LI Wei-Shan, XU Meng-Qing, LIAO You-Hao, TAN Chun-Lin, YI Jin.Performance Improvement of Polyethylene-Supported PAMS Electrolyte Using Urea as Foaming Agent[J]. Acta Phys. -Chim. Sin., 2011,27(07): 1689-1694
76. ZHAO Xing, ZHUANG Quan-Chao, QIU Xiang-Yun, XU Shou-Dong, SHI Yue-Li, CUI Yong-Li.Electrochemical Performance of Cr2O3/TiO2 Composite Material for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2011,27(07): 1666-1672
77. CHENG Feng, HUANG Ke-Long, LIU Su-Qin, FANG Xue-Song, ZHANG Xin.Surfactant Carbonization to Synthesize a Fe3O4/C Composite and Its Electrochemical Performance[J]. Acta Phys. -Chim. Sin., 2011,27(06): 1439-1445
78. ZHANG Hui-Min, HU Rui-Sheng, HU Jia-Nan, ZHANG Yu-Long.Preparation and Catalytic Activities of La2CoAlO6 for Methane Combustion[J]. Acta Phys. -Chim. Sin., 2011,27(05): 1169-1175
79. Lü Rong-Guan, YANG Jun, WANG Jiu-Lin, NULI Yan-Na.Electrodeposition and Electrochemical Property of Porous Li-Si Film Anodes for Lithium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2011,27(04): 759-763
80. TANG Yan, ZHONG Ben-He, GUO Xiao-Dong, LIU Heng, ZHONG Yan-Jun, NIE Xiang, TANG Hong.Effects of Mixed Solvents on the High-Rate Performance of Li3V2(PO4)3/C Prepared by Sol-Gel Method[J]. Acta Phys. -Chim. Sin., 2011,27(04): 869-874
81. SU Chang, LU Guo-Qiang, XU Li-Huan, ZHANG Cheng, MA Chun-An.Synthesis and Properties of Spindle-Shaped LiFePO4 for the Cathode Material of Lithium Ion Battery[J]. Acta Phys. -Chim. Sin., 2011,27(03): 609-614
82. AN Ting, ZHAO Feng-Qi, YI Jian-Hua, FAN Xue-Zhong, GAO Hong-Xu, HAO Hai-Xia, WANG Xiao-Hong, HU Rong-Zu, PEI Qing.Preparation, Characterization, Decomposition Mechanism and Non-Isothermal Decomposition Reaction Kinetics of the Super Thermite Al/CuO Precursor[J]. Acta Phys. -Chim. Sin., 2011,27(02): 281-288
83. ZHANG Qiu-Mei, SHI Zhi-Cong, LI Yi-Xiao, GAO Dan, CHEN Guo-Hua, YANG Yong.Recent Advances in Fluorophosphate and Orthosilicate Cathode Materials for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2011,27(02): 267-274
84. WANG Xiao-Ya, CHENG Qian, HUANG Tao, YU Ai-Shui.Effect of Calcination Atmosphere on Li/Ni Disorder and Electrochemical Performance of Layered LiNi0.5Mn0.5O2[J]. Acta Phys. -Chim. Sin., 2011,27(02): 437-442
85. CUI Wen-Yu, AN Mao-Zhong, YANG Pei-Xia, ZHANG Jin-Qiu.Cathodic and Thermal Stabilities of the P(VdF-HFP)-Based Ionic Liquid Composite Polymer Electrolyte[J]. Acta Phys. -Chim. Sin., 2011,27(01): 78-84
86. CHEN Shi-Yu, WANG Zhao-Xiang, FANG Xiang-Peng, ZHAO Hai-Lei, LIU Xiao-Jiang, CHEN Li-Quan.Characterization of TiS2 as an Anode Material for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2011,27(01): 97-102
87. ZHOU Xiao-Ling, HUANG Rui-An, WU Zhao-Cong, YANG Bin, DAI Yong-Nian.Synthesis and Electrochemical Properties of High-Rate Spinel Li4Ti5Ol2/TiN Anode Material for Lithium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2010,26(12): 3187-3192
88. CHANG Zhao-Rong, DAI Dong-Mei, LI Bao, TANG Hong-Wei.Effect of Hydrazine on the Performance of LiNi0.5Mn1.5O4Cathode Materials[J]. Acta Phys. -Chim. Sin., 2010,26(10): 2633-2637
89. LI Ya-Juan, ZHAN Hui, LIU Su-Qin, HUANG Ke-Long, ZHOU Yun-Hong.Nanosized Flame Retarded HydroxideMagnesium/Poly(ethylene-oxide) Composite Polymer Electrolyte[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2387-2391
90. HUANG Yan, ZHANG Xing-Wang, LEI Le-Cheng.Preparation, Characterization and Catalytic Activity for ortho- Dichlorobenzene Ozonation of Fe-, Mn-Doped Xerogels[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2443-2448
91. DAI Ke-Hua, MAO Jing, ZHAI Yu-Chun.High Rate Capability of 5 V LiNi0.5Mn1.5O4 Cathode Materials Synthesized via a Gel-Combustion Method[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2130-2134
92. SHEN Bin, WANG Yong-An, WANG Zhi-Fei, ZHANG Ling.Catalytic Activity of an Oxime Carbapalladacycle Complex Grafted onto Superparamagnetically Mesoporous Nanoparticles for the Heck Reaction[J]. Acta Phys. -Chim. Sin., 2010,26(07): 1860-1866
93. QIU Xiang-Yun, ZHUANG Quan-Chao, WANG Hong-Ming, CUI Yong-Li, FANG Liang, SUN Shi-Gang.Influence of Electrolyte Composition on the Intercalation-Deintercalation Process of Lithium Ion in Spinel LiMn2O4[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1499-1506
94. QU Xiao-Hua, LIU Jie, WANG Zhao-Xiang, CAO Dian-Liang, FANG Xiang-Peng, ZHANG Ling, DUAN Jing-Lai, YAO Hui-Jun, CHEN Yan-Feng, SUN You-Mei, HOU Ming-Dong.Preparation of Microporous Membranes by Swift Heavy Ion Irradiation and Impedance Characterization[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1722-1726
95. ZHANG Xiao-Yu, JIANG Wei-Jun, ZHU Xiao-Pei, QI Lu.Characterization of LiNi1/3Mn1/3Co1/3O2 Synthesized by Wet-Chemical Method[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1507-1514
96. LI Li, LU Dan, JI Yuan, ZHAO Yue-Hong.Preparation of Nanocomposite Ag/TiO2-ZrO2 and the Microwave Enhanced Photocatalytic Degradation of Methyl Orange[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1323-1329
97. YANG Chang-Hu, MA Zhong-Quan, LI Feng, HE Bo, YUAN Jian-Hui, ZHANG Zhen-Hua.Spectrum Analysis on Phase Transformations in TiO2 Thin Films[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1349-1354
98. CUI Wen-Yu, AN Mao-Zhong, YANG Pei-Xia.Preparation of an Ionic Liquid Gel Polymer Electrolyte and Its Compatibility with a LiFePO4 Cathode[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1233-1238
99. ZHANG Hui-Juan, SONG Huai-He, ZHOU Ji-Sheng, ZHANG Hong-Kun, CHEN Xiao-Hong.Preparation and Electrochemical Properties of SnO2/Onion-Like Hollow Carbon Nanoparticle Composites as Anode Materials for Lithium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1259-1263
100. GUO Xiang-Yun, JIN Guo-Qiang, WANG Ying-Yong.Preparations and Catalytic Applications of High Surface Area Silicon Carbide[J]. Acta Phys. -Chim. Sin., 2010,26(04): 1143-1150
101. CHANG Yu-Qing, HUANG Ling, SUN Shi-Gang.Electrodeposition and Electrochemical Properties of Ternary Sn-Co-Zn Alloy Electrodes as Anodes for Lithium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2010,26(03): 561-566
102. SUN Jian-Qiu, GONG Lu, SHEN Jing, LIN Zhou, LI Quan-Xin.Sol-Gel Preparation of Porous C12A7-Cl- Crystals[J]. Acta Phys. -Chim. Sin., 2010,26(03): 795-798
103. XIONG Li-Zhi, HE Ze-Qiang.A New Rheological Phase Route to Synthesize Nano-LiVOPO4 Cathode Material for LithiumIon Batteries[J]. Acta Phys. -Chim. Sin., 2010,26(03): 573-577
104. CHANG Zhao-Rong, YU Xu, TANG Hong-Wei, WEI Wen-Qiang, DAI Dong-Mei.Influence of Al Doping Content on the Structure and Electrochemical Properties of LiNi1/3Co2/3-xAlxO2[J]. Acta Phys. -Chim. Sin., 2010,26(03): 567-572
105. LU Hua-Quan, WU Feng, SU Yue-Feng, LI Ning, CHEN Shi, BAO Li-Ying.Electrochemical Performance of LiNi0.5Mn0.5O2 as Cathode Material for Lithium-Ion Batteries Prepared by Oxalate Co-Precipitation Method[J]. Acta Phys. -Chim. Sin., 2010,26(01): 51-56
106. TAN Xiao-Lan, CHENG Xin-Qun, MA Yu-Lin, ZUO Peng-Jian, YIN Ge-Ping.Film Formation and Cycleability of LiBOB-Based Electrolyte[J]. Acta Phys. -Chim. Sin., 2009,25(10): 1967-1971
107. YANG Jiu-Long, LI Jian-Feng, LU Yong.Nitration of Benzene in a Continuous-Flow Microreactor Integrated with Microfiber-Structured Nafion/SiO2 Solid Acid Catalyst[J]. Acta Phys. -Chim. Sin., 2009,25(10): 2045-2049
108. ZHENG Jun-Chao, LI Xin-Hai, WANG Zhi-Xing, LI Jin-Hui, WU Ling, LI Ling-Jun, GUO Hua-Jun.A Coalescence Mechanism for the Composite Cathode Material xLiFePO4·yLi3V2(PO4)3[J]. Acta Phys. -Chim. Sin., 2009,25(09): 1916-1920
109. JIANG Dong-Dong, FU Yan-Bao, MA Xiao-Hua.Fabrication and Characterization of Tin Nanorod Electrodes for Lithium Ion Rechargeable Batteries[J]. Acta Phys. -Chim. Sin., 2009,25(08): 1481-1484
110. FENG Ji-Jun, LIU Xiang-Zhe, LIU Xiao-Zhen, JIANG Jian-Zhuang, ZHAO Jing.Hydrothermal Syntheses and Properties of LiV3-xMnxO8 as Cathode Materials for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2009,25(08): 1490-1494
111. ZHONG Mei-E, ZHOU Zhi-Hui, ZHOU Zhen-Tao.Electrochemical Performance of High-Density LiFePO4/C Composites Synthesized by Solid State-Carbothermal Reduction Method[J]. Acta Phys. -Chim. Sin., 2009,25(08): 1504-1510
112. LI Li, MA Yu, CAO Yan-Zhen, JI Yuan, GUO Yi-Hang.Preparation of Periodic Mesoporous H6P2W18O62/TiO2(Brij-76) Composite and Microwave Enhanced Photocatalytic Degradation of Monochlorobenzene[J]. Acta Phys. -Chim. Sin., 2009,25(07): 1461-1466
113. HU Guo-Rong, CAO Yan-Bing, PENG Zhong-Dong, DU Ke, JIANG Qing-Lai.Preparation of Li2FeSiO4 Cathode Material for Lithium-Ion Batteries by Microwave Synthesis[J]. Acta Phys. -Chim. Sin., 2009,25(05): 1004-1008
114. GAO Hong-Quan, LAI Yan-Qing, ZHANG Zhi-An, LIU Ye-Xiang.Electrochemical Behaviors of New Lithium Salt LiBC2O4F2 in EC+DMC Solvents[J]. Acta Phys. -Chim. Sin., 2009,25(05): 905-910
115. FAN Xiao-Yong, ZHUANG Quan-Chao, WEI Guo-Zhen, KE Fu-Sheng, HUANG Ling, DONG Quan-Feng, SUN Shi-Gang.Fabrication and Performance of Cu6Sn5 Alloy Anode Using Porous Cu as Current Collector[J]. Acta Phys. -Chim. Sin., 2009,25(04): 611-616
116. WU Feng, WANG Meng, SU Yue-Feng, CHEN Shi.Surface Modification of LiCo1/3Ni1/3Mn1/3O2 by TiO2-Coating[J]. Acta Phys. -Chim. Sin., 2009,25(04): 629-634
117. CHEN Qi-Feng, JIANG Dong, XU Yao, WU Dong, SUN Yu-Han.Visible Region Photocatalysis of Ce-Si/TiO2 Synthesized Using Sol-Gel-Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2009,25(04): 617-623
118. ZHUANG Quan-Tiao, WEI Guo-Zhen, DONG Quan-Feng, SUN Shi-Gang.Influence of Temperature on the Performance of a Graphite Electrode[J]. Acta Phys. -Chim. Sin., 2009,25(03): 406-410
119. ZHANG Guo-Qiang, MA Li, WU Zhong-Jie, ZHANG Hai-Yan, NI Pei.Electrochemical Behaviour of the Composite Polymer Electrolyte P(VDF-HFP)-PMMA/CaCO3(SiO2)[J]. Acta Phys. -Chim. Sin., 2009,25(03): 555-560
120. MA Ruo-Biao, FU Yan-Bao, MA Xiao-Hua.Preparation and Electrochemical Performance of Tin-Dioxide Filled Multi-Walled Carbon Nanotubes[J]. Acta Phys. -Chim. Sin., 2009,25(03): 441-445
121. XU Jie; YAO Wan-Hao; YAO Yi-Wen; WANG Zhou-Cheng; YANG Yong.Effect of Fluoroethylene Carbonate Additive on the Performance of Lithium Ion Battery[J]. Acta Phys. -Chim. Sin., 2009,25(02): 201-206
122. LI Yang; XIE Hua-Qing; TU Jiang-Ping.SnS with Various Morphologies and Sizes as Anode Material for Lithium Ion Batteries[J]. Acta Phys. -Chim. Sin., 2009,25(02): 365-370
123. HUA Zheng-He; LI Dong; FU Hao.Sol-Gel Template Synthesis and Characterization of Magnetoelectric CoFe2O4/BaTiO3 Nanotubes[J]. Acta Phys. -Chim. Sin., 2009,25(01): 145-149
124. WANG Tao, HE Jian-Ping, ZHANG Chuan-Xiang, ZHOU Jian-Hua, GUO Yun-Xia, CHEN Xiu, DI Zhi-Yong, SUN Dun, WANG Dao-Jun.Preparation and Electrochemical Properties of Ordered Mesoporous C/NiO Composites[J]. Acta Phys. -Chim. Sin., 2008,24(12): 2314-2320
125. YANG Shun-Yi; WANG Xian-You; WEI Jian-Liang; LI Xiu-Qin; TANG An-Ping.Preparation and Electrochemical Performance of Na-Mn-O Cathode Materials[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1669-1674
126. HUANG Jun-Jie; JIANG Zhi-Yu.Electrochemical Performance of LiMn2O4 Thin Film Electrode Fabricated by Ink-Jet Printing Technique[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1563-1567
127. ZHANG Hua; ZHOU Yong-Ning; WU Xiao-Jing; FU Zheng-Wen.Electrochemical Properties of CuF2 Films Fabricated by Pulsed Laser Deposition[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1287-1291
128. LI Fan-Qun; LAI Yan-Qing; ZHANG Zhi-An; GAO Hong-Quan; YANG Juan.Electrochemical Behaviors of Et4NBF4+LiPF6/EC+PC+DMC Electrolyte on Graphite Electrode[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1302-1306
129. WANG Meng; WU Feng; SU Yue-Feng; CHEN Shi.Electrochemical Characteristics of Y2O3-Coated LiCo1/3Ni1/3Mn1/3O2[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1175-1179
130. LI Jin-Huan; KANG Wan-Li; YAN Wen-Hua; GUO Yi-Hang; GAO Hong-Feng; LIU Zhong-He.Preparation of Eu3+ Doped Titania Nanocrystals and Photocatalytic Degradation Partially Hydrolyzed Polyacrylamide[J]. Acta Phys. -Chim. Sin., 2008,24(06): 1030-1034
131. ZHOU Jian-Hua; HE Jian-Ping; JI Ya-Jun; ZHAO Gui-Wang; ZHANG Chuan-Xiang; CHEN Xiu; WANG Tao.Influence of Hierarchical Porosity in Carbon Material on Electrocatalytic Property of Supported Pt Nanoparticles[J]. Acta Phys. -Chim. Sin., 2008,24(05): 839-843
132. WANG Jian-Hua; LI Bin; WU Hai-Yan; GUO Yu-Zhong.Synthesis of Mesoporous SnO2 and Its Application in Lithium-Ion Battery[J]. Acta Phys. -Chim. Sin., 2008,24(04): 681-685
133. WU Yu-Cheng; LIU Xiao-Lu; YE Min; XIE Ting; HUANG Xin-Min.Preparation and Properties of Carbon Nanotube-TiO2 Nanocomposites[J]. Acta Phys. -Chim. Sin., 2008,24(01): 97-102
134. ZHAN Ying-Ying; CAI Guo-Hui; ZHENG Yong; SHEN Xiao-Nv; ZHENG Ying; WEI Ke-Mei.Synthesis of High Surface Area Silicon Carbide and Its Application in CO Oxidation Reaction[J]. Acta Phys. -Chim. Sin., 2008,24(01): 171-175
135. WANG Ya-Dan; WANG Jian; MU Qi-Yong; LI Yong-Wei; QI Lu.Electrochemical Performances of LiMn2O4-based Electrode with Water-soluble Binder[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 14-17
136. QI Lu; SONG Zhao-Shuang; XU Hua; MAO Yong-Zhi; WU Ning-Ning; LIU Zheng-Yao.Electrochemical Performance of LithiumIon Battery Power Syetemfor Electric Vehicles[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 21-25
137. ZHANG Chun-Ling; JIANG Wei-Jun; ZHANG Jing; QI Lu.Performance of LiMn1.5Ni0.5-xCuxO4 as 5V Cathode Material for Lithium-ion Battery[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 31-35
138. TANG Ding-Guo.Application of Polymer LithiumIon Batteries Based on IPN[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 18-20
139. HOU Xian-Quan; JIANG Wei-Jun; QI Lu; HAN Li-Juan.Synthesis and Properties of Layered LiNi0.8Co0.2-xMgxO2 Cathode Material[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 40-45
140. FAN Mao-Song; LEI Xiang-Li; WU Ning-Ning; QI Lu.Electrochemical Performance of LiMn2O4 Power Battery[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 36-39
141. WANG Hai-Yan; LIU Xin-Hou; WU Da-Yong.Electrospinning and Electrospun Membranes[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 67-74
142. AN Hong-Li; WU Ning-Ning; LEI Xiang-Li; XU Jin-Long; QI Lu.Electrochemical Performance of LithiumIon Battery for Plug-in Hybrid Electric Vehicle Applications[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 60-66
143. GUO Ying-Jun; CHEN Hui; QI Lu.Progress in Electrolyte Solutions for Lithium-ion Battery[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 80-89
144. LEE Meng-Lung; LEE Yi-Da; CHANG Chie-Tai; GAO Tong-Han; LEE Torng-Jinn.Application and Technology of Aluminum Bag Lithium-Ion Polymer Battery[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 100-106
145. GUO Ying-Jun; LI Qi-Qi-Ge; NING Ying-Kun; QI Lu; TANG Hong-Wu.Performance of Liquid Electrolyte for Lithium-ion Battery at Elevated-temperature[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 1-4
146. FENG Hua-Jun; CHEN Yuan;DAI Ke-Hua; SONG Zhao-Shuang; MA Jian-Wei; QI Lu.Preparation and Characterization of a Novel Kind of Polymer Electrolyte Composite Membrane for Lithium-Ion Battery[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1922-1926
147. CHEN Yong-Chong; XU Xing-Jun; CUI Hong-Zhi; DAI Ke-Hua; SONG Zhao-Shuang; JIANG Wei-Jun; QI Lu.Preferred Orientation of Crystals and the Intensity Ratios of XRD Peaks of Cathode Material LiCoO2[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1948-1953
148. HOU Chun-Ping; YUE Min.A Novel Cathode Material Lithium Vanadium Phosphate Synthesized by Liquid-phase Sphericizing Granulation[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1954-1957
149. WANG Feng; HAO Ya-Juan; JIN Guo-Qiang; GUO Xiang-Yun.Effects of the Reaction Conditions in Preparation of Si3N4 Nanowires[J]. Acta Phys. -Chim. Sin., 2007,23(10): 1503-1507
150. ZHANG Wei; WANG Shu-Liang; MA Yun-Qing; WANG Cui-Ping; LIU Xing-Jun.Influence of Interface Diffusion between Al Substrate and TiO2 Filmon Photocatalytic Activity[J]. Acta Phys. -Chim. Sin., 2007,23(09): 1347-1352
151. TANG Hong-Wei; ZHU Zhi-Hong; CHANG Zhao-Rong; CHEN Zhong-Jun.Drawing and Application of Phase Diagram Related to Eutectic Mixed Lithium Salts[J]. Acta Phys. -Chim. Sin., 2007,23(08): 1265-1268
152. WEI Ying-Jin; LI Xu; WANG Chun-Zhong; ZHAN Shi-Ying; CHEN Gang.Preparation and Electrochemical Properties of Cu Doped V2O5[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1090-1094
153. ZHANG Hong-Fang; FU Ping-Ping; SONG Ying-Jie; DU Chen-Shu; YANG Hua-Bin; ZHOU Zuo-Xiang; WU Meng-Tao; HUANG Lai-He.Preparation and Properties of Sandwich-type Si/Fe/Si Film Anode for Lithium-ion Battery[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1065-1070
154. HUANG Dong-Sheng; ZENG Ren-Jie; CHEN Chao-Feng; LI Yu-Hua.Hydrophilicity of TiO2 Thin Films Codoped with Iron and Nitrogen[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1037-1041
155. ZHAO Meng; WANG Jin-Xing; FENG Cai-Hui; ZOU Bo; CHEN Cheng; WANG Zhu-Yi; WU Feng-Qing; ZOU Le-Hui.Preparation and Gas Sensing Properties to Formaldehyde of TiO2/Ag2O Nanocrystalline[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1003-1006
156. LI Hong-Jian; CHEN Gang; LI Zhong-Hua; ZHOU Chao.Synthesis and Photocatalytic Decomposition of Water under Visible Light Irradiation of La2Ti2-xCoxO7 with Pyrochlore Structure[J]. Acta Phys. -Chim. Sin., 2007,23(05): 761-764
157. WU Lun-Peng; ZHAO Lian-Hua; ZHANG Hai-Ming; ZHAO Qing-Nan.Effects of the Adsorption of Oxygen on the Photocatalytic Activity of TiO2 Films Using PhotocurrentMethod[J]. Acta Phys. -Chim. Sin., 2007,23(05): 765-768
158. ZHANG Xiao-Fei; HU Rui-Sheng; GAO Guan-Jun; MENG He; SU Hai-Quan.Influence of Two Complexants on Structure and Performance of Ce-Sn-O Complex Oxides[J]. Acta Phys. -Chim. Sin., 2007,23(05): 659-663
159. LIU Su-Qin; LI Shi-Cai; HUANG Ke-Long; CHEN Zhao-Hui.Effect of Doping Ti4+ on the Structure and Performances of Li3V2(PO4)3[J]. Acta Phys. -Chim. Sin., 2007,23(04): 537-542
160. WANG Huan-Ping; ZHANG Qi-Long; YANG Hui; SUN Hui-Ping.Synthesis and Microwave Dielectric Properties of (Ca1-xMgx)SiO3 Ceramic by Sol-Gel Process[J]. Acta Phys. -Chim. Sin., 2007,23(04): 609-613
161. ZHOU Hong-Wei;LI Huai-Xiang;JIANG Zheng-Wei;ZUO Xiang-Qing.Treatment of ZnS:Mn Phosphors by Partial Sublimation of SnO2:Sb Xerogel[J]. Acta Phys. -Chim. Sin., 2007,23(01): 88-91
162. HUANG Ke-Long;YANG Sai;LIU Su-Qin;WANG Hai-Bo.Kinetics of Electrode Processes of LiFePO4 in Saturated Lithium Nitrate Solution[J]. Acta Phys. -Chim. Sin., 2007,23(01): 129-133
163. QIN Hai-Ying;XIE Jian;MI Jian-Li;TU Jian;ZHAO Xin-Bing.Solvothermal Synthesis and Electrochemical Lithiation/Delithiation Performance of FeSb2 Nanorods[J]. Acta Phys. -Chim. Sin., 2006,22(12): 1555-1559
164. HUANG Ling;JIANG Hong-Hong;KE Fu-Sheng;FAN Xiao-Yong;ZHUANG Quan-Chao;YANG Fang-Zu;SUN Shi-Gang.Structure and Properties of Three-dimensional Reticular Sn-Co Alloy Electrodes as Anode Material for Lithium Batteries[J]. Acta Phys. -Chim. Sin., 2006,22(12): 1537-1541
165. XU Yu-Hong;ZHANG Bao-Hong;GONG GUI-Ying;MA Ping .Electrochemical Properties Study of Sb2O3 doped Li4Ti5O12[J]. Acta Phys. -Chim. Sin., 2006,22(11): 1336-1341
166. XIE Jian;ZHAO Xin-Bing;YU Hong-Ming;QI Hao;CAO Gao-Shao;TU Jiang-Ping .Preparation, Characterization and Electrochemical Li-absorption/extraction Behaviors of Nanosized Co-Sn Intermetallic Compounds[J]. Acta Phys. -Chim. Sin., 2006,22(11): 1409-1412
167. QIAO Bin;TANG Zi-Long;ZHANG Zhong-Tai;CHEN Lei.Photoluminescent and Electroluminescent Characteristics of ZnGa2O4:Cr3+ Red Phosphor[J]. Acta Phys. -Chim. Sin., 2006,22(10): 1291-1295
168. FENG Chun-Bo;DU Zhi-Ping;Zhao Yong-Hong;TAI Xiu-Mei;LI Qiu-Xiao .Photocatalytic Activity of Au Modified Nano-TiO2 for NPE-10 Degradation[J]. Acta Phys. -Chim. Sin., 2006,22(08): 953-957
169. ZHUANG Da-Gao;ZHAO Xin-Bing;XIE Jian;TU Jian;ZHU Tie-Jun;CAO Gao-Shao.One-step Solid-state Synthesis and Electrochemical Performance of Nb-doped LiFePO4/C[J]. Acta Phys. -Chim. Sin., 2006,22(07): 840-844
170. LIU Yi-An;XUE Cheng-Shan;ZHUANG Hui-Zhao;ZHANG Xiao-Kai;TIAN De-Heng;WU Yu-Xin;SUN Li-Li;AI Yu-Jie;WANG Fu-Xue.Structure and Synthesis of GaN Powder by Sol-Gel Method[J]. Acta Phys. -Chim. Sin., 2006,22(06): 657-660
171. WANG Zhong;TIAN Wen-Huai;LI Xing-Guo.Synthesis and Electrochemical Properties of Sn-Sb Alloy Prepared by Hydrogen Plasma-metal Reaction[J]. Acta Phys. -Chim. Sin., 2006,22(06): 752-755
172. XUE Ming-Zhe; CHENG Sun-Chao; YAO Jia; FU Zheng-Wen.Electrochemical Properties of SnSe Thin Film Electrode Fabricated by Pulsed Laser Deposition[J]. Acta Phys. -Chim. Sin., 2006,22(03): 383-387
173. XU Meng-Qing; ZUO Xiao-Xi; LI Wei-Shan; ZHOU Hao-Jie; LIU Jian-Sheng; YUAN Zhong-Zhi.Effect of Butyl Sultone on the Li-ion Battery Performance and Interface of Graphite Electrode[J]. Acta Phys. -Chim. Sin., 2006,22(03): 335-340
174. YE Qing; XU Bo-Qing.Textural and Structure Characterizations of Ce1-xMnxO2Prepared by Citric Acid Sol-Gel Method[J]. Acta Phys. -Chim. Sin., 2006,22(03): 345-349
175. ZHUANG Quan-chao; FAN Xiao-yong; XU Jin-mei; CHEN Zuo-feng; DONG Quan-feng; JIANG Yan-xia; HUANG Ling; SUN Shi-gang.Electrochemical Impedance Spectroscopic Study of the First Delithiation of Spinel Lithium Manganese Oxide[J]. Acta Phys. -Chim. Sin., 2006,22(02): 234-238
176. YANG Xiao; NI Jiang-feng; HUANG You-yuan; CHEN Ji-tao; ZHOU Heng-hui; ZHANG Xinxiang.Effect of Ti-Doping on Different Morphologic LiCoO2[J]. Acta Phys. -Chim. Sin., 2006,22(02): 183-188
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179. WANG Guo-guang WANG Jian-ming MAO Wen-qu LIU Li-qing ZHANG Jian-qing CAO Chu-nan.Structure and Electrochemical Performance of LiNiyCo0.1-yMn1.9O4 Cathode Materials Prepared by a Precipitation Method[J]. Acta Phys. -Chim. Sin., 2005,21(11): 1285-1290
180. LIU Rui-quan; XIE Ya-hong; LI Zhi-jie; WANG Ji-de; SUN Yi-gang.Application of Proton Conductors (Ce0.8La0.2)1-xCaxO2-δ in Synthesis of Ammonia[J]. Acta Phys. -Chim. Sin., 2005,21(09): 967-970
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182. PENG Feng; CHEN Shui-hui; ZHANG Lei; WANG Hong-juan; XIE Zhi-yong.Preparation of Visible-light Response Nano-sized ZnO Film and Its Photocatalytic Degradation to Methyl Orange[J]. Acta Phys. -Chim. Sin., 2005,21(08): 944-948
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184. HUANG You-yuan; ZHOU Heng-hui; CHEN Ji-tao; GAO De-shu; SU Guang-yao.The Effect of Ti4+, Mg2+ Co-doping on Performance of LiNi0.4Co0.2Mn0.4O2[J]. Acta Phys. -Chim. Sin., 2005,21(07): 725-729
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