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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2014,Vol.30>> Issue(10)>> 1957-1962     doi: 10.3866/PKU.WHXB201408041         中文摘要
PHYSICAL CHEMISTRY OF MATERIALS
Synthesis and Interfacial Electron Transfer of a Composite Film of Graphene and Tungsten Oxide
LI Wen-Zhang2, LIU Yang2, LI Jie2, YANG Ya-Hui1, CHEN Qi-Yuan2
1. College of Resources and Environment, Hunan Agricultural University, Changsha 410128, P. R. China;
2. School of Chemistry and Chemical Engineering, Central South University, Changsha 410083, P. R. China
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Composite films of graphene and tungsten oxide were fabricated by dip-coating with ammonium metatungstate as the precursor and polyvinylpyrrolidone as the bridging agent. The as-prepared composites were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and Raman spectroscopy. Photocurrent test, electrochemical impedance spectroscopy (EIS), transient photocurrent spectroscopy,and intensity-modulated photocurrent spectroscopy were used to study the transfer process and transport behavior of the charge carriers at the interface of the film electrodes. The results showed that the tungsten oxide nanoparticles were sufficiently composited with graphene. The efficiency of photoelectric conversion improved significantly. The transient constant and the electron-hole lifetime increased after the incorporation of graphene. The electron transit time of the composite film was reduced and was found to be only 47.5% of that of the tungsten oxide film.



Keywords: Tungsten oxide   Graphene   Composite film   Photoelectrochemistry   Interfacial electron transfer  
Received: 2014-05-15 Accepted: 2014-07-22 Publication Date (Web): 2014-08-04
Corresponding Authors: YANG Ya-Hui Email: Yangyahui2002@sina.com

Fund: The project was supported by the National High Technology Research and Development Program of China (863) (2011AA050528), National Natural Science Foundation of China (21171175), and Hunan Provincial Natural Science Foundation, China (13JJ6003).

Cite this article: LI Wen-Zhang, LIU Yang, LI Jie, YANG Ya-Hui, CHEN Qi-Yuan. Synthesis and Interfacial Electron Transfer of a Composite Film of Graphene and Tungsten Oxide[J]. Acta Phys. -Chim. Sin., 2014,30 (10): 1957-1962.    doi: 10.3866/PKU.WHXB201408041

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76. RAN Ke, CHEN Qing, ZUO Jian-Min.Fabrication and Structure Characterization of Quasi-2-Dimensional Amorphous Carbon Structures[J]. Acta Phys. -Chim. Sin., 2012,28(07): 1551-1555
77. BI Dong-Qin, XU Yi-Ming.Influence of Iron Oxide Doping on the Photocatalytic Degradation of Organic Dye X3B over Tungsten Oxide[J]. Acta Phys. -Chim. Sin., 2012,28(07): 1777-1782
78. ZHANG Xiao, YANG Rong, WANG Chen, HENG Cheng-Lin.Cell Biocompatibility of Functionalized Graphene Oxide[J]. Acta Phys. -Chim. Sin., 2012,28(06): 1520-1524
79. TIAN Xiang-Gui, ZHANG Yue, YANG Tai-Sheng.First-Principles Study of H2 Dissociative Adsorption Reactions on WO3 Surfaces[J]. Acta Phys. -Chim. Sin., 2012,28(05): 1063-1069
80. LIU Bo, SUN Hong-Juan, PENG Tong-Jiang.Factor Group Analysis of Molecular Vibrational Modes of Graphene and Density Functional Calculations[J]. Acta Phys. -Chim. Sin., 2012,28(04): 799-804
81. HUANG Ye, LIU Yu-Yang, LI Wen-Zhang, CHEN Qi-Yuan.Effects of Calcination Temperature on Morphologies and Photoelectrochemical Properties of Anodized WO3 Nanoporous Films[J]. Acta Phys. -Chim. Sin., 2012,28(04): 865-870
82. JIN Yu, CHEN Hong-Yuan, CHEN Ming-Hai, LIU Ning, LI Qing-Wen.Carbon Nanotube/Polyaniline/Graphene Composite Paper and Its Electrochemical Capacitance Behaviors[J]. Acta Phys. -Chim. Sin., 2012,28(03): 609-614
83. XIE Peng-Yang, ZHUANG Gui-Lin, LÜ Yong-An, WANG Jian-Guo, LI Xiao-Nian.Enhanced Bonding between Noble Metal Adatoms and Graphene with Point Defects[J]. Acta Phys. -Chim. Sin., 2012,28(02): 331-337
84. XU Ke, SHEN Lai-Fa, MI Chang-Huan, ZHANG Xiao-Gang.Synthesis and Electrochemical Performance of Graphene Modified LiFePO4 Cathode Materials[J]. Acta Phys. -Chim. Sin., 2012,28(01): 105-110
85. ZHANG Xiao-Yan, SUN Ming-Xuan, SUN Yu-Jun, LI Jing, SONG Peng, SUN Tong, CUI Xiao-Li.Photoelectrochemical Properties of Graphene Oxide Thin Film Electrodes[J]. Acta Phys. -Chim. Sin., 2011,27(12): 2831-2835
86. TANG Jun, KANG Chao-Yang, LI Li-Min, XU Peng-Shou.Direct Graphene Growth by Depositing Carbon Atoms on Si Substrate Covered by SiC Buffer Layers[J]. Acta Phys. -Chim. Sin., 2011,27(12): 2953-2959
87. YUE Zhao, ZHANG Wei, WANG Cheng, LIU Guo-Hua, NIU Wen-Cheng.Photoinduced Electron Transfer between CdS Quantum Dots and Gold Electrodes[J]. Acta Phys. -Chim. Sin., 2011,27(12): 2814-2820
88. YANG Xiao-Wei, HE Yu-Shi, LIAO Xiao-Zhen, MA Zi-Feng.Improved Graphene Film by Reducing Restacking for Lithium Ion Battery Applications[J]. Acta Phys. -Chim. Sin., 2011,27(11): 2583-2586
89. BU Yu-Yu, LI Wei-Bing, YU Jian-Qiang, WANG Xiu-Tong, QI Mei-Ling, NIE Meng-Yan, HOU Bao-Rong.Fabrication of SrTiO3 Nanocrystalline Film Photoelectrode and Its Photoelectrochemical Anticorrosion Properties for Stainless Steel[J]. Acta Phys. -Chim. Sin., 2011,27(10): 2393-2399
90. LU Xiang-Jun, DOU Hui, YANG Su-Dong, HAO Liang, ZHANG Fang, ZHANG Xiao-Gang.Fabrication and Electrochemical Capacitive Behavior of Freestanding Graphene/Polyaniline Nanofibre Film[J]. Acta Phys. -Chim. Sin., 2011,27(10): 2333-2339
91. YUAN Wen-Hui, LI Bao-Qing, LI Li.Superior Graphene for Hydrogen Adsorption Prepared by the Improved Liquid Oxidation-Reduction Method[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2244-2250
92. MIN Shi-Xiong, Lü Gong-Xuan.Preparation of CdS/Graphene Composites and Photocatalytic Hydrogen Generation from Water under Visible Light Irradiation[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2178-2184
93. PENG Tian-You, KE Ding-Ning, ZENG Peng, ZHANG Xiao-Hu, FAN Ke.Preparation and Photoelectrochemical Performance of BiVO4 Film Electrode[J]. Acta Phys. -Chim. Sin., 2011,27(09): 2160-2166
94. YING Hong, WANG Zhi-Yong, GUO Zheng-Duo, SHI Zu-Jin, YANG Shang-Feng.Reduced Graphene Oxide-Modified Bi2WO6 as an Improved Photocatalyst under Visible Light[J]. Acta Phys. -Chim. Sin., 2011,27(06): 1482-1486
95. ZHANG Yi, CHEN Biao, YANG Zu-Pei, ZHANG Zhi-Jun.Controlled Synthesis and Characterization of the Structure and Property of Fe3O4 Nanoparticle-Graphene Oxide Composites[J]. Acta Phys. -Chim. Sin., 2011,27(05): 1261-1266
96. SUN Da-Li, PENG Sheng-Lin, OUYANG Jun, OUYANG Fang-Ping.Electronic Transport Properties of Graphene Nanoribbons with Nanoholes[J]. Acta Phys. -Chim. Sin., 2011,27(05): 1103-1107
97. LI Yun-Xia, WEI Zi-Dong, ZHAO Qiao-Ling, DING Wei, ZHANG Qian, CHEN Si-Guo.Preparation of Pt/Graphene Catalyst and Its Catalytic Performance for Oxygen Reduction[J]. Acta Phys. -Chim. Sin., 2011,27(04): 858-862
98. WANG Zhi-Ping, LUO Hong, GAO Li-Hua, WANG Ke-Zhi.Electrostatically Self-Assembled Films Prepared Using Bipolar Thiophene Hemicyanine and Prussian Blue[J]. Acta Phys. -Chim. Sin., 2011,27(03): 754-758
99. YANG Yong-Hui, SUN Hong-Juan, PENG Tong-Jiang, HUANG Qiao.Synthesis and Structural Characterization of Graphene-Based Membranes[J]. Acta Phys. -Chim. Sin., 2011,27(03): 736-742
100. DAI Xian-Qi, LI Yan-Hui, ZHAO Jian-Hua, TANG Ya-Nan.Effects of Vacancy and Boron Doping on Si Adsorption on Graphene[J]. Acta Phys. -Chim. Sin., 2011,27(02): 369-373
101. LUO Ying, CUI Xiao-Li, XIE Jing-Ying.Preparation and Visible Light Photoelectrochemical Response of TiO2-MoO3 Composite Nanotube Thin Films[J]. Acta Phys. -Chim. Sin., 2011,27(01): 135-142
102. YANG Xin-Li, YIN An-Yuan, DAI Wei-Lin, FAN Kang-Nian.Synthesis of Highly Efficient WO3-Doped MCF Catalyst and Its Application in the Selective Oxidation of Cyclopentene to Glutaraldehyde[J]. Acta Phys. -Chim. Sin., 2011,27(01): 177-185
103. WU Xiao-Qin, ZONG Rui-Long, MU Hao-Jie, ZHU Yong-Fa.Cataluminescence Performance on Catalysts of Graphene Supported Platinum[J]. Acta Phys. -Chim. Sin., 2010,26(11): 3002-3008
104. ZHANG Qiao-Bao, FENG Zeng-Fang, HAN Nan-Nan, LIN Ling-Ling, ZHOU Jian-Zhang, LIN Zhong-Hua.Preparation and Photoeletrochemical Performance of CdS Quantum Dot Sensitized ZnO Nanorod Array Electrodes[J]. Acta Phys. -Chim. Sin., 2010,26(11): 2927-2934
105. XU Hai-Di, QIU Chun-Tian, ZHANG Qiu-Lin, LIN Tao,GONG Mao-Chu, CHEN Yao-Qiang.Influence of Tungsten Oxide on Selective Catalytic Reduction of NOx with NH3 over MnOx -CeO2 /ZrO2-TiO2Monolith Catalyst[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2449-2454
106. LI Wen-Zhang, LI Jie, WANG Xuan, ZHANG Shu-Juan, CHEN Qi-Yuan.Photoelectrochemical Properties of Cubic Tungsten Trioxide Films Obtained by the Polymeric Precursor Method[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2343-2348
107. HU Yao-Juan, JIN Juan, ZHANG Hui, WU Ping, CAI Chen-Xin.Graphene: Synthesis, Functionalization and Applications in Chemistry[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2073-2086
108. WEN Zhu-Liang, YANG Su-Dong, SONG Qi-Jun, HAO Liang, ZHANG Xiao-Gang.High Activity of Pd/Graphene Catalysts for Ethanol Electrocatalytic Oxidation[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1570-1574
109. GAN Lin, LIU Song, LI Dan-Na, GU Hang, CAO Yang, SHEN Qian, WANG Zhen-Xing, WANG Qing, GUO Xue-Feng.Facile Fabrication of the Crossed Nanotube-Graphene Junctions[J]. Acta Phys. -Chim. Sin., 2010,26(04): 1151-1156
110. JIANG Lei, HUANG Hui, WANG Chun-Tao, ZHANG Wen-Kui, GAN Yong-Ping, TAO Xin-Yong.Photoelectrochromic Properties of TiO2-xNx/NiO Bilayer Thin Films[J]. Acta Phys. -Chim. Sin., 2010,26(02): 299-303
111. TANG Jun, LIU Zhong-Liang, KANG Chao-Yang, YAN Wen-Sheng, XU Peng-Shou, PAN Hai-Bin, WEI Shi-Qiang, GAO Yu-Qiang, XU Xian-Gang.Annealing Time Dependence of Morphology and Structure of Epitaxial Graphene on 6H-SiC(0001) Surface[J]. Acta Phys. -Chim. Sin., 2010,26(01): 253-258
112. LI Wen, LENG Wen-Hua, NIU Zhen-Jiang, LI Xiang, FEI Hui, ZHANG Jian-Qing, CAO Chu-Nan.Enhanced Photoelectrochemical Performance of WO3 Film Electrode under Visible Light by Electrochemical Etching Fluorination in Aqueous Solutions Containing Fluorine[J]. Acta Phys. -Chim. Sin., 2009,25(12): 2427-2432
113. YU Yong, LIU Shi-Jun, LI Jie, CHEN Qi-Yuan.Preparation and Characterization ofMesoporous Tungsten Oxides[J]. Acta Phys. -Chim. Sin., 2009,25(09): 1890-1894
114. YUAN Jia-Guo; ZHANG Yu-Zhi; LE Jun; SONG Li-Xin; HU Xing-Fang.Spectrum Investigations of Chloro-Alkoxide Sol-Gel Nanostructured Tungsten Oxide Thin Films[J]. Acta Phys. -Chim. Sin., 2009,25(02): 267-272
115. YU Zhi-Yong; ZHANG Wei; MA Ming; CUI Xiao-Li.Visible Light Photoelectrochemical Response of Nitrogen-Doped TiO2 Thin Films Prepared by Anodic Oxidation of Titanium Nitride Films[J]. Acta Phys. -Chim. Sin., 2009,25(01): 35-40
116. ZHANG Wei; CUI Xiao-Li; JIANG Zhi-Yu.Effect of Composite Modes on Photoelectrochemical Properties of MWCNTs/TiO2 Nanocomposite Films[J]. Acta Phys. -Chim. Sin., 2008,24(11): 1975-1980
117. CHEN Qiao-Lin; ZHOU Jian-Zhang; LIANG Jin-Ling; LIN Ling-Ling; LIN Zhong-Hua.Spectroscopic and Photoelectrochemical Properties of DNA/CdS Nanoparticle Composites[J]. Acta Phys. -Chim. Sin., 2008,24(05): 749-754
118. ZHU Lv-Jun; XU Qun-Jie; CAO Wei-Min; WAN Zong-Yue; ZHOU Guo-Ding; LIN Chang-Jian.Photoelectrochemical Study on the Complex of PASP and Tungstate as Inhibitors of Cupronickel B10’s Corrosion[J]. Acta Phys. -Chim. Sin., 2008,24(05): 805-809
119. SU Zhao-Hui; CHEN Qi-Yuan; LI Jie; LIU Shi-Jun.Preparation and Characterization of Mesoporous Silicon Dioxide Doped with Tungsten[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1760-1764
120. MAN Yi; ZONG Rui-Long; ZHU Yong-Fa.Preparation and Photoelectrochemical Properties of Bi2MoO6 Films[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1671-1676
121. ZHU Lei; CUI Xiao-Li; SHEN Jie; YANG Xi-Liang; ZHANG Zhuang-Jian.Visible Light Photoelectrochemical Response of Carbon-doped TiO2 Thin Films Prepared by DC Reactive Magnetron Sputtering[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1662-1666
122. MA Na; JI Sheng-Fu; WU Ping-Yi; HU Lin-Hua; NIE Ping-Ying.Preparation, Characterization and Catalytic Performance for Hydrodesulfurization of WxC/SBA-16 Catalysts[J]. Acta Phys. -Chim. Sin., 2007,23(08): 1189-1194
123. TAI Hui-Ling; JIANG Ya-Dong; XIE Guang-Zhong; DU Xiao-Song; CHEN Xuan.Preparation and Gas Sensitive Properties of Polyaniline/Titanium Oxide Composite Thin Films[J]. Acta Phys. -Chim. Sin., 2007,23(06): 883-888
124. MA Liang; MA Jie; LIU Hui.Composite Electrodeposition of CoNiP-BaFe12O19Magnetic Thin Film[J]. Acta Phys. -Chim. Sin., 2007,23(04): 590-594
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126. ZHOU Yong-Ning;WU Chang-Liang;ZHANG Hua;WU Xiao-Jing;FU Zheng-Wen.The Electrochemical Properties of LiF-Ni Nanocomposite Thin Film[J]. Acta Phys. -Chim. Sin., 2006,22(09): 1111-1115
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128. HAO Yan-Zhong; HAN Wen-Tao.Preparation and Photoelectrochemical Properties of Titanate Nanotubes[J]. Acta Phys. -Chim. Sin., 2006,22(02): 221-225
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130. SHI Jing-ying; LENG Wen-hua; CHENG Xiao-fang; ZHANG Jian-qing; CAO Chu-nan.Photocatalytic Oxidation of Methyl Red by TiO2 in a Photoelectrochemical Cell[J]. Acta Phys. -Chim. Sin., 2005,21(09): 971-976
131. BAO Xing-Wang;ZHANG Jin-Long;LIANG Xue-Hai;HUANG Jia-Zhen;ZHANG Li-Zhong.Preparation of TiO2 Thin Films at Low Temperature and Characterization of Their Properties[J]. Acta Phys. -Chim. Sin., 2005,21(01): 69-73
132. Guo Jia-Hao;He Xiao-Ying;Guo Min;Cai Sheng-Min;Chen Xiu-Ying;Peng Xiao-Jun.Photoelectrochemical Studies of the TiO2 Nanocrystalline Electrode Sensitized by Novel Cyanine Dye[J]. Acta Phys. -Chim. Sin., 2004,20(08): 849-853
133. Zhang Qi;Li Xin-Jun;Li Fang-Bai;Chang Jie.Investigation on Visible -light Activity of WOx/TiO2 Photocatalyst[J]. Acta Phys. -Chim. Sin., 2004,20(05): 507-511
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136. Zhou Guo-Ding;Kamkin A N;Liao Qiang-Qiang.Photoelectrochemical Study of Copper-Nickel and Copper-Cobalt Electrodes in Alkaline Solution[J]. Acta Phys. -Chim. Sin., 2001,17(07): 614-618
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156. LI Guang-Yong, WU Xiao-Han, HE Wei-Na, FANG Jian-Hui, ZHANG Xue-Tong.Controlled Assembly of the Graphene-based Aerogel[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
157. WANG Cheng-Xian, YU Fei, MA Jie.Applications of Graphene-based Hybrid Material as Electrodes in Microbial Fuel Cells[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
158. ZHU Jie-Jun, SUN Hai-Bin, WU Yao-Zheng, WAN Jian-Guo, WANG Guang-Hou.Graphene: Synthesis, Characterization and Application in Transparent Conductive Films[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
159. WANG Yun-Jing, LIU Ying-Qiu, GAO Xiu-Xiu, ZHAN Yan-Shan, PAN Li-Yang, ZHANG Wen-Kai, FANG Xiao-Min.Surface Defects Passivation of Graphene Quantum Dots by Amino Functionalization and its Photoluminescence Emission Enhancement[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
160. LIANG Jia-Xu, XIAO Zhi-Chang, ZHI Lin-Jie.Graphenal Polymers: 3D Carbon-rich Polymers as Energy Materials with both Electronic and Ionic Transport Path[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
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