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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2015,Vol.31>> Issue(3)>> 576-582     doi: 10.3866/PKU.WHXB201501201         中文摘要
PHYSICAL CHEMISTRY OF MATERIALS
Optical and Electrical Properties of CH3NH3PbI3 Perovskite Thin Films Transformed from PbO-PbI2 Hybrid Films
DING Xu-Kun, LI Xiao-Min, GAO Xiang-Dong, ZHANG Shu-De, HUANG Yu-Di, LI Hao-Ran
State Key Laboratory of High Performance Ceramics and Superfine Microstructures, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050, P. R. China
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Organic-inorganic halide perovskites have been shown to be outstanding photovoltaic materials, achieving remarkably high power conversion efficiency (15%) of sunlight to electricity within the past 4 years. The controllable synthesis of organic- inorganic halide perovskites is fundamental to their applications in photovoltaic devices. Here we explore a novel strategy to prepare a typical halide peroskite CH3NH3PbI3 by transforming PbO-PbI2 hybrid materials. CH3NH3PbI3 thin films were deposited on glass substrates by reacting ultrasonic-assisted successive ionic layer adsorption and reaction (SILAR)-derived PbO-PbI2 hybrid films with CH3NH3I vapor at 110 ℃. The microstructure and crystallinity of the films, together with the optical and electrical properties were characterized. Results show that CH3NH3PbI3 thin films possess perovskite crystal structure and uniform surface morphology with grain size up to 400 nm. In the visible band, CH3NH3PbI3 thin films showed low transmittance (below 10%), with a band gap of 1.58 eV. The surface resistivity of CH3NH3PbI3 thin films was as high as 1000 MΩ, indicating the dielectric nature of obtained CH3NH3PbI3 films, with a dielectric constant of εr(100 Hz)=155 on low frequency. The current work opens an effective route toward high quality organicinorganic halide perovskite films with good crystallinity and optical properties, which make them suitable for application in photovoltaic devices, and other optical and electrical applications.



Keywords: CH3NH3PbI3   Thin film   Perovskite   Successive ionic layer adsorption and reaction   Vapor process   Photovoltaic material  
Received: 2014-11-13 Accepted: 2015-01-19 Publication Date (Web): 2015-01-20
Corresponding Authors: LI Xiao-Min Email: lixm@mail.sic.ac.cn

Fund: The project was supported by the National Natural Science Foundation of China (50502038, 10576036).

Cite this article: DING Xu-Kun, LI Xiao-Min, GAO Xiang-Dong, ZHANG Shu-De, HUANG Yu-Di, LI Hao-Ran. Optical and Electrical Properties of CH3NH3PbI3 Perovskite Thin Films Transformed from PbO-PbI2 Hybrid Films[J]. Acta Phys. -Chim. Sin., 2015,31 (3): 576-582.    doi: 10.3866/PKU.WHXB201501201

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68. LI Wen-Zhang, LI Jie, WANG Xuan, ZHANG Shu-Juan, CHEN Qi-Yuan.Photoelectrochemical Properties of Cubic Tungsten Trioxide Films Obtained by the Polymeric Precursor Method[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2343-2348
69. ZHU Yan-Feng, DU Rong-Gui, LI Jing, QI Hai-Qing, LIN Chang-Jian.Photogenerated Cathodic Protection Properties of a TiO2 Nanowire FilmPrepared by a Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2349-2353
70. SUN Wen-Li, XU Jun, LU Wen-Qi.Chemical Structure and Growth Mechanism of a-SixC1-x:H Films Prepared by Plasma Enhanced Magnetron Sputtering[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2311-2316
71. CHAO Wen-Liu, WAN Yong, WANG Yun-Xia, LIU Chang-Song.Tribological Properties of Cu-Doped TiO2 Films[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2317-2322
72. SHEN Qian, GAN Lin, LIU Song, CAO Yang, WANG Zhen-Xing, HUI Jing-Shu, GUO Xue-Feng.Reversible Photomodulation of Organic Transistor Performance by Conformation-Induced Capacitive Coupling[J]. Acta Phys. -Chim. Sin., 2010,26(07): 1941-1946
73. YANG Chang-Hu, MA Zhong-Quan, LI Feng, HE Bo, YUAN Jian-Hui, ZHANG Zhen-Hua.Spectrum Analysis on Phase Transformations in TiO2 Thin Films[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1349-1354
74. YUAN Wei-Zhong, ZHANG Feng-Bo, YUAN Jin-Ying, XIE Xu-Ming, HONG Xiao-Yin.Effect ofMolecular Structure on the Surface Morphology of Ultrathin Films by Competing Crystallization and Dewetting Processes[J]. Acta Phys. -Chim. Sin., 2010,26(04): 1157-1163
75. JIANG Lei, HUANG Hui, WANG Chun-Tao, ZHANG Wen-Kui, GAN Yong-Ping, TAO Xin-Yong.Photoelectrochromic Properties of TiO2-xNx/NiO Bilayer Thin Films[J]. Acta Phys. -Chim. Sin., 2010,26(02): 299-303
76. WANG Xiao-Yan, DONG Gui-Fang, QIAO Juan, WANG Li-Duo, QIU Yong.Preparation and Field-Effect Property of Solution-Processed Multilayer Zinc Oxide[J]. Acta Phys. -Chim. Sin., 2010,26(01): 249-252
77. LI Zhen-Hua, JIANG Yuan, ZHAO Pei, SHANG Xue-Fu, YANG Hui, WANG Miao.Synthesis of Single-Walled Carbon Nanotube Films with Large Area and High Purity by Arc-Discharge[J]. Acta Phys. -Chim. Sin., 2009,25(11): 2395-2398
78. CHEN Xun, GENG Qiang, LIU Jun-Feng, DING Zheng-Xin, DAI Wen-Xin, WANG Xu-Xu.Influence of Conducting Substrates on the Photoinduced Hydrophilicity of TiO2 Films[J]. Acta Phys. -Chim. Sin., 2009,25(11): 2237-2242
79. QU Shao-Hua, JIA Li-Hui.Mechanical Properties of Si/DLC Films on Au and Au-Cu Substrates[J]. Acta Phys. -Chim. Sin., 2009,25(11): 2391-2394
80. ZHANG Jing-Yu, LIU Qing-Feng, LIU Qian.Combinatorial Optimization for the Anti-Corrosion Properties of Ti Doped Zn-Al Alloy Films[J]. Acta Phys. -Chim. Sin., 2009,25(09): 1763-1768
81. DONG Xiang, TAO Jie, LI Ying-Ying, WANG Tao, ZHU Hong.Photoelectrochemical Properties of Three-Dimensional Network TiO2 Nanowire Film Prepared by Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2009,25(09): 1874-1882
82. LIANG Ji-Ran, HU Ming, WANG Xiao-Dong, LI Gui-Ke, JI An, YANG Fu-Hua, LIU Jian, WU Nan-Jian, CHEN Hong-Da.Fabrication and Infrared Optical Properties of Nano Vanadium Dioxide Thin Films[J]. Acta Phys. -Chim. Sin., 2009,25(08): 1523-1529
83. CAO Yong-Qiang, LONG Hui-Jin, CHEN Yong-Mei, CAO Ya-An.Photocatalytic Activity of TiO2 Films with Rutile/Anatase Mixed Crystal Structures[J]. Acta Phys. -Chim. Sin., 2009,25(06): 1088-1092
84. WANG Hao, ZHONG Cheng, JIANG Cheng-Jie, GU Xiong, LI Jin, JIANG Yi-Ming.Electrochemical Behavior of ITO Films during Anodic and Cathodic Polarization in Sodium Hydroxide Solutions[J]. Acta Phys. -Chim. Sin., 2009,25(05): 835-839
85. YUAN Jia-Guo; ZHANG Yu-Zhi; LE Jun; SONG Li-Xin; HU Xing-Fang.Spectrum Investigations of Chloro-Alkoxide Sol-Gel Nanostructured Tungsten Oxide Thin Films[J]. Acta Phys. -Chim. Sin., 2009,25(02): 267-272
86. ZHANG Hong-Wei, ZHANG Zheng-Fu, LI Yang, YANG Xi-Hun, LIU Shuo.Structural Effects and Electrooxidation Activity of a Two-Dimensional Multilayer PtRu/PtNd Alloy Nanostructure Thin Film[J]. Acta Phys. -Chim. Sin., 2008,24(12): 2268-2274
87. GAO Cheng-Yao; CHANG Ming.Ta/BDD Film Electrode for Electrochemical Oxidation Nitrophenol[J]. Acta Phys. -Chim. Sin., 2008,24(11): 1988-1994
88. ZHAO Feng-Ming; SHEN Hai-Ping; CHEN Zhao-Yang; MA Chun-An.Electrocatalytic Reduction of Maleic Acid at Bundles of TiO2 Anodization Film[J]. Acta Phys. -Chim. Sin., 2008,24(11): 2139-2142
89. HUO Wei-Liang; LIU Qing-Feng; LIU Qian; ZHU Li-Hui; WANG Li.Application of Combinatorial Material Chip Method in Screening of Anticorrosion Zn-Al Alloy[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1703-1708
90. WANG Shuo; LUO Chong; ZHAO Ying; XIONG Shao-Zhen.Al-Induced Crystallization of Polycrystalline Silicon Thin Films Based on Solution Method[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1689-1693
91. HUANG Jun-Jie; JIANG Zhi-Yu.Electrochemical Performance of LiMn2O4 Thin Film Electrode Fabricated by Ink-Jet Printing Technique[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1563-1567
92. ZHANG Hua; ZHOU Yong-Ning; WU Xiao-Jing; FU Zheng-Wen.Electrochemical Properties of CuF2 Films Fabricated by Pulsed Laser Deposition[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1287-1291
93. AO Jian-Ping; SUN Guo-Zhong; YAN Li; KANG Feng; YANG Liang; HE Qing; ZHOU Zhi-Qiang; LI Feng-Yan; SUN Yun.Properties of One-Step Electrodeposited Cu(In1-x, Gax)Se2 Thin Films[J]. Acta Phys. -Chim. Sin., 2008,24(06): 1073-1079
94. TANG Yu-Xin; TAO Jie; TAO Hai-Jun; WU Tao; WANG Ling; ZHANG Yan-Yan; LI Zhuan-Li; TIAN Xi-Lin.Fabrication and Characterization for Transparent Electrodes of TiO2 Nanotube Arrays on Fluorine-Doped Tin Oxide-Coated Glass[J]. Acta Phys. -Chim. Sin., 2008,24(06): 1120-1126
95. WANG Lin; CHEN Shun-Quan; LIU Yuan.NiO/LaMnO3 Catalysts for Steam Reforming of Ethanol[J]. Acta Phys. -Chim. Sin., 2008,24(05): 849-854
96. WANG Zhu-Yi; CHEN Cheng; FENG Cai-Hui; WANG Jin-Xing; ZOU Bo; ZHAO Meng; WU Feng-Qing.Synthesis, Characterization and Humidity Sensitive Properties of Nanocrystalline LaCoxFe1-xO3[J]. Acta Phys. -Chim. Sin., 2008,24(03): 375-378
97. MIAO Yue; YUAN Hong-Kuan; CHEN Hong.Electronic Structure and Magnetism of Double Perovskite Sr2-xLaxCrReO6[J]. Acta Phys. -Chim. Sin., 2008,24(03): 448-452
98. BULGAN G.; LIANG Shu-Hui; TENG Fei; YAO Wen-Qing; ZHU Yong-Fa.Effect of Ce Doping on the Structure and Catalytic Activity of La1-xCexCoO3 Catalysts[J]. Acta Phys. -Chim. Sin., 2008,24(02): 205-210
99. HU Jing; YANG Mei-Ni; LU Feng-Ting; DING Li-Ping; ZHANG Shu-Juan; FANG Yu.Monolayer Assembly of Pyrene on Glass Plate Surface and Its Selective Sensing Performances to Organic Copper (II) Salts[J]. Acta Phys. -Chim. Sin., 2007,23(12): 1839-1845
100. CHU Yan-Qiu; WU Bo; WU Liang; SHUI Qing; FU Zheng-Wen.Electrochromic Properties of Bismuth Oxide Thin Films Prepared by Reactive Pulsed Laser Deposition[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1787-1791
101. MAN Yi; ZONG Rui-Long; ZHU Yong-Fa.Preparation and Photoelectrochemical Properties of Bi2MoO6 Films[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1671-1676
102. ZHU Lei; CUI Xiao-Li; SHEN Jie; YANG Xi-Liang; ZHANG Zhuang-Jian.Visible Light Photoelectrochemical Response of Carbon-doped TiO2 Thin Films Prepared by DC Reactive Magnetron Sputtering[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1662-1666
103. ZHANG Wei; WANG Shu-Liang; MA Yun-Qing; WANG Cui-Ping; LIU Xing-Jun.Influence of Interface Diffusion between Al Substrate and TiO2 Filmon Photocatalytic Activity[J]. Acta Phys. -Chim. Sin., 2007,23(09): 1347-1352
104. BULGAN G.; TENG Fei; LIANG Shu-Hui; YAO Wen-Qing; ZHU Yong-Fa.Effect of Cu Doping on the Structure and Catalytic Activity of LaMnO3 Catalyst[J]. Acta Phys. -Chim. Sin., 2007,23(09): 1387-1392
105. YUAN Hao; LI Qing-Hua; SHA Fei; XIE Li-Li; TIAN Zhen; WANG Li-Jun.Application of Ultraviolet Treatment in the Synthesis of Pure-silica Zeolite Thin Films with Low Dielectric Constant[J]. Acta Phys. -Chim. Sin., 2007,23(08): 1219-1223
106. LI Shi-Bin; WU Zhi-Ming; ZHU Kui-Peng; JIANG Ya-Dong; LI Wei; LIAO Nai-Man.Effect of Substrate Temperature on the Optical Properties of a-Si:H Films by RF-PECVD[J]. Acta Phys. -Chim. Sin., 2007,23(08): 1252-1256
107. YANG Hui; SHEN Qian-Hong; GAO Ji-Wei.Morphology Control of Anatase TiO2 Films Prepared at Low Temperature Using 4,4’-isopropylidenediphenol[J]. Acta Phys. -Chim. Sin., 2007,23(08): 1269-1274
108. ZHANG Hong-Fang; FU Ping-Ping; SONG Ying-Jie; DU Chen-Shu; YANG Hua-Bin; ZHOU Zuo-Xiang; WU Meng-Tao; HUANG Lai-He.Preparation and Properties of Sandwich-type Si/Fe/Si Film Anode for Lithium-ion Battery[J]. Acta Phys. -Chim. Sin., 2007,23(07): 1065-1070
109. TAI Hui-Ling; JIANG Ya-Dong; XIE Guang-Zhong; DU Xiao-Song; CHEN Xuan.Preparation and Gas Sensitive Properties of Polyaniline/Titanium Oxide Composite Thin Films[J]. Acta Phys. -Chim. Sin., 2007,23(06): 883-888
110. WU Lun-Peng; ZHAO Lian-Hua; ZHANG Hai-Ming; ZHAO Qing-Nan.Effects of the Adsorption of Oxygen on the Photocatalytic Activity of TiO2 Films Using PhotocurrentMethod[J]. Acta Phys. -Chim. Sin., 2007,23(05): 765-768
111. WU Yan; YAO Wen-Qing; ZHU Yong-Fa.Interfacial Structure of Ta2O5/Si Filmand Photoactivity[J]. Acta Phys. -Chim. Sin., 2007,23(05): 625-629
112. YANG Ya-Jie; JIANG Ya-Dong; XU Jian-Hua.Preparation and Properties of Conducting Polymeric Ultrathin Films[J]. Acta Phys. -Chim. Sin., 2007,23(04): 484-488
113. FANG Shu-Mei; OU Yan; LIN Jing-Dong; LIAO Dai-Wei.Preparation of Cu/Sr3Ti2O7 and Its Photocatalytic Activity of Watersplitting for Hydrogen Evolution[J]. Acta Phys. -Chim. Sin., 2007,23(04): 601-604
114. MA Liang; MA Jie; LIU Hui.Composite Electrodeposition of CoNiP-BaFe12O19Magnetic Thin Film[J]. Acta Phys. -Chim. Sin., 2007,23(04): 590-594
115. YAN Shan-Shan;WU Lian-Di;CHEN Feng;ZHANG Jin-Long.Low-temperature Preparation and Characterization of TiO2 Thin Films with a Bicrystalline Framework[J]. Acta Phys. -Chim. Sin., 2007,23(03): 414-418
116. YANG Xi-Kun;LI Yang;HENG Gen-Hua.Structure and Catalytic Properties of PtRu Alloy Thin-film[J]. Acta Phys. -Chim. Sin., 2007,23(03): 389-393
117. GAO Li-Ning;LU Feng-Ting;HU Jing; FANG; Yu.Progress in the Studies of Fluorescent Film Sensors[J]. Acta Phys. -Chim. Sin., 2007,23(02): 274-284
118. ZHANG Shi-Cheng;YAO Wen-Qing;ZHU Yong-Fa;SHI Li-Yi.Preparation and Photoelectrochemical Properties of Bi2WO6 Films with Visible Light Response[J]. Acta Phys. -Chim. Sin., 2007,23(01): 111-115
119. LIU Wen-Yuan;LI Chi-Lin;FU Zheng-Wen .Stability of Lithium Phosphorous Oxynitride Thin Films in Humid Air[J]. Acta Phys. -Chim. Sin., 2006,22(11): 1413-1418
120. ZHOU Yong-Ning;WU Chang-Liang;ZHANG Hua;WU Xiao-Jing;FU Zheng-Wen.The Electrochemical Properties of LiF-Ni Nanocomposite Thin Film[J]. Acta Phys. -Chim. Sin., 2006,22(09): 1111-1115
121. CHEN Ming-An;XIE Xuan;QI Hai-Ying;ZHANG Xin-Ming;LI Hui-Zhong;YANG Xi .Characterization of Self-assembled Bis-[triethoxysilylpropyl]tetrasulfide Silane Films on Surface of 2A12-T6 Aluminum Alloy[J]. Acta Phys. -Chim. Sin., 2006,22(08): 1025-1029
122. ZHAO Feng-Ming;MA Chun-An;CHU You-Qun;XU Ying-Hua.Oxygen Reduction on Ni-MnO2 Electrode in Alkaline Solution[J]. Acta Phys. -Chim. Sin., 2006,22(06): 716-720
123. ZHONG Cheng;JIANG Yi-Ming;LUO Yu-Feng;LIAO Jia-Xing;WU Wei-Wei;LI Jin.Two New Methods for Characterizing the Kinetics of the Complexation of Metal/Organic Thin Films and Oxidation of Metal Thin Films[J]. Acta Phys. -Chim. Sin., 2006,22(06): 696-700
124. ZHOU Li-Jun;YAN Shan-Shan;TIAN Bao-Zhu;CHEN Feng;ZHANG Jin-Long;HUANG Jia-Zhen.Preparation and Characterization of Anatase-Brookite TiO2 Film on the PET Surface[J]. Acta Phys. -Chim. Sin., 2006,22(05): 569-573
125. XUE Ming-Zhe; CHENG Sun-Chao; YAO Jia; FU Zheng-Wen.Electrochemical Properties of SnSe Thin Film Electrode Fabricated by Pulsed Laser Deposition[J]. Acta Phys. -Chim. Sin., 2006,22(03): 383-387
126. LI Hai-Ling; WANG Wen-Jing; KANG Guo-Hu; HUANG Jin-Zhao; XU Zheng.The Effect of Reactive Pressure to Fe:NiOx Film as Anode Catalytic Film in Hydrogen Producing System by Solar Cell[J]. Acta Phys. -Chim. Sin., 2006,22(03): 330-334
127. SHI Jian-zhen; FANG Jing-huai; MU Ren-wang; LI Ya-li.Preparation of Au Core-Ag Shell Nanoparticles Film and Its SERS Activity Study[J]. Acta Phys. -Chim. Sin., 2006,22(02): 135-140
128. WANG Ying; LIU Wen-yuan; FU Zheng-wen.Electrochemistry of Mn4N with Lithium[J]. Acta Phys. -Chim. Sin., 2006,22(01): 65-70
129. CHEN Yong-Hong;WEI Yi-Jun;ZHONG Hong-Hai;GAO Jian-Feng;LIU Xing-Qin;MENG Guang-Yao.Synthesis and Properties of La0.5RE0.3Sr0.2FeO3-δ (RE = Nd, Ce, Sm) System with Two Rare Earths for Cathodes[J]. Acta Phys. -Chim. Sin., 2005,21(12): 1357-1362
130. DAI Wen-xin; WANG Xu-xu; FU Xian-zhi; LIU Ping; LIN Hua-xiang.Effect of Halides on Photo-induced Hydrophilicity over TiO2 Films[J]. Acta Phys. -Chim. Sin., 2005,21(11): 1274-1279
131. LIU Ping; JIANG Yi-ming; GUO Feng; XIE Heng-bo; LI Jin.Studies on the Transport Behavior in Ag/TCNQ Thin Films[J]. Acta Phys. -Chim. Sin., 2005,21(10): 1073-1075
132. PENG Feng; CHEN Shui-hui; ZHANG Lei; WANG Hong-juan; XIE Zhi-yong.Preparation of Visible-light Response Nano-sized ZnO Film and Its Photocatalytic Degradation to Methyl Orange[J]. Acta Phys. -Chim. Sin., 2005,21(08): 944-948
133. XUE Ming-zhe; FU Zheng-wen.Electrochemical Properties of LiFePO4 Cathode Thin Film Fabricated by Pulsed Laser Deposition[J]. Acta Phys. -Chim. Sin., 2005,21(07): 707-710
134. XIONG Yu-hua; LI Feng-yi.Degradation of Polyethylene Film by Fe3+/TiO2 Photocatalyst[J]. Acta Phys. -Chim. Sin., 2005,21(06): 607-611
135. CHEN Zhi-gang; TANG Yi-wen; ZHANG Li-sha; CHEN Zheng-hua; JIA Zhi-jie.Electrochemical Deposition and Characterization of Zinc Oxide Thin Films[J]. Acta Phys. -Chim. Sin., 2005,21(06): 612-615
136. LI Jian-Kang; YAO Xi.

Preparation and Study on Pb(ZrxTi1-x)O3 Ferroelectric Thin Films and Compositionally Graded Thin Films on LaNiO3/Si Substrates

[J]. Acta Phys. -Chim. Sin., 2005,21(05): 512-516

137. BAO Xing-Wang;ZHANG Jin-Long;LIANG Xue-Hai;HUANG Jia-Zhen;ZHANG Li-Zhong.Preparation of TiO2 Thin Films at Low Temperature and Characterization of Their Properties[J]. Acta Phys. -Chim. Sin., 2005,21(01): 69-73
138. Wang Juan; Zhang Chang-Rui; Feng Jian.Modification of Nanoporous Silica Film by Trimethylchlorosilane[J]. Acta Phys. -Chim. Sin., 2004,20(12): 1399-1403
139. Yu Chun-Ling;Zhai Jin;Ge Hong-Li;Wan Mei-Xiang;Jiang Lei;Li Ze-Sheng;Li Tie-Jin.Ordered Self-assembly of Polymer Nano-structure[J]. Acta Phys. -Chim. Sin., 2004,20(10): 1258-1261
140. Wang Hai-Shui;Wang Yi-Bing;Xi Shi-Quan.A Review for the Preparation and Structural Characterization of Thin Films of Charge-Transfer Complexes[J]. Acta Phys. -Chim. Sin., 2004,20(10): 1281-1286
141. Shen Jie;Wo Song-Tao;Cui Xiao-Li;Cai Zhen-Wei;Yang Xi-Liang;Zhang Zhuang-Jian.Photoelectrochemical Characteristics of Nano-Titanium Dioxide Thin Films Prepared by RF Magnetron Sputtering[J]. Acta Phys. -Chim. Sin., 2004,20(10): 1191-1195
142. Cao Jiang-Lin;Leng Wen-Hua;Zhang Jian-Qing;Cao Chu-Nan.Adsorption Behavior and Photooxidation Kinetics of OH- at TiO2 Thin Film Electrodes[J]. Acta Phys. -Chim. Sin., 2004,20(07): 735-739
143. Ren Da-Sen;Bei Zong-Min;Huang Li;Shen Jie;Cui Xiao-Li;Yang Xi-Liang;Zhang Zhuang-Jian.The Effect of Dopant Sb on the Superhydrophilicity and the Microstructure of the Nanoscale TiO2 Thin Film[J]. Acta Phys. -Chim. Sin., 2004,20(04): 414-416
144. Liao Wei;Wei Fang;Cao Wei-Xiao;Zhao Xin-Sheng.Monitoring Layer-by-layer Assembling of Films Containing Diazo-resines by Attenuated Total Reflection Fourier Transform Infrared Spectroscopy[J]. Acta Phys. -Chim. Sin., 2004,20(04): 405-408
145. Chen You-Jiang;Sun Shi-Gang;Gong Hui;Chen Sheng-Pei;Zhou Zhi-You;Li Jun-Tao.Nanostructured Films Prepared on Pt Microelectrode through Square Wave Oxidation-reduction Cycles and Their Particular IR Properties[J]. Acta Phys. -Chim. Sin., 2004,20(02): 129-133
146. Tang Zhi-Yuan;Song Shi-Dong;Liu Jian-Hua;Pan Li-Zhu;Nan Jun-Min.Electrochemical Properties of La1-xSrxNi1-yCoyO3 Bifunctional Oxygen Electrodes[J]. Acta Phys. -Chim. Sin., 2003,19(09): 785-790
147. Ren Da-Sen;Cui Xiao-Li;Zhang Qun;Wo Song-Tao;Yang Xi-Liang;Zhang Zhuang-Jian;Lu Ming.Characteristics of SiO2-TiO2 Complex Thin Films Prepared by Sol Method[J]. Acta Phys. -Chim. Sin., 2003,19(09): 829-833
148. Liang Xin-Yi;Zhang Li-Ming;Ding Hong-Yuan;Qin Yong-Ning.Supported Catalyst LaCoO3/γ-Al2O3 Prepared by Impregnating under Ultrasound[J]. Acta Phys. -Chim. Sin., 2003,19(07): 666-669
149. Wang Shan;Fang Yu;Zhang Ying;Wang MingZhen;Hu DaoDao;Liao YiKun.Preparation of Chitosan/CdS Composite Films and Their Sensing Properties to Pyridine[J]. Acta Phys. -Chim. Sin., 2003,19(06): 514-518
150. Zhang Wen-Kui;Yang Xiao-Guang;Wang Yun-Gang;Yu Li-Yang;Ma Chun-An.Electrochemical Behaviors of Pd/Mm Rare Earth Film Electrodes in KOH Solution[J]. Acta Phys. -Chim. Sin., 2003,19(06): 569-572
151. Zhang Xi-Yao;Pan Xin-Yu;Zhang Qi-Feng;Xu Bei-Xue;Jiang Hong-Bing;Liu Chun-Ling;Gong-Qi-Huang;Wu Jin-Lei.Synthesis of Silver Oxide Nano-scale Thin Films and Photoactivated Dynamic Luminescence from Their Nanoparticles[J]. Acta Phys. -Chim. Sin., 2003,19(03): 203-207
152. Cui Xiao-Li;Jiang Zhi-Yu.Electrochemical Behavior of ITO/TiO2 Electrode under UV Illumination[J]. Acta Phys. -Chim. Sin., 2002,18(11): 1014-1017
153. Zhao Zhuan-Qing;Yao Su-Wei;Zhang Wei-Guo;Gong Zheng-Lie.Preparation and Photoelectrochemical Performance of Photoelectrode of TiO2 Film on Nickel[J]. Acta Phys. -Chim. Sin., 2002,18(05): 473-476
154. Zhang Sheng-Mao;Gao Yong-Jian;Zhang Zhi-Jun;Dang Hong-Xin;Liu Wei-Min;Xue Qun-Ji.Preparation and Characterization of Selfassembly Nanocomposite Thin Film[J]. Acta Phys. -Chim. Sin., 2002,18(05): 451-454
155. Zhao Wen-Kuan;Fang You-Ling.Synthesis of Photocatalytic Activity TiO2 Thin Films at LowTemperature[J]. Acta Phys. -Chim. Sin., 2002,18(04): 368-371
156. Ma Jian-Hua;Wu Guang-Ming;Cheng Yin-Bing;Sun Qi;Wang Jun-Ling;Shen Jun;Wang Jue.Preparation of Hydrophobic Optical Silica Thin Film with Sol-gel Method[J]. Acta Phys. -Chim. Sin., 2001,17(12): 1112-1116
157. Yu Hai-Hu;Wu Hong-Biao;Li Xiao-Fu;Zhu Yun-Zhou;Jiang De-Sheng.Self-assembly and Optical Properties of Silica Nanoparticulate Thin Films[J]. Acta Phys. -Chim. Sin., 2001,17(12): 1057-1061
158. Xiao Xu-Rui;Zhang Jing-Bo;Lin Yuan;Yin Feng;Li Xue-Ping.Study of the Kinetics of Nanocrystalline Semiconductor Thin Film Electrode Processes by Intensity Modulated Photocurrent Spectroscopy[J]. Acta Phys. -Chim. Sin., 2001,17(10): 918-923
159. Li Liao-Sha;Sui Zhi-Tong.Physical Chemistry Behavior of Enrichment Selectivity of TiO2 in Perovskite[J]. Acta Phys. -Chim. Sin., 2001,17(09): 845-849
160. Zhang Li;Ren Yan-Jie;Cai Sheng-Min.Photoelectrochromism of Dyesensitized Nanoporous TiO2 Film Combined with Electrodeposited MoO3 Film[J]. Acta Phys. -Chim. Sin., 2001,17(09): 817-819
161. Weng Duan;Ding Hong-Mei;Wu Xiao-Dong;Xu Lu-Hua;Chen Zhen.Catalytic Performance of Rare Earth Nanometer Materials LaMnO3+ë[J]. Acta Phys. -Chim. Sin., 2001,17(03): 248-251
162. Yu Jia-Guo;Zhao Xiu-Jian;Chen Wen-Mei;Lin Li;Zhang Ai-Li.Photocatalytic Activity and Hydrophilic Property of TiO2/SiO2 Composite Nanometer Thin Films[J]. Acta Phys. -Chim. Sin., 2001,17(03): 261-264
163. Zhang Yu-Zhi;Kuai Su-Lan;Huang Yin-Song;Wang Zhong-Chun;Hu Xing-Fang.X-ray Photoelectron Spectroscopic Study on Electrochromic Molybdenum Oxide Films[J]. Acta Phys. -Chim. Sin., 2001,17(01): 79-82
164. Wu Wei-Dong;Zhang Zhan-Wen;Luo Jiang-Shan;Tang Yong-Jian;Zheng Yong-Ming;Lu Xiao-Ming;Zhao Peng-Ji.Study of CuxC60 Film UV-Vis Absorption Spectrum[J]. Acta Phys. -Chim. Sin., 2001,17(01): 83-86
165. Yu Jia-Guo, Zhao Xiu-Jian, Zhao Qing-Nan.Preparation and Characterization of TiO2 Nnometer Thin Films by Sol-gel Process[J]. Acta Phys. -Chim. Sin., 2000,16(09): 792-797
166. Li Jian-Chang, Xue Zeng-Quan, Zhang Hao, Zeng Yan, Liu Wei-Min, Wu Quan-De.Chiral Fractal Patterns of TCNQ Thin Films Grown by Vacuum Evaporation[J]. Acta Phys. -Chim. Sin., 2000,16(07): 579-582
167. Li Jian-Chang, Song Yan-Lin, Xue Zeng-Quan, Liu Wei-Min, Jiang Lei, Zhu Dao-Ben.Microstructure and Electric Properties of Polyaniline-TCNQ Complex Thin Film Grown by Vacuum Evaporation[J]. Acta Phys. -Chim. Sin., 2000,16(04): 289-293
168. Wang Wei, Lin Guo-Dong, Zhang Hong-Bin, Xiong Zhi-Tao.Ag/La0.6Sr0.4MnO3 Catalysts for Deep Oxidation of CH4 and CH3OH at Low Concentrations[J]. Acta Phys. -Chim. Sin., 2000,16(04): 299-306
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171. Chen Chao-Hui, Yao Jian-Nian.Preparation of Photochromic WO3/4,4'-BPPOBp Superlattice Film[J]. Acta Phys. -Chim. Sin., 1999,15(10): 865-867
172. Jiang Li-Zhong, Zhou Ming-Fei, Liu Xian-Nian, Qin Qi-Fei.CeO2 Thin Film as a Lithium-ion-storage Mterial Fabricted by Pulsed Laser Deposition[J]. Acta Phys. -Chim. Sin., 1999,15(08): 752-756
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175. Zhong Chong-Min, Wang-De-Zheng, Takashi Ushikubo, Keisuke Wada.The Adsorption of Methanol,Water and Ethylene on a Niobium Oxide Thin Film[J]. Acta Phys. -Chim. Sin., 1998,14(03): 219-225
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