ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2015,Vol.31>> Issue(11)>> 2151-2157     doi: 10.3866/PKU.WHXB201510083         中文摘要
Growth, Electronic Structure and Thermal Stability of Ni on ZrO2(111) Thin Film Surfaces
HAN Yong, XU Qian, JU Huan-Xin, ZHU Jun-Fa
National Synchrotron Radiation Laboratory and Collaborative Innovation Center of Suzhou Nano Science and Technology, University of Science and Technology of China, Hefei 230029, P. R. China
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The growth mode, electronic structure, and thermal stability of Ni nanoparticles on thin ZrO2(111) film surfaces were investigated using X-ray photoelectron spectroscopy, ultraviolet photoelectron spectroscopy, and low-energy electron diffraction. Stoichiometric ZrO2(111) thin films with thickness of 3 nm were epitaxially grown on a Pt(111) single-crystal surface. The results indicate that the growth of Ni vapor deposited on thin ZrO2(111) films follows two-dimensional growth up to 0.5 ML (monolayer), followed by threedimensional growth (i.e., the Stranski-Krastanov growth mode). The Ni 2p3/2 binding energy (BE) increases with decreasing Ni coverage. We used the Auger parameter method to differentiate the contributions to this BE shift from the initial-state and final-state effects. The main contribution to the Ni 2p core level BE shift is made by the final-state effect. However, at low Ni coverages, the initial-state effect also contributes. This suggests that at the initial stage of Ni growth on the ZrO2(111) surface, Ni and ZrO2 interact strongly, leading to charge transfer from Ni to the ZrO2 substrate, with the appearance of partially positively charged Niδ+. Thermal stability studies of Ni/ZrO2(111) model catalysts with two different coverages (0.05 and 0.5 ML) indicate further oxidation of Ni to Ni2+ and concurrent diffusion of Ni into the ZrO2 substrate at elevated temperatures. These findings provide an atomic-level fundamental understanding of the interactions between Ni with ZrO2, which is essential for identifying the structures of real ZrO2-supported Ni catalysts.

Keywords: Nickel   Zirconia   Model catalyst   X-ray photoelectron spectroscopy   Ultraviolet photoelectron spectroscopy  
Received: 2015-08-06 Accepted: 2015-10-08 Publication Date (Web): 2015-10-08
Corresponding Authors: ZHU Jun-Fa Email:

Fund: The project was supported by the National Natural Science Foundation of China (U1232102, 21403205) and National Key Basic Research Program of China (973) (2013CB834605).

Cite this article: HAN Yong, XU Qian, JU Huan-Xin, ZHU Jun-Fa. Growth, Electronic Structure and Thermal Stability of Ni on ZrO2(111) Thin Film Surfaces[J]. Acta Phys. -Chim. Sin., 2015,31 (11): 2151-2157.    doi: 10.3866/PKU.WHXB201510083

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62. LI Xue-Ling, YUE Bao-Hua, WANG Xue-Guang, YU Fei, KONG Ling-Hua, LU Xiong-Gang, DING Wei-Zhong.Preparation of NiO/MgxSi1-xOy Catalysts and Their Application in Catalytic Cracking of Tar Components in Hot Coke Oven Gas[J]. Acta Phys. -Chim. Sin., 2009,25(04): 762-766
63. XU Jun-Ke; LI Zhao-Jing; WANG Ji-Hui; ZHOU Wei; MA Jian-Xin.Characterization and Analysis of Carbon Deposited on the Surface of Ni/Al2O3 Catalyst for Methane Dry Reforming[J]. Acta Phys. -Chim. Sin., 2009,25(02): 253-260
64. XU Jun-Ke; REN Ke-Wei; WANG Xiao-Lei; ZHOU Wei; PAN Xiang-Min; MA Jian-Xin.Effect of La2O3 on Ni/γ-Al2O3 Catalyst for Biogas Reforming to Hydrogen[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1568-1572
65. RUAN Xiao-Yun; FANG Yun; FAN Ye.Preparation of Ultrafine Nickel Powders in SDS-PVP Aqueous Solution[J]. Acta Phys. -Chim. Sin., 2008,24(08): 1513-1518
66. MA Ying; CHEN Min; SONG Cui; ZHENG Xiao-Ming.Catalytic Oxidation of Toluene, Acetone and Ethyl Acetate on a New Pt-Pd/Stainless Steel Wire Mesh Catalyst[J]. Acta Phys. -Chim. Sin., 2008,24(07): 1132-1136
67. ZHANG Rui-Min; FAN Guang-Yin; LI Cheng; WANG Ying-Ying; LI Rui-Xiang; CHEN Hua; LI Xian-Jun.Hydrogenation of Quinoline over Ru/ZrO2·xH2O[J]. Acta Phys. -Chim. Sin., 2008,24(06): 965-970
68. ZHANG Jin; ZHANG Tong-Lai; YANG Li; ZHANG Jian-Guo; CUI Yan.Preparation, Crystal Structure and Thermal Decomposition Character of [Ni(CHZ)3]SO4·3H2O[J]. Acta Phys. -Chim. Sin., 2008,24(05): 760-766
69. WANG Lin; CHEN Shun-Quan; LIU Yuan.NiO/LaMnO3 Catalysts for Steam Reforming of Ethanol[J]. Acta Phys. -Chim. Sin., 2008,24(05): 849-854
70. QIAN Li-Ping; DENG Wen-Li.Adsorption Characteristics of Self-assembled 1-Octadecanol Layer on HOPG[J]. Acta Phys. -Chim. Sin., 2008,24(03): 443-447
71. CHEN Yu-Ting; ZHANG Hai-Yan; ZHANG Guo-Qing; CHEN Yi-Ming; ZHU Qing-Feng.Influence of Addition of Carbon Nanotubes in the Hydrogen Storage Alloy Electrode on the Performance of SC High Power Batteries[J]. Acta Phys. -Chim. Sin., 2008,24(03): 527-532
72. CHENG Zhi-Peng; YANG Yi; WANG Yi; LI Miao-Miao; LI Feng-Sheng.Oxidation Ability of Nanocrystalline Ni-Coated Al Powders[J]. Acta Phys. -Chim. Sin., 2008,24(01): 152-156
73. FENG Rui-Xiang; CAO Yu-Liang; AI Xin-Ping; YANG Han-Xi.AgNi Alloy Used as Anodic Catalyst for Direct Borohydride Fuel Cells[J]. Acta Phys. -Chim. Sin., 2007,23(06): 932-934
74. REN Jun-Xia; ZHOU Zhen; YAN Jie.Effects of Yttrium-Doping on High-temperature Electrochemical Performances of Nickel Hydroxide Electrodes[J]. Acta Phys. -Chim. Sin., 2007,23(05): 738-742
75. LI Cui-Ping;ZHAO Rui-Hong;GUO Fen;CHEN Jian-Feng.Preparation and Characterization of Ni Catalysts Supported on Organized Mesoporous Alumina[J]. Acta Phys. -Chim. Sin., 2007,23(02): 157-161
76. YU Dan-Mei;CHEN Chang-Guo;SI Yu-Jun;ZHOU Shang-Qi;WANG Li.Study on the Electronic Structure of Doped Nickel Hydroxide Using the DV-Xα Method of Quantum Chemistry[J]. Acta Phys. -Chim. Sin., 2007,23(01): 27-31
77. ZOU Ji-Jun;LIU Chang-Jun.Preparation of NiO/SrTiO3 with Cold Plasma Treatment for PhotocatalyticWater Splitting[J]. Acta Phys. -Chim. Sin., 2006,22(08): 926-931
78. GAO Jie;WANG Shi-Zhong.Study of Ni Composite Anodes for Dimethyl Ether Fuel Cell[J]. Acta Phys. -Chim. Sin., 2006,22(07): 851-855
79. CHEN Hu;XU Xing-You;GAO Jian;YANG Xu-Jie;LU Lu-De;WANG Xin.Study on Crystal Structure of [Ni(phen)3](ClO4)2[J]. Acta Phys. -Chim. Sin., 2006,22(07): 856-859
80. SUN Yuan-Hua;ZHANG Tong-Lai;ZHANG Jian-Guo;YANG Li;QIAO Xiao-Jing.Kinetics of Flash Pyrolysis of [Co(CHZ3](ClO42 and [Ni(CHZ)3](ClO4)2[J]. Acta Phys. -Chim. Sin., 2006,22(06): 649-652
81. NI Wen-Bin;LIU Tian-Qing;GUO Rong.Effect of SDS on the Electrochemical Oscillation of Nickel in HNO3/Cl-/H2O Solution[J]. Acta Phys. -Chim. Sin., 2006,22(04): 502-506
82. HU Yun-Wan;QIAN Hui-Qin;CHEN Qiao;MAO Hong-Ying;SONG Fei;HUANG Han;LI Hai-Yang;HE Pi-Mo;BAO Shi-Ning.The Thin Films Growth of Fluorescein on Ag(110)[J]. Acta Phys. -Chim. Sin., 2006,22(04): 470-474
83. ZHAO Peng; FANG Hui-jue; XUE Teng; QI Xi-min; LU Jia-xing.Diffusion Coefficients and Rate Constants of NiCl2(bpy)3 in DMF Determined by Chronocoulometry[J]. Acta Phys. -Chim. Sin., 2005,21(11): 1235-1239
84. FENG Shao-bin; SHANG Shi-bo; BAO Xiang; FENG Li-ting; ZHANG Jing-wei; LI Zong-hui.Study of Potential Activation Phenomenon and Initial Process of the Metal Electrodeposition[J]. Acta Phys. -Chim. Sin., 2005,21(05): 463-467
85. TAO Xiao-Jun; LI Zhi-Wei; CHEN Hong-Jie; ZHANG Ping-Yu; ZHANG Zhi-Jun; WU Zhi-Shen; DANG Hong-Xin.A New Approach to Synthesize Nickel Nanoparticles[J]. Acta Phys. -Chim. Sin., 2005,21(05): 569-572
86. WU Mei-Yin; WANG Jian-Ming; ZHANG Jian-Qing; CAO Chu-Nan.Structure and Electrochemical Performance of Mn-substituted Nickel Hydroxide[J]. Acta Phys. -Chim. Sin., 2005,21(05): 523-527
87. WANG Xiao-Feng; WANG Da-Zhi; LIANG Ji.Pseudo-capacitance of Ultrafine Nickel Hydroxide Prepared by Sol-gel Method[J]. Acta Phys. -Chim. Sin., 2005,21(02): 117-122
88. LIU Jian;ZHAO Zhen;XU Chun-Ming.The Structures of VOx/ZrO2 and K-VOx/ZrO2 Catalysts and Their Catalytic Performances for Diesel Soot Oxidation[J]. Acta Phys. -Chim. Sin., 2005,21(02): 156-160
89. Yang Fang-Zu;Ma Zhao-Hai;Huang Ling;Xu Shu-Kai;Zhou Shao-Min.Electrodeposition, Structure and Properties of an Amorphous Ni-W-B/ZrO2 Composite Coating[J]. Acta Phys. -Chim. Sin., 2004,20(12): 1411-1416
90. Ma Zhong-Yi;Xu Run;Yang Cheng;Wei Wei;Li Wen-Huai;Sun Yu-Han.Preparation and Surface Properties of Different Zirconia Polymorphs[J]. Acta Phys. -Chim. Sin., 2004,20(10): 1221-1225
91. Chen Ming-An;Zhang Xin-Ming;Xie Xuan.Interphase Analysis of Adhesion Bonded Aluminum Sheet/polypropylene and Maleic Anhydride Grafted Polypropylene by XPS[J]. Acta Phys. -Chim. Sin., 2004,20(08): 882-886
92. Huang Han;Yan Xin-Cheng;Mao Hong-Ying;Chen Qiao;Qian Hui-Qin;Zhang Jian-Hua;Li Hai-Yang;He Pi-Mo;Bao Shi-Ning.The Electronic States of Ordered Thin Film of Perylene on Ag (110)[J]. Acta Phys. -Chim. Sin., 2004,20(08): 892-896
93. Fu Tie-Xiang;Tao Jun;Li Dan.Synthesis and Gas Sensitive Properties of Mixed-Ligand Complex Ni(mnt)(bipyO2) with Big Conjugate System[J]. Acta Phys. -Chim. Sin., 2004,20(08): 843-848
94. Liu Ying-Xin;Wei Zuo-Jun;Chen Ji-Xiang;Zhang Ji-Yan;Li Xin-Xue;Wei Xiong-Hui.Sol-gel Preparation,Characterization and Hydrogenation Property of Silica Supported Ni Catalyst[J]. Acta Phys. -Chim. Sin., 2004,20(07): 780-784
95. Wang Qin-Ping;Lü Xing-Mei;Chen Hong-Tao;Zhou Li-Hua;Chen Shu-Sen;Lü Dian-Zhen.Activity Coefficients of HCl in the Nickel Sulfate Solution[J]. Acta Phys. -Chim. Sin., 2004,20(02): 186-190
96. Chen Ji-Xiang;Qiu Ye-Jun;Zhang Ji-Yan;Su Wan-Hua.Influence of La2O3 and CeO2 Promoters on Physico-chemical Properties and Catalytic Performance of Ni/MgO Catalyst in Methane Reforming with Carbon Dioxide[J]. Acta Phys. -Chim. Sin., 2004,20(01): 76-80
97. Xu Zong-Xiang;Lin Jing-Dong;Ou Yan;Liao Dai-Wei.Preparation of Hollow Carbon Spheres by Catalytic Pyrolysis of C2H2[J]. Acta Phys. -Chim. Sin., 2003,19(11): 1035-1038
98. Li Chun-Lin;Fu Yi-Lu;Bian Guo-Zhu.Surface Basicity and Catalytic Performance on Ni/Ce-Zr-Al-O Catalyst for CO2+CH4 Reforming[J]. Acta Phys. -Chim. Sin., 2003,19(10): 902-906
99. Wang Shi-Zhong;Ishihara Tatsumi.Improvement of the Performance of Fuel Cells Anodes with Sm3+ Doped CeO2 Interlayer[J]. Acta Phys. -Chim. Sin., 2003,19(09): 849-853
100. Wang Shi-Zhong;Ishihara Tatsumi.Improvement of the Performance of Fuel Cells Anodes with Sm3+ Doped CeO2[J]. Acta Phys. -Chim. Sin., 2003,19(09): 844-848
101. Zeng Yue;Zheng Yang-Cun;Yi Jian-Long;Yu Shang-Ci;Yang Chun-Ming;Li Ze-Lin.Kinetics and Mechanism of Hypophosphite Electrooxidation on a Nickel Electrode[J]. Acta Phys. -Chim. Sin., 2003,19(08): 718-722
102. Gu Feng-Cai;Zhao Zhu-Xuan;Li Ying-Hui;Men Juan;Yan Ju-Ming;Liu Rui-Xian;Zhang Li-Hua.Preparation and Characterization of SurfaceModified SnO2 Nanocrystals[J]. Acta Phys. -Chim. Sin., 2003,19(07): 621-625
103. Zhao Yong-Xiang;Qin Xiao-Qin;Hou Xi-Cai;Xu Xian-Lun;Liu Dian-Sheng.Preparation,Characterization and Properties of Selective Hydrogenation on Ni-based Catalysts[J]. Acta Phys. -Chim. Sin., 2003,19(05): 450-454
104. Liu Yue;Liu Jia-Wen;Yang Xiao-Zhen.Cationic Reaction Mechanism for Ethylene Polymerization of New Nickel Catalysts[J]. Acta Phys. -Chim. Sin., 2002,18(12): 1068-1070
105. Ma Yan-Feng;Li Wei;Zhang Ming-Hui;Zhang Bao-Gui;Tao Ke-Yi.New Method of Preparing NiP and NiPB Amorphous Alloys Using Nickel Hypophosphite as Reactant[J]. Acta Phys. -Chim. Sin., 2002,18(10): 938-942
106. Zhou Xing-Fu;Han Ai-Jie;Chu Dao-Bao;Lin Chang-Jian;Tian Zhong-Qun.Preparation of Nanocrystalline NiO by Electrochemical Dissolution of Nickel[J]. Acta Phys. -Chim. Sin., 2002,18(07): 613-616
107. Qiu Li-Mei;Liu Fen;Zhao Liang-Zhong.Synthesis of K-Pb-Tl-O Complex Oxides and XPS Study on Their Electronic Structure[J]. Acta Phys. -Chim. Sin., 2002,18(07): 633-635
108. Zhu Jian-Xin;Li Jin-Hui;Nie Yong-Feng.Vacuum Thermal Recycling of Used Ni-Cd Batteries[J]. Acta Phys. -Chim. Sin., 2002,18(06): 536-539
109. Kong Jing-Lin;Xue Kuan-Hong;Shao Ying;He Chun-Jian;Chen Qiao-Ling.Measurements for the Kinetic Parameters of Electrocatalytic Oxidation of Ethanol at the Nickel Nanowire Electrode[J]. Acta Phys. -Chim. Sin., 2002,18(03): 268-271
110. Shi Shen-Lei;Lou Hui;Zhang Jian-Hua;Lü Ping;Jiang Ning;He Pi-Mo;Bao Shi-Ning.Investigation on the Interface between COT-H and Ru by UPS[J]. Acta Phys. -Chim. Sin., 2002,18(01): 30-33
111. Ng Seikweng;Hu Sheng-Zhi.Reformulation of two Ni(Ⅱ)-8-hydroxyquinoline complexes from Calculated Structure Factors[J]. Acta Phys. -Chim. Sin., 2001,17(11): 1040-1044
112. Dong Dong;Zhang Sheng;Zhu Tao;Gan Liang-Bing;Liu Zhong-Fan.FullereneTerminated SAMs on Gold(111):Formation and Characterization[J]. Acta Phys. -Chim. Sin., 2001,17(11): 978-981
113. Xu Yan-Qi;Cai Wei-Li;Wang Yin-Hai;Mou Ji-Mei.Fabrication and Characterization of Ordered Nanoporous Ni Membranes[J]. Acta Phys. -Chim. Sin., 2001,17(11): 991-994
114. Zhong Shun-He;Chen Song-Zhe;Xin Xiu-Lan.Laser Stimulated Surface Reaction of C2H4 on Nickel Sulfate[J]. Acta Phys. -Chim. Sin., 2001,17(10): 936-939
115. Zhao Liang-Zhong;Liu Fen;Li Jian-Zhang;Xu Yong-Tong.XPS Study of Three Dimensional C/SiC Composites[J]. Acta Phys. -Chim. Sin., 2001,17(09): 802-805
116. Yang Yong-Lai;Xu Heng-Yong;Li Wen-Zhao.Study on Carbon Deposition of CH4,C2H6 and C2H4 Cracking over Ni-based Catalysts[J]. Acta Phys. -Chim. Sin., 2001,17(09): 773-775
117. Zhou Guo-Ding;Kamkin A N;Liao Qiang-Qiang.Photoelectrochemical Study of Copper-Nickel and Copper-Cobalt Electrodes in Alkaline Solution[J]. Acta Phys. -Chim. Sin., 2001,17(07): 614-618
118. Zhang Jian-Hua;Wu Yue;Zhuang You-Yi;Zhang Han-Jie;Li Hai-Yang;He Pi-Mo;Bao Shi-Ning;Liu Feng-Qin;K.Yibulaxin;Qian Hai-Jie.Orbital Symmetry of the Acetylene on Ru(1010) Surface[J]. Acta Phys. -Chim. Sin., 2001,17(07): 600-603
119. Yang Zhi-Hong;Luo He-Kuan;Mao Bing-Quan;Tang Rui-Guo;Yu Ding-Sheng;Wang Gui-Hua.In Situ UVVis Studies on Nickel Catalyst for Ethylene Polymerization[J]. Acta Phys. -Chim. Sin., 2001,17(05): 460-464
120. Zhao Liang-Zhong;Liu Fen;Zhang Lin.XPS Study on Electronic Structure for LnCu2O4(Ln=Gd, Nd)[J]. Acta Phys. -Chim. Sin., 2001,17(04): 310-313
121. Wang Yu;Liu Guan-Kun;He Feng-Rong;Tong Ye-Xiang.Electrodeposition of Ho-Ni Alloy from Dimethyformamide Bath[J]. Acta Phys. -Chim. Sin., 2001,17(03): 206-209
122. Zhang Yu-Zhi;Kuai Su-Lan;Huang Yin-Song;Wang Zhong-Chun;Hu Xing-Fang.X-ray Photoelectron Spectroscopic Study on Electrochromic Molybdenum Oxide Films[J]. Acta Phys. -Chim. Sin., 2001,17(01): 79-82
123. Liu Tian-Qing, Zou Ai-Hua, Guo Rong.Effect of Surfactant and Cosurfactant on the Protecting Corrosion for Nickel[J]. Acta Phys. -Chim. Sin., 2000,16(10): 899-905
124. Han Chun-Ying, Xing Xiao-Peng, Zhang Xia, Gao Zhen, Zhu Qi-He.Formation and Photodissociation of Fe、Co、Ni/P Binary Cluster lons[J]. Acta Phys. -Chim. Sin., 2000,16(09): 818-824
125. Cao Xiao-Yan, Wu Wei, Wang Dong, Ge Mao-Fa, Wang Dian-Xun.Hel Photoelectron Spectroscopic Study on the Electronic Structure of the Derivatives of 1,2,5-thiadiazole[J]. Acta Phys. -Chim. Sin., 2000,16(06): 491-495
126. Bian Guo-Zhu, Yin Ya-Dong, Fu Yi-Lu, Wu Zhong-Hua, Hu Tian-Dou, Liu Tao.Preparation and Crystallization of Nanosized Amorphous Nickel Sulfide by Using γ -irradiation[J]. Acta Phys. -Chim. Sin., 2000,16(01): 55-59
127. Zhao Liang-Zhong, Wang Rui-Lan, Xu Hong-Yu, Li Hong-Cheng, Liu Shi-Hong.XPS Studies of Superconducting Gd-Ba-Cu-O Films[J]. Acta Phys. -Chim. Sin., 1999,15(05): 398-402
128. Jin Rong-Chao, Chen Yan-Xin, Cui Wei, Li Wen-Zhao, Yu Chun-Ying, Jiang Yi.Mechanism of Catalytic Partial Oxidation of Methane to Synthesis Gas on Nickel Catalyst[J]. Acta Phys. -Chim. Sin., 1999,15(04): 313-318
129. Zhang Zhao-Liang, Sun Dong-Sheng, Yang Xi-Yao.Properties of AB5-type Hydrogen Storage Alloy Electrodes[J]. Acta Phys. -Chim. Sin., 1998,14(10): 954-956
130. Yuan An-Bao, Cheng Shao-An, Zhang Jian-Qing, Cao Chu-Nan.Electrochemical lmpedance Spectroscopy of Porous Nickel Electrode and its Mathematical Model[J]. Acta Phys. -Chim. Sin., 1998,14(09): 804-810
131. Zhong Chong-Min, Wang-De-Zheng, Takashi Ushikubo, Keisuke Wada.The Adsorption of Methanol,Water and Ethylene on a Niobium Oxide Thin Film[J]. Acta Phys. -Chim. Sin., 1998,14(03): 219-225
132. Sun Zheng, Zheng Shi-Jun, Meng Ling-Peng, Qiao Chun-Hua, Wang Dian-Xun.Hel Photoelectron Spectroscopical and Theoretical Studies of the Electronic Structure and Molecular Obital Character in some Alkyl Thioether Compounds[J]. Acta Phys. -Chim. Sin., 1998,14(01): 78-83
133. Han Ji-Hong,Xu Wei,Gu Chang-Xin,Hua Zhong-Yi,Niu Guo-Xing,Zhu Chong-Ye,Chen Hai-.EXAFS Studies on the Local Structure of Ni and Mo in Nickel-molybdenum Catalyst System[J]. Acta Phys. -Chim. Sin., 1997,13(12): 1108-1114
134. Liu Zhi-Xian,Shi Shuang-Qun,Zhang Jian-Jun,Song Xin-Fang,Meng Min-Quan.Coordinating Properties of Nickel(II) tetra(4-N-benzylpyridyl) porphyrin in Aqueous Solution[J]. Acta Phys. -Chim. Sin., 1997,13(07): 659-662
135. Zhou Yu-Ming,Ge Yu-Hua,Gou Shao-Hua,Ju Huang-Xian,Liu Ju-Zheng.The Thermal Stability and Electrochemical Behaviors of A Novel Macrocyclic Dinuclear Nickel(III) Complex[J]. Acta Phys. -Chim. Sin., 1997,13(07): 598-602
136. Li Sheng,Li Ying,Wang Xiao-Hui,Ding Chuan-Fan,Chen Wen-Wu,Gao Yi-Qin,Wang Dian-X.Hel Photoelectron Spectroscopic study of the Electronic Structure on B(OCH3)3[J]. Acta Phys. -Chim. Sin., 1996,12(07): 641-643
137. Shen Yong,Zhang Zong-Tao,Zhao Bin,Zhu Yu-Zhen,Hu Li-Ming.Preparation of Spherical Ultrafine Nickel Powder by Chemical Reduction in Aqueous Solution[J]. Acta Phys. -Chim. Sin., 1996,12(05): 460-463
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139. Lu Er-Dong, Ji Ming-Rong, Ma Mao-Sheng, Liu Xian-Ming, Xu Peng-Shou.XPS Investigation of Anodic Passive Films on Fe60Ni40 Polycrystalline Alloy[J]. Acta Phys. -Chim. Sin., 1995,11(11): 1031-1035
140. Liu Yuan,Zhong Bing,Peng Shao-Yi,Wu Dong,Fan Wen-Hao.The Preparation and Characterization of Ultrafine ZrO2[J]. Acta Phys. -Chim. Sin., 1995,11(09): 781-784
141. Chen Rui-Zhi, Zheng Shi-Jun, Cai Xin-Hua, Meng Ling-Peng, Wang Dian-Xun.Gas -phase Studies of Cyano Derivatives of Benzene Series by HeI Ultraviolet Photoelectron Spectroscopy[J]. Acta Phys. -Chim. Sin., 1995,11(05): 433-437
142. Xie Lei, Wang De-Zheng, Wei Xu-Ming, Cao Yu-Ming, Guo Xie-Xian, Ushikubo T, Wada K.The Preparation of A |Model Nb Oxide Catalyst Epitaxially Grown[J]. Acta Phys. -Chim. Sin., 1995,11(03): 234-241
143. Zhang Bing, Zhang Fei-Hua, Fang Li, Zhang Fu-Yi, Lin Miao.Studies on the Reactions of Nickel Ion with n-Alkanes in the Gas Phase Using Time of Flight Mass Spectrometer[J]. Acta Phys. -Chim. Sin., 1994,10(12): 1059-1061
144. Wang Ze-Xin, Zhang Ji-Shu, Yu Xiao-An, Hao Ce, Chen Zong-Qi.Effect of the Ni(510) Step Surface for the Dissociative Adsorption of Hydrogen Molecule[J]. Acta Phys. -Chim. Sin., 1994,10(10): 915-920
145. Wang Dian-Xun, Li Ying, Li Sheng, Chen Ben-Ming.He I Photoelectron Spectroscopy(UPS) of Isotopic 18O2 Molecules[J]. Acta Phys. -Chim. Sin., 1994,10(09): 771-773
146. Xu Bin, Zhu Chong-Ye, Li Quan-Zhi.Surface Species of Molybdenum-Nickel Loaded Catalysts and Their Catalytic Activity[J]. Acta Phys. -Chim. Sin., 1994,10(06): 543-548
147. Zhao Liang-Zhong.Evalustion of the Reactivity between Bi-Sr-Ca-Cu-O Superconductor and Oxide Substrate Materials[J]. Acta Phys. -Chim. Sin., 1994,10(05): 409-412
148. Yang Li-Ting, Chang Qing, Wang Feng-Li, Wang An-Zhou.Kinetics and Mechanism of Oxidation of α-alanine by Dihydroxydiperiodatonickelate (IV) Complex Ion[J]. Acta Phys. -Chim. Sin., 1994,10(04): 297-302
149. Wang Dian-Xun, Zheng Shi-Jun, Meng Ling-Peng, Cai Xin-Hua, Dai Cui-Chen, Xu Guang-Zhi, J. B. Peel.HeI Ultraciolet Photoelectron Spectroscopic Studies of Thienyl Polyethylenic Dimethyl Malonates Comopunds[J]. Acta Phys. -Chim. Sin., 1994,10(02): 179-182
150. Cai Xiao-Hai, Liu Ying-Jun, Liu Zhi-Wei, Xie You-Chang.An EXAFS Study on Support Effect of NiO Dispersion State[J]. Acta Phys. -Chim. Sin., 1994,10(01): 15-18
151. Shao Shu-Min; Xi Guang-Kang; Wang Jun-Rong; Li Sheng-Lin; Yang Xue-Zhu; Wang Jin-He; Zhou Zhi-Qiang; He Tian-Xi; Yu Bao-Xia.Activated Chemisorption of CH4 On Ni Surface and La Film[J]. Acta Phys. -Chim. Sin., 1992,8(06): 767-771
152. Xie En-Hai; Meng Qing-Shui; Wang Zhi-Pu.Kinetics of Oxidation of Sodium Tartrate by Ni(IV) Periodate Complex in Aqueous Alkaline Medium[J]. Acta Phys. -Chim. Sin., 1992,8(04): 500-504
153. Zhou Guo-Ding; Zhang Guo-Qing; Tong Ru-Ting; Jin Shi-Xun; Cai Sheng-Min.Study of Passivation and Pitting Corrosion for Ni Electrode in Borax-Borate Solution[J]. Acta Phys. -Chim. Sin., 1992,8(03): 418-423
154. Zhang Yu-Gen; Li Jian-Min.The Electronic Absorption Spectra of Divalent Copper and Nickel Edta Complex Crystals[J]. Acta Phys. -Chim. Sin., 1992,8(02): 251-254
155. Xiao Shu-Yong; Yao Jie; Meng Zhong-Yue.Probe Into NH3-TPD Curve of Ni-Containing Zeolite Out The View of Acidity[J]. Acta Phys. -Chim. Sin., 1991,7(06): 721-724
156. Lin Hua-Kuan; Zhou Zhi-Fen; Gu Zong-Xin; Chen Rong-Ti.Thermodynamic and Calorimetric Study on the Formation of Binary Complex Compounds of Nickel(II) with some α-Amino Acids and Oxalate[J]. Acta Phys. -Chim. Sin., 1991,7(01): 82-86
157. ZHANG Xiao-Ning, Hollimon Valerie, Brodus DaShan.Method for Attaching Thiol Groups Directly on a Silicon (111) Substrate[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
158. NIE Wang-Xin, ZOU Xiu-Jing, WANG Xue-Guang, DING Wei-Zhong, LU Xiong-Gang.Preparation of Highly-Dispersed Ni-Ce-Zr Oxides over Mesoporous γ-Alumina and Their Catalytic Properties for CO2 Methanation[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
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