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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2016,Vol.32>> Issue(2)>> 474-480     doi: 10.3866/PKU.WHXB201511104         中文摘要
Preparation and Application of Polyaniline Doped with Different Sulfonic Acids for Supercapacitor
LIN You-Cheng, ZHONG Xin-Xian, HUANG Han-Xing, WANG Hong-Qiang, FENG Qi-Peng, LI Qing-Yu
Key Laboratory for the Chemistry and Molecular Engineering of Medicinal Resources, Ministry of Education, Guangxi Key Laboratory of Low Carbon Energy Materials, School of Chemistry and Pharmaceutial Sciences, Guangxi Normal University, Guilin 541004, Guangxi Zhuang Autonomous Region, P. R. China
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Polyaniline (PANI) nanomaterials doped with three different sulfonic acid surfactants (perfluorinated sulfonic acid ion exchange resin (Nafion), sodium dodecyl sulfate (SDS), and sodium dodecyl benzene sulfonate (SDBS)) were prepared using an emulsion polymerization method with manganese dioxide (MnO2) as the oxidant. The structure and morphology of the products were studied by scanning electron microscopy (SEM), Fourier transform infrared (FTIR) spectroscopy, and X-ray diffraction (XRD). Symmetric redox supercapacitor was assembled with doped PANI as the active electrode material. The electrochemical performances of the materials were evaluated by cyclic voltammetry (CV), electrochemical impedance spectroscopy (EIS), and galvanostatic charge-discharge tests. These results suggest that the introduction of surfactant is beneficial for the formation of a fiber structure and increases the dispersion of PANI. A PANI-Nafion network with distributed porosity and average diameters of 30-40 nm is obtained. The specific capacitances of PANI-Nafion, PANI-SDS, and PANI-SDBS electrodes at 0.1 A·g-1 are 385.3, 359.7, and 401.6 F·g-1, respectively. Among these electrodes PANI-Nafion delivers the best cycle performance, maintaining 70.7% of its initial capacitance after 1000 cycles.



Keywords: Polyaniline   Organic sulfonic acid   Emulsion polymerization   Nanofiber   Supercapacitor  
Received: 2015-07-20 Accepted: 2015-11-06 Publication Date (Web): 2015-11-10
Corresponding Authors: ZHONG Xin-Xian, LI Qing-Yu Email: zhongxx2004@163.com;liqingyu62@126.com

Fund: The project was supported by the China Postdoctoral Science Foundation (2014M562499XB) and National Natural Science Foundation of China (U1401246, 51474110).

Cite this article: LIN You-Cheng, ZHONG Xin-Xian, HUANG Han-Xing, WANG Hong-Qiang, FENG Qi-Peng, LI Qing-Yu. Preparation and Application of Polyaniline Doped with Different Sulfonic Acids for Supercapacitor[J]. Acta Phys. -Chim. Sin., 2016,32 (2): 474-480.    doi: 10.3866/PKU.WHXB201511104

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56. ZHANG Fang, YUAN Chang-Zhou, ZHANG Xiao-Gang, ZHANG Luo-Jiang, XU Ke.5-Sulfosalicylic Acid-Assisted Hydrothermal Synthesis and Supercapacitive Properties of Co-Ni Layered Double Hydroxides[J]. Acta Phys. -Chim. Sin., 2010,26(12): 3175-3180
57. ZHANG Xiao-Bo, CHEN Ming-Hai, ZHANG Xiao-Gang, LI Qing-Wen.Preparation of Porous Carbon Nanofibers by Electrospinning and Their Electrochemical Capacitive Behavior[J]. Acta Phys. -Chim. Sin., 2010,26(12): 3169-3174
58. WANG Jin-Xing, YU Lian-Xiang, WANG Hao-Ming, RUAN Sheng-Ping, LI Jia-Jing, WU Feng-Qing.Preparation and Triethylamine Sensing Properties of Ce-Doped In2O3 Nanofibers[J]. Acta Phys. -Chim. Sin., 2010,26(11): 3101-3105
59. TIAN Ying, YAN Jing-Wang, LIU Xiao-Xue, XUE Rong, YI Bao-Lian.Electrochemical Capacitance of Composites with MnOx Loaded on the Surface of Activated Carbon Electrodes[J]. Acta Phys. -Chim. Sin., 2010,26(08): 2151-2157
60. LI Li-Min, LIU En-Hui, LI Jian, YANG Yan-Jing, SHEN Hai-Jie, HUANG Zheng-Zheng, XIANG Xiao-Xia.Polyaniline-Based Carbon for a Supercapacitor Electrode[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1521-1526
61. JI Qian-Qian, GUO Pei-Zhi, ZHAO Xiu-Song.Preparation of Chitosan-Based Porous Carbons and Their Application as Electrode Materials for Supercapacitors[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1254-1258
62. ZANG Yang, HAO Xiao-Gang, WANG Zhong-De, ZHANG Zhong-Lin, LIU Shi-Bin.Copolymerization and Capacitive Performance of Composite Carbon Nanotubes/Polyaniline/Nickel Hexacyanoferrate Films[J]. Acta Phys. -Chim. Sin., 2010,26(02): 291-298
63. PANG Xu, MA Zheng-Qing, ZUO Lie.Sn Doped MnO2 Electrode Material for Supercapacitors[J]. Acta Phys. -Chim. Sin., 2009,25(12): 2433-2437
64. FU Qing-Bin, GAO Bo, SU Ling-Hao, YUAN Chang-Zhou, LU Xiang-Jun, ZHANG Xiao-Gang.Preparation of Polypyrrole/Benzenesulfonic Functionalized Multi-Walled Carbon Nanotubes Induced by Hydrogen Bonding and Their Electrochemical Behavior[J]. Acta Phys. -Chim. Sin., 2009,25(11): 2199-2204
65. SUN Zhe, LIU Kai-Yu, ZHANG Hai-Feng, LI Ao-Sheng, XU Xiao-Cun.Study on Meso-C/MnO2 Asymmetric Supercapacitors[J]. Acta Phys. -Chim. Sin., 2009,25(10): 1991-1997
66. JIANG Qi, ZHAO Xiao-Feng, HUANG Bin, DU Bing, ZHAO Yong.Effect of the Activated Carbon Reactivation on Its Electrochemical Capacitance[J]. Acta Phys. -Chim. Sin., 2009,25(04): 757-761
67. DU Bing, JIANG Qi, ZHAO Xiao-Feng, LIN Sun-Zhong, MU Pei-Shan, ZHAO Yong.Preparation of PPy/CNTs Composite Based on the Electrostatic Absorption Effect[J]. Acta Phys. -Chim. Sin., 2009,25(03): 513-518
68. CHEN Li; ZHANG Xiao-Gang; YUAN Chang-Zhou; CHEN Sheng-Yao.Electrochemical Properties of Poly(3,4-ethylenedioxythiophene)/Manganese Oxide Synthesized by Interfacial Polymerization[J]. Acta Phys. -Chim. Sin., 2009,25(02): 304-308
69. CHANG Guo-Qing, ZHENG Xi, CHEN Ri-Yao, CHEN Xiao, CHEN Li-Qin, CHEN Zhen.Silver Nanoparticles Filling in TiO2 Hollow Nanofibers by Coaxial Electrospinning[J]. Acta Phys. -Chim. Sin., 2008,24(10): 1790-1796
70. SU Bi-Tao; ZUO Xian-Wei; HU Chang-Lin; LEI Zi-Qiang.Synthesis and Electromagnetic Properties of Polyaniline/CoFe2O4 Nanocomposite[J]. Acta Phys. -Chim. Sin., 2008,24(10): 1932-1936
71. JIANG Qi; ZHANG Qian; DU Bing; ZHAO Xiao-Feng; ZHAO Yong.Preparation and Electrochemical Properties of CNTs-PANI Composite Material via Finite Field Polymerization[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1719-1723
72. ZENG Wen-Wen; HUANG Ke-Long; YANG You-Ping; LIU Su-Qin; LIU Ren-Sheng.Solvothermal Synthesis and Capacitance Performance of Co3O4 with Different Morphologies[J]. Acta Phys. -Chim. Sin., 2008,24(02): 263-268
73. YANG Jing; LIU Ya-Fei; CHEN Xiao-Mei; HU Zhong-Hua; ZHAO Guo-Hua.Carbon Electrode Material with High Densities of Energy and Power[J]. Acta Phys. -Chim. Sin., 2008,24(01): 13-19
74. WANG Hai-Yan; LIU Xin-Hou; WU Da-Yong.Electrospinning and Electrospun Membranes[J]. Acta Phys. -Chim. Sin., 2007,23(Supp): 67-74
75. YANG Jian-Jun; HUANG Jun-Jie; JIANG Zhi-Yu.Supercapacitance of MnO2 Thin Film Electrodes Prepared Using Jet Printing Method[J]. Acta Phys. -Chim. Sin., 2007,23(09): 1365-1369
76. WANG Jie; XU You-Long; SUN Xiao-Fei; XIAO Fang; MAO Sheng-Chun.Capacitance Properties of Porous Polypyrrole Thick Films Prepared Electrochemically by Multi-step Polymerization[J]. Acta Phys. -Chim. Sin., 2007,23(06): 877-882
77. LU Xin-Mei; WU Quan-Fu; MI Hong-Yu; ZHANG Xiao-Gang.Electrochemical Capacitance of Camphorsulfonic Acid Doped Polyaniline Microtubes Prepared at Low Temperature[J]. Acta Phys. -Chim. Sin., 2007,23(06): 820-824
78. GUO Xiao-Li; GUO Min; WANG Xin-Dong.Bienzymatic Glucose Biosensor Based on Graphite Electrode Modified with Nanofibrous Polyaniline[J]. Acta Phys. -Chim. Sin., 2007,23(04): 585-589
79. FENG Zhen-Zhen;NULI Yan-Na;YANG Jun.Conductive Sulfur-Containing Material/Polyaniline Composite for Cathode Material of Rechargeable Magnesium Batteries[J]. Acta Phys. -Chim. Sin., 2007,23(03): 327-331
80. WANG Jie;XU You-Long;CHEN Xi;DU Xian-Feng;LI Xi-Fei.Effect of Doping Ions on Electrochemical Capacitance Properties of Polypyrrole Films[J]. Acta Phys. -Chim. Sin., 2007,23(03): 299-304
81. YANG Zhao-Hui;ZHANG Mao-Feng;CAO Wei-Xiao.Self-assembly Films of Poly(4-diazosulfonate Styrene-co-4-vinylpyridine) with Polyaniline and Their Photoelectric Conversion Properties[J]. Acta Phys. -Chim. Sin., 2007,23(01): 1-5
82. WEN Jing-bang; ZHOU Hai-hui; LI Song-lin; LUO Sheng-lian; CHEN Jin-hua; KUANG Ya-fei.Growth Process of Nano-fibrous Polyaniline Film on Stainless Steel[J]. Acta Phys. -Chim. Sin., 2006,22(01): 106-109
83. TANG Tian-di; CHEN Jiu-ling; LI Yong-dan.Treatment of the Carbon Nanofiber Surfaces in Mixed Concentrated HNO3-H2SO4 and the Catalytic Activity of Supported Pd-Pt for Naphthalene Hydrogenation[J]. Acta Phys. -Chim. Sin., 2005,21(07): 730-734
84. MA Hui-ru; GUAN Jian-guo; LU Guo-jun; YUAN Run-zhang.The Preparation and Characterization of PAn-PEG-PAn Rod-coil Triblock Copolymers[J]. Acta Phys. -Chim. Sin., 2005,21(06): 627-631
85. CAI Cheng-Dong; ZHOU Jian-Zhang; QI Li; XI Yan-Yan; LAN Bi-Bo; WU Ling-Ling; LIN Zhong-Hua.Conductance of a Single Conducting Polyaniline Nanowire[J]. Acta Phys. -Chim. Sin., 2005,21(04): 343-346
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87. WANG Xiao-Feng; RUAN Dian-Bo; WANG Da-Zhi; LIANG Ji.Hybrid Electrochemical Supercapacitors Based on Polyaniline and Activated Carbon Electrodes[J]. Acta Phys. -Chim. Sin., 2005,21(03): 261-266
88. Chen Wei-Ping;Feng Xin;Wang Chang-Song;Sun Sheng-Hua;Lu Xiao-Hua.The Interface Properties of Potassium Titanate Whiskers[J]. Acta Phys. -Chim. Sin., 2004,20(08): 868-870
89. Chen Hong;Chen Jin-Song;Zhou Hai-Hui;Jiao Shu-Qiang;Chen Jin-Hua;Kuang Ya-Fei.The Application of Nano-fibrous Polyaniline in Electrochemical Capacitor[J]. Acta Phys. -Chim. Sin., 2004,20(06): 593-597
90. Dong Ping;Zhou Jian-Zhang;Xi Yan-Yan;Cai Cheng-Dong;Zhang Yan;Zou Xu-Dong;Huang Huai-Guo;Wu Ling-Ling;Lin Zhong-Hua.The Growth Mechanism of Eletrosynthesized Polyaniline Nanotubules in Alumina Template[J]. Acta Phys. -Chim. Sin., 2004,20(05): 454-458
91. Jiang Qi;Lu Xiao-Ying;Zhao Yong;Yu Zuo-Long.Effect of Microstructure’s Change on Electrochemical Capacitance of Carbon Nanotubes[J]. Acta Phys. -Chim. Sin., 2004,20(05): 546-549
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94. Zhou Hai-Hui;Jiao Shu-Qiang;Chen Jin-Hua;Wei Wan-Zhi;Kuang Ya-Fei.Electrocatalytic Oxidation of Methanol on Nano-fibular Polyaniline Electrode Modified with Pt Microparticles[J]. Acta Phys. -Chim. Sin., 2004,20(01): 9-14
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106. Zhang Bao-Hong;Zhang Na.Research on Nanophase MnO2 for Electrochemical Supercapacitor[J]. Acta Phys. -Chim. Sin., 2003,19(03): 286-288
107. Chen Di-Zhao;Liang Yi-Zeng;Xu Cheng-Jian.Rank Analysis on Two-dimensional Kinetic Data and Its Related Application[J]. Acta Phys. -Chim. Sin., 2002,18(10): 924-929
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111. Ding Wen;Fan Zhi-Kang;Xu Chuan-Xiang;Lu Feng-Ji.Metal Core/Polymer Coating Compounded Suspension for Electrorheologic Fluid[J]. Acta Phys. -Chim. Sin., 2001,17(06): 496-500
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114. Mu Shao-Lin, Yang Yi-Fei.Polyaniline Used as An Electron Transfer Mediator for the Catalyzed Dehydrogenating Renction of Alcohol[J]. Acta Phys. -Chim. Sin., 2000,16(09): 830-834
115. Huo Li-Hua, Wang Dong-Mei, Zeng Guang-Fu, Xi Shi-Quan.Preparation and Properties of Conducting Polymer of Doped Polyaniline LB Film[J]. Acta Phys. -Chim. Sin., 2000,16(07): 632-635
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