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Acta Physico-Chimica Sinca  2016, Vol. 32 Issue (10): 2475-2487    DOI: 10.3866/PKU.WHXB201607121
ARTICLE     
Two-Dimensional Layered Zeolite Precursors: Syntheses, Modifications and Catalytic Applications
Zhen-Chao ZHAO,Wei-Ping ZHANG*()
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Abstract  

Two-dimensional layered zeolite precursors (LZPs) with layered structural units of parent threedimensional zeolites possess the properties of the parent materials but with an open framework structure. The structural properties of these materials therefore provide new opportunities to synthesize new zeolites and fabricate sub-zeolites with distinct structures, making them a hot topic in zeolite research. Enormous LZPs were synthesized by the direct crystallization or post-modification of their three-dimensional parent structures. Several layer manipulation strategies, including swelling, delamination, pillaring and layer reassembly have been developed on two-dimensional LZPs. These strategies have provided access to zeolites with new structures as well as materials even violating the theoretical rules, which have greatly enhanced the field of two-dimensional LZPs, and expanded their applications in catalysis and separation. Herein, we have reviewed the structural characteristics of two-dimensional LZPs, as well as summarizing their syntheses, modifications, and catalytic applications. We have also proposed the future perspectives of two-dimensional LZPs.



Key wordsTwo-dimensional layer      Lamellar zeolite      Topotactic conversion      Structure modification      Catalytic application     
Received: 25 May 2016      Published: 12 July 2016
MSC2000:  O643  
Fund:  The project was supported by the National Natural Science Foundation of China(21173029,21373035);and Fundamental Research Funds for the Central Universities in China(DUT16RC(3)002)
Corresponding Authors: Wei-Ping ZHANG     E-mail: wpzhang@dlut.edu.cn
Cite this article:

Zhen-Chao ZHAO,Wei-Ping ZHANG. Two-Dimensional Layered Zeolite Precursors: Syntheses, Modifications and Catalytic Applications. Acta Physico-Chimica Sinca, 2016, 32(10): 2475-2487.

URL:

http://www.whxb.pku.edu.cn/10.3866/PKU.WHXB201607121     OR     http://www.whxb.pku.edu.cn/Y2016/V32/I10/2475

Fig 1 Illustration of the topotactic conversion process of typical LZPs14
Name of layer silicate Name of zeolite Framework type,order
EU-19 EU-20,-20b CAS,disordered25-26
MCM-65(as made) MCM-65(calcined) CDO,fairly ordered27
PLS-1 CDS-1 CDO,fairly ordered28
UZM-13,17,19 UZM-25 CDO,well ordered29
RUB-36,38,48 RUB-37 CDO,well ordered30
PLS-4 unnamed CDO,well ordered31
ERS-12(as made) ERS-12(calcined) incomplete condensation32
MCM-47(as made) MCM-47(calcined) highly disordered33
PREFER Ferrierite FER,well ordered19
PLS-3 CDS-3 FER,well ordered31
MCM-22-precursor MCM-22 MWW,well ordered7
ERB-1 ERB-1(calcined) MWW,well ordered34
ITQ-1(as-made) ITQ-1(calcined) MWW,well ordered35
NU-6(1) NU-6(2) NSI,well ordered24
RUB-39 RUB-41 RRO,well ordered23
R-RUB-18 RUB-24 RWR,fairly ordered40
HAc-RUB-15 silica-sodalite SOD,fairly ordered36
CIT-10 SSZ-50 RTH,well ordered37
[F,Tet-A]-AlPO-1 unnamed AFO,well ordered20
HPM-2 unnamed MTF,well ordered38
DPA-P-HLS unnamed AST,well ordered39
Table 1 Compilation of published zeolite syntheses via topotactic condensation of LZPs*
Fig 2 Transformation of UTL molecular sieve into layered Ge-COK-14 and further into COK-14 molecular sieve45
Fig 3 Illustration showing the swelling of MCM-22P,delamination,and SiO2 pillaring52,53
Fig 4 Process of post-synthesizing interlayer expanded MWW through dialkoxysilylation of MCM-22P77
Fig 5 Topotactic conversion of layered RUB-36 to FER- or CDO-type zeolites102 CTAOH: cetyltrimethylammonium hydroxide
Fig 6 ADOR method in a cycle scheme demonstrating the mechanism for the synthesis of two novel zeolites: IPC-2 (OKO) and IPC-4 (PCR)103
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