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ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2017,Vol.33>> Issue(2)>> 356-363     doi: 10.3866/PKU.WHXB201610191         中文摘要
Crystal Structure, Thermal Decomposition and Interaction with CT-DNA of Three 2-Hydroxy-1-naphthaldehyde Acyl Hydrazones
ZHAO Shun-Sheng, LI Lan-Lan, LIU Xiang-Rong, DING Zuo-Cheng, YANG Zai-Wen
College of Chemistry and Chemical Engineering, Xi′an University of Science and Technology, Xi′an 710054, P. R. China
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Three acyl hydrazones N'-((2-hydroxynaphthalen-1-yl)methylene)-2-phenylacetohydrazide (1), N'-((2-hydroxynaphthalen-1-yl) methylene)-2-(4-hydroxyphenyl)acetohydrazide hydrate (2), and N'-((2-hydroxynaphthalen-1-yl) methylene)-2-(2-methoxyphenyl) acetohydrazide hydrate (3) were synthesized and then characterized by elemental analysis and single-crystal X-ray diffraction. The crystallographic data indicated that both compounds 2 and 3 crystallized in the monoclinic crystal lattice, space group C2/c, while compound 1 crystallized in the orthorhombic space group Pbca. The thermal decomposition processes of the three hydrazones were studied by thermogravimetry. The thermal decomposition temperatures of compounds 1, 2, and 3 were 318.23, 319.04, and 323.01℃, respectively. Meanwhile, the apparent activation energies for thermal decomposition for compounds 1, 2, and 3 were 115.90, 145.18, and 129.38 kJ·mol-1, respectively, calculated according to the Kissinger and Ozawa equations. The interactions of compounds 1-3 with calf thymus (CT)-DNA were evaluated by microcalorimetry. The results indicated these interactions were homogenous endothermic processes with non-identical interaction time (1.00-50.0 min) and interaction enthalpies (0.47-15.50 kJ·mol-1). The interaction enthalpies of compounds 1 and 2 were higher than those of their precursors, while the interaction enthalpy of compound 3 was lower than that of its precursor.



Keywords: Acyl hydrazone   Crystal structure   Thermogravimetry   Microcalorimetry   DNA binding  
Received: 2016-09-05 Accepted: 2016-10-19 Publication Date (Web): 2016-10-19
Corresponding Authors: LIU Xiang-Rong Email: xkchemistry@163.com

Fund: The project was supported by the National Natural Science Foundation of China (21103135, 21073139, 21301139), Natural Science Basic Research Plan in Shaanxi Province, China (2016JM2011), and Scientific Research Program Funded by Shaanxi Provincial Education Commission, China (15JK1492).

Cite this article: ZHAO Shun-Sheng, LI Lan-Lan, LIU Xiang-Rong, DING Zuo-Cheng, YANG Zai-Wen. Crystal Structure, Thermal Decomposition and Interaction with CT-DNA of Three 2-Hydroxy-1-naphthaldehyde Acyl Hydrazones[J]. Acta Phys. -Chim. Sin., 2017,33 (2): 356-363.    doi: 10.3866/PKU.WHXB201610191

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63. YANG Zi-Liang;YANG Si-Hai;LI Guo-Bao;LIN Jian-Hua.Synthesis, Structure and Thermal Properties of [HN(C2H5)3][B5O6(OH)4][J]. Acta Phys. -Chim. Sin., 2007,23(03): 285-288
64. QU Xiu-Kui;SUN De-Zhi;ZHENG Wen-Qing;LIU Min;WEI Xi-Lian.Host-Guest Complexation of Cyclodextrin with a Series of New Kind of Surfactants[J]. Acta Phys. -Chim. Sin., 2007,23(01): 116-119
65. GUO Jin-Yu;ZHANG Jian-Guo;ZHANG Tong-Lai;WU Rui-Feng;YU Wei.Thermal Decomposition Mechanisms of a Three-dimensional Framework Coordination Polymer [Cu(HCOO)2(H2O)2][J]. Acta Phys. -Chim. Sin., 2006,22(10): 1206-1211
66. YUAN Wei;LI He-Xian;WANG Ying;WANG Guo-Chang.Theoretical Prediction of Crystal Structure of N-(1-naphthyl) Succinimide Compound[J]. Acta Phys. -Chim. Sin., 2006,22(09): 1071-1074
67. HU Xin-Gen;YU Li;LIN Rui-Sen;FANG Ying-Ying;LI Wen-Bing .Study on Hydrophobic Self-association of Aliphatic α-amino Acids by Flow Microcalorimetry[J]. Acta Phys. -Chim. Sin., 2006,22(08): 1034-1039
68. CHEN Hu;XU Xing-You;GAO Jian;YANG Xu-Jie;LU Lu-De;WANG Xin.Study on Crystal Structure of [Ni(phen)3](ClO4)2[J]. Acta Phys. -Chim. Sin., 2006,22(07): 856-859
69. CHEN Feng-Ying; CAO Wen-Kai; HE Shui-Yang; WANG Bao-Huai; ZHANG You-Min.Synthesis, Characterization and Thermochemistry Properties of RE(III) and 2-oxo-propionic Acid Salicyloyl Hydrazone Complexes[J]. Acta Phys. -Chim. Sin., 2006,22(03): 280-285
70. YANG Jian;QIU Tai;SHEN Chun-Ying.Synthesis and Characterization of a Novel Precursor for BCN Compound[J]. Acta Phys. -Chim. Sin., 2005,21(12): 1373-1377
71. QIU Xiao-Mei; LI Ling; WEI Xi-Lian; YIN Bao-Lin; SUN De-Zhi.A Study on Complexation between α-cyclodextrin and Bis-quaternary Ammonium Surfactants[J]. Acta Phys. -Chim. Sin., 2005,21(12): 1415-1418
72. SHAN Hai-wei CHEN Dong-hua TANG Wan-jun.Thermodynamics and Thermal Analysis Kinetics of MC2O4 (M=Mn, Fe, Co, Ni, Cu, Zn)[J]. Acta Phys. -Chim. Sin., 2005,21(09): 1001-1005
73. LI Lin-yan; LI Guo-bao; LIAO Fu-hui; LIN Jian-hua.Synthesis and Structure of La[B5O8(OH)(H2O)]NO3•2H2O[J]. Acta Phys. -Chim. Sin., 2005,21(07): 769-773
74. Wu Wang-Ting;Yang Rui;Hu Ting;Peng Ke;He Shui-Yang;Hu Rong-Zu.Thermochemistry of Salicylaldehyde-1H-benzotriazol Acetyl Hydrazone Complexes with RE (III)[J]. Acta Phys. -Chim. Sin., 2004,20(09): 1144-1149
75. Shi Xue-Song;Du Miao;Bu Xian-He.Development of the Coordination Chemistry of Diazamesocycles[J]. Acta Phys. -Chim. Sin., 2004,20(08S): 917-923
76. Wang Shi-Bing;Song Ming-Zhi;Wei Xi-Lian;Yin Bao-Lin;Sun De-Zhi.A Study on Interactions between α-cyclodextrin and a Series of New Kind of Surfactants in Aqueous Solutions by Microcalorimetry[J]. Acta Phys. -Chim. Sin., 2004,20(08): 837-842
77. Jiao Bao-Juan;Zhu Li;Yang Xu-Wu;Chen San-Ping;Gao Sheng-Li;Shi Qi-Zhen.Thermochemistry of the Ternary Complex Tb(Et2dtc)3(phen)[J]. Acta Phys. -Chim. Sin., 2004,20(07): 767-771
78. Xu Fen;Sun Li-Xian;Tan Zhi-Cheng;Liang Jian-Guo;Zhou Dan-Hong;Di You-Ying;Lan Xiao-Zheng;Zhang Tao.Studies on Thermal Decomposition Mechanism and Kinetics of Aspirin[J]. Acta Phys. -Chim. Sin., 2004,20(01): 50-54
79. Li Zeng-He;Yin Chen;Wang Ru-Ji;Wang Ping;Guo Hong-You.Synthesis and Crystal Structure of an Inorganic-Organic Hybrid CompoundCo(μ2-bpy)V2O6 (bpy=4,4’-bipyridine)[J]. Acta Phys. -Chim. Sin., 2003,19(12): 1133-1137
80. Wang Xin-Qing;Wang Miao;Li Zhen-Hua;Zhu Hai-Bin;Wang Feng-Fei.Purification and Characterization of Single-Walled Carbon Nanotubes Produced by Arc-Discharge[J]. Acta Phys. -Chim. Sin., 2003,19(05): 428-431
81. Liu Bei-Ping;Tan Zhi-Cheng;Yu Hua-Guang;Lan Xiao-Zheng;Zhang Da-Shun;Liu Ping;Sun Li-Xian.Thermodynamic Properties of [Ho2(Ala)4(H2O)8]Cl6 (Ala=alanine)[J]. Acta Phys. -Chim. Sin., 2003,19(05): 445-449
82. Hou An-Xin;Qu Song-Sheng;Wong Wai-Kwok;Liu Yi.Microcalorimetric Study of the Action of Two Kinds of Lanthanide Monoporphyrinate Complexes on Growth Metabolism of Escherichia Coli[J]. Acta Phys. -Chim. Sin., 2003,19(02): 134-138
83. Wang Wen-Zhi;Fan Neng-Ting.Synthesis and Crystal Structure of 4,4’-Oxobis(propham)[J]. Acta Phys. -Chim. Sin., 2003,19(01): 75-78
84. Zhang Hong-Lin;Yu Xiu-Fang;Zhang Gang.Thermokinetics of Activation of Metal Ions to Amylase Catalyzed Reaction[J]. Acta Phys. -Chim. Sin., 2002,18(12): 1125-1128
85. He Shui-Yang;Cao Wen-Kai;Hu Ting;Zhao Jian-She;Zhang Wei-Ping;Xue Gang-Lin;Hu Rong-Zu.Synthesis, Characterization and Thermochemical Properties of La(III) with Salicylaldehyde-1H- benzotriazol-1-aceylhydrazone[J]. Acta Phys. -Chim. Sin., 2002,18(10): 865-870
86. Ning Jia-Cheng;Yang Ao;Guan Ye-Di;Wang Zhe-Ming;Yan Chun-Hua.The Resolution of the Optical Active Derivatives of Ketorolac and the Determination of its Absolute Configuration[J]. Acta Phys. -Chim. Sin., 2002,18(09): 821-824
87. Zhang Hao;Suo Quan-Ling;Wang Yi-Bin;Wang Li;Weng Lin-Hong;Leng Xue-Bing.Synthesis and Crystal Structure of (μ3-S)FeCo2(CO)7(dppfe)[J]. Acta Phys. -Chim. Sin., 2002,18(08): 746-749
88. Liu Guang;Zhang ShiWei.Synthesis and Structure of a Novel 18Mo Polyoxomolybdate[J]. Acta Phys. -Chim. Sin., 2002,18(07): 624-628
89. Gao Zhen-Ting;Liu Yi;Huang Yu-Ping;Shen Ping;Qu Song-Sheng.Thermokinetic Study on the Growth Metabolism of Ura-auxotrophic Mutant of[J]. Acta Phys. -Chim. Sin., 2002,18(07): 590-594
90. Li Qi;Wen Xiao-Quan;Cai Xiao-Hai;Wang Xian-Rong;Xie You-Chang.Software BVStr for Analyzing the Structure of Crystal and Surface Based on the Bond Valence Theory[J]. Acta Phys. -Chim. Sin., 2002,18(06): 558-562
91. Song Xiang-Zhi;Liu Guang;Zhang Shi-Wei.Synthesis and Crystal Structures of Cancer Cell Inducers of Differentiation PMDH[J]. Acta Phys. -Chim. Sin., 2002,18(06): 545-549
92. Lu Xue-Fang;Zhang Hai-Rong;Li Yi;Liu Jing;Yang Guo-Qiang.Luminescence Properties and Crystal Structure of Two Metal 8-hydroxyquinoline Complexes at High Pressure[J]. Acta Phys. -Chim. Sin., 2001,17(10): 898-903
93. Zhang Hong-Lin;Yu Xiu-Fang.Microcalorimetric Study of the Oscillation System for the Extraction of Acetic Acid with Primary Amine with Primary Amine[J]. Acta Phys. -Chim. Sin., 2001,17(09): 855-858
94. Liu Xin-Mei;Yan Zi-Feng;Wang Huai-Ping.Optimization of Zeolite for Producing Lighter Olefin and Diesel in FCC Process[J]. Acta Phys. -Chim. Sin., 2001,17(06): 547-551
95. Zeng Xi-Rui;Zhang Yong;You Xiao-Zeng.Substituent Effect of the Peroxyoxalate Chemiluminescence[J]. Acta Phys. -Chim. Sin., 2001,17(04): 361-363
96. Shang Zhi-Cai;Yi Ping-Gui;Yu Qing-Sen;Lin Rui-Sen.Reaction Mechanism between Ciprofloxacin Hydrochloride and Bovine Serum Albumin[J]. Acta Phys. -Chim. Sin., 2001,17(01): 48-52
97. Li Xi, Liu Yi, Wu Jun, Zhao Ru-Ming, Qu Song-Sheng.Microcalorimetric Study of the Action of Selenium-containing Complexes on Growth Metabolism of Escherichia coli[J]. Acta Phys. -Chim. Sin., 2000,16(06): 568-572
98. Zhang Yao-Jun, Xin Qin.Studies on Differential Heats H2 Adsorption over γ-Mo2N Catalysts by Microcalorimetry[J]. Acta Phys. -Chim. Sin., 2000,16(05): 464-467
99. Zhao Bo, Zhang Dao, Cao Yang, Chen Wen-Jian, Sun Zhen-Rong, Wang Zu-Geng.Analysis of the Second-order Nonlinear Optical Properties of some Chalcones[J]. Acta Phys. -Chim. Sin., 2000,16(05): 422-425
100. Zhang Wen-Qin, Zhang Zhi-Ming, Zheng Yan, Wang Shu-Li, Zhao Shu-Na.Crystal Structure and Photochemical Properties of r-1,c-2,t-3,t-4-1,3-bis(4-biphenyl)-2,4-di(4-pyridyl)cyclobutane[J]. Acta Phys. -Chim. Sin., 2000,16(03): 207-213
101. Tang Hou-Kuang, He Ji, Liu Yi, Wang Cun-Xin, Xie Chang-Li, Qu song-Sheng.Growth Thermograms of Bacterial Variation Strains[J]. Acta Phys. -Chim. Sin., 1999,15(12): 1112-1114
102. Wu Man-Jiang, Ai Li, Chen Wen-Hai, Chen Wei, Xue Qun-Ji.The Association of Anionic Surfactants with β-cyclodextrin[J]. Acta Phys. -Chim. Sin., 1999,15(12): 1115-1118
103. Chen Zhen, Wang Ru-Ji.Synthesis of Transition Metal Chalcogenide [M(en)3]2Sn2Se6(M=Mn,Zn) and Studies of Thermogravimeric Properties[J]. Acta Phys. -Chim. Sin., 1999,15(12): 1070-1075
104. Miao Fang-Ming, Fan Zhi, Zhou Wei-Hong, Qi Li-Ning, Li Ai-Xiu, Liu Xiao-Lan.Synthesis and Crystal Structure and Quantum Chemistry of Tris(2-benzimidazylmethyl)amine with Manganese(II)[J]. Acta Phys. -Chim. Sin., 1999,15(09): 775-782
105. Wang Xiao-Ling, Suo Quan-Ling, Wang Yi-Bing, Sun Jie.Synthesisi and Crystal Structure of FeCo2(CO)73-S)(O[P(SCH2)2]2)[J]. Acta Phys. -Chim. Sin., 1999,15(08): 757-760
106. Zeng Hong-Xia, Li Zhi-Ping, Wang Han-Qing.Physical Chemistry Property of Water/TX-100/Hexanol/Octane Reverse Microemulsion[J]. Acta Phys. -Chim. Sin., 1999,15(06): 522-527
107. Ding Er-Run, Wu Shu-Lin, Li Qing-Shan, Yin Yuan-Qi.Synthesis,Structural Characterization and Reaction of the Chiral Clusters[J]. Acta Phys. -Chim. Sin., 1999,15(03): 241-246
108. Zhou Pei-Jiang, Hu Yun-Chu, Ling Xing-Yuan, Yang Feng, Song Zhao-Hua, Qu Song-Sheng, Zhu Ying-Guo.Microcalorimetric and Nonequlibrium Thermodynamic Studies on the Gemination and Growth of Seeds[J]. Acta Phys. -Chim. Sin., 1999,15(03): 274-278
109. Wei Kun, Shi Yan, He Lun-Yan.Crystal Structure and Infrared Spectra of Nanocrystalling Rare Earth Mixed Oxides Dy1-xSrxCoO3-y[J]. Acta Phys. -Chim. Sin., 1998,14(10): 957-960
110. Li Yue-Qing, Deng Li-Zhi, Zhou Xiao-Hai, Zhang Shao-Hui, Yang Qing-Chuan.The Crystal Structure and the Second Harmonic Generation Efficiency of the Sulfosalicylate[J]. Acta Phys. -Chim. Sin., 1998,14(09): 778-783
111. Zhou Pei-Jiang, Xie Chang-Li, Yang Feng, Qu Song-Sheng, Wu Jin-Ping, Li Cai-Wei.Microcalorimetric and Nonlinear Dynamic Study on the Finite Growth of Escherichia Coli[J]. Acta Phys. -Chim. Sin., 1998,14(02): 174-177
112. Liu Yong-Jun,Liu Ying,Sun Hai-Tao,Nan Zhao-Dong,Zhang Hong-Lin.Determination of the Optimum Acidity of Bacteria Growth by Microcalorimetric Method[J]. Acta Phys. -Chim. Sin., 1997,13(07): 637-639
113. Wang Tian-Zhi,Wu Ding-Quan,Huang Zai-Yin,Qu Song-Sheng,Li Dong-Feng,Liao Zhan-Ru.Studies on Model Compound of Purple Acid Phosphatases Hydrolysis of ATP[J]. Acta Phys. -Chim. Sin., 1997,13(07): 643-646
114. Xiong Ya,Pan Zheng-Jun,Wang Hong,Wu Ding-Quan,Kang Li-Shan,Qu Song-Sheng.Studies on the Thermokinetic Model of Mitochondrial Metabolism and its Evolutionary Optimization[J]. Acta Phys. -Chim. Sin., 1997,13(06): 503-509
115. Yan Cheng-Nong,Liu Yi,Qu Song-Sheng,Chen Chun-Ying,Xu Hui-Bi.Studies on Cell Kinetics Ⅷ. Characteristics of the Action of Na2SeO3 on Rhizopus Nigrocans[J]. Acta Phys. -Chim. Sin., 1997,13(04): 354-357
116. Chen Xue-An,Zhao Ling,Li Yan,Chen Ben-Ming.Preparation and Crystal Structure of PbCuP2O7[J]. Acta Phys. -Chim. Sin., 1997,13(02): 113-118
117. Tan An-Min,Xu Bo,Qu Song-Sheng.Microcalorimetric Study on Induced Differentiation of Tumour Cells by Drug[J]. Acta Phys. -Chim. Sin., 1996,12(09): 849-851
118. Zhuang Hong-Hui,Wu Ding-Ming,Huang Jian-Quan,Huang Jin-Ling.Synthesis and Crystal Structure of [Cu4Cl4(TTTA)2][J]. Acta Phys. -Chim. Sin., 1996,12(08): 761-765
119. Liu Yi,Wang Cun-Xin,Xie Chang-Li,Qu Song-Sheng,Hao Zong-Yu.Studies on Cell Kinetics IV.Thermokinetics of Bacterial Unideal Growth Process[J]. Acta Phys. -Chim. Sin., 1996,12(07): 659-663
120. Lu Qing-Wei,Wang Yi-Bing,Suo Quan-Ling,Wu Bao-Shan,Sun Jie.Synthesis and Crystal Strucutre of Fe3(CO)8(C6H5NC)(μ3-S)2[J]. Acta Phys. -Chim. Sin., 1996,12(06): 532-536
121. Xiong Ya,Huang Su-Qiu,Wu Ding-Quan,Qu Song-Sheng.Studies on the Interactions of Two Kinds of Water-Soluble Porphyrins with DNA[J]. Acta Phys. -Chim. Sin., 1996,12(06): 543-546
122. Liu Yi,Tan An-Min,Xie Chang-Li,Wang Cun-Xin,Qu Song-Sheng,Hao Zong-Yu.Cell Kinetic Study III.Thermokinetic Study of Bacterial Arithmetic Series Growth[J]. Acta Phys. -Chim. Sin., 1996,12(05): 451-455
123. Li Zhi-Ping,Yu Xiu-Fang,Hang Hu,Lu Mao-Sun,Zhang Hong-Lin.Study of the Promoter Action of Ginseng for S.aureus[J]. Acta Phys. -Chim. Sin., 1996,12(05): 468-471
124. Liu Yi, Tan An-Min, Xie Chang-Li, Wang Cun-Xin, Qu Song-Sheng, Hao Zong-Yu.Cell Kinetic Study II.Thermokinetic Study of the Process of Cell Growth Inhibited by Metabolites[J]. Acta Phys. -Chim. Sin., 1996,12(04): 377-381
125. Feng Ying, Liu Yi, Xie Chang-Li, Qu Song-Sehng, Yue Zhi-Feng, Feng Chang-Jian, Shen Hao-Yu, Zhang Xiang-Cai.Study on the Comparative Half Inhibitory Concentrations of Schiff Base Drugs Effect on Different Bacteria[J]. Acta Phys. -Chim. Sin., 1996,12(03): 229-234
126. Liu Yi,Xie Wei-Hong,Xie Chang-Li,Qu Song-Sheng.Thermokinetic Study of the Limited Growth of Bacteria[J]. Acta Phys. -Chim. Sin., 1996,12(02): 156-158
127. Liu Yi,Xie Chang-Li,Qu Song-Sheng,Deng Feng-Jiao,Guo Yu.Thermokinetic Study of Mitochondrial External Metabolism[J]. Acta Phys. -Chim. Sin., 1995,11(10): 929-931
128. Jin Xiang-Lin,Jiang Yi-Jia,Zhang Shi-Wei,Tang You-Qi.Synthesis and Crystal Structure of the Imidazale-bridged Dicopper(II) Complex with Tetraaza Macrocycles[J]. Acta Phys. -Chim. Sin., 1995,11(10): 932-936
129. Xiong Ya,Huang Su-Qiu,Wu Ding-Quan,Qu Song-Sheng.The Interaction of Water-soluble Quaternary Ammonium Pridine Pophyrins with DNA Studied by Microcalorimetry[J]. Acta Phys. -Chim. Sin., 1995,11(10): 957-960
130. Miao Fang-Ming, Liu Xiao-Lan, Chen Hong-Li, Cui Xue-Qi, Wang Hong-Gen, Wang Ru-Ji, Yao Xin-Kan.Synthesis and Structural Study of Bis(N-Phenylsalicylaldiminato)(1,10-Phenanthroline) Co(II)[J]. Acta Phys. -Chim. Sin., 1995,11(09): 824-827
131. Zhang Guo-Xiu,Yu xiu-Fang.Study on the Thermodynamical Functions of the Hydrolytic Polymerization of Chromium(III) Ion by Microcalorimetric Method[J]. Acta Phys. -Chim. Sin., 1995,11(08): 766-768
132. Guo Jin-Liang,Sun Feng,Li Yong,Dong Chang-Xiong.Crystal Structure of Dichloro-(5,10,15,20-tetraphenylporphinato) phosphorus(V) Chloride Dichloromethane Solvate[J]. Acta Phys. -Chim. Sin., 1995,11(04): 360-364
133. Hou Yong-Kang, Gao Min, Li Li-Pu, Ma Zhi-Mei.Studies of Trail and Error Method for Cyrstal Structural Determinations(III) Application and Program System of SYSTEM 90[J]. Acta Phys. -Chim. Sin., 1994,10(12): 1087-1092
134. Zheng Yu, Xie Wei-Wen, Zhang Lin-Na, Fu Gui-Xiang, Yu Lu, Zhu Zi-Ying.Thermal Decompositon Process and the Fragmentation Regularity of FAB-Mass Spectra of the Complex [Na3Fe(C2O4)3]·5H2O[J]. Acta Phys. -Chim. Sin., 1994,10(09): 774-778
135. Wu Bing-Fang, Su Hai-Quan, Yan Xiu-Ying, Hu Xiang, Liu Shu-Tang, Liu Qi-Wang, Shi Jian-Qiu.Synthesis and Crystal Structure of Rh2(μ-SC6H5)2(CO)4[J]. Acta Phys. -Chim. Sin., 1994,10(09): 847-851
136. Zhang Bin, Wang Zhe-Min, Liu Shi-Xiong, Huang Jin-Ling.Synthesis and Crystal Structure of a New Metal-rich Layered Ternary Tantalum Telluride TaNi2Te2[J]. Acta Phys. -Chim. Sin., 1994,10(06): 508-513
137. Wang Zhe-Min, Guan Tie-Tang, Zhuang Hong-Hui.Crystal Structure of Soft X-Ray Analyzer Crystal——Octadecyl Hydrogen Maleate(OHM, C22H40O4)[J]. Acta Phys. -Chim. Sin., 1994,10(05): 413-417
138. Zheng Ji-Min, Che Yun-Xia, Wang Ru-Ji, Wang Hong-Gen.Crystal Structure of 1:1 Adduct of Glycine and m-nitrobenzoic Acid[J]. Acta Phys. -Chim. Sin., 1994,10(01): 64-68
139. Ma Jian-Fang; Wei Ge-Cheng; Ni Jia-Zuan.Syntheses and Crystal Structures of the Complexes of rare Earth with Fumaric Acid[J]. Acta Phys. -Chim. Sin., 1993,9(06): 752-759
140. Yang Qing-Chuan; Dai Sheng; Zhou Hong-Bing; Zhou Qi-Feng; Tang You-Qi.The Molecular and Crystal Structures and Thermal Properties of the Mesogenic 2,5-BIS(4-Ethylbenzoyl) Oxystyrene and 2,5-BIS(4-Methoxybenzoyl) Oxybenzaldehyde[J]. Acta Phys. -Chim. Sin., 1993,9(06): 795-801
141. Cheng Qing-Tang; Li Jing-Hua; Lou Xiang-Dong.Investigation on Dehydration of Calcium Oxalate Monohydrate by Correlative Judging Method[J]. Acta Phys. -Chim. Sin., 1993,9(05): 675-678
142. Ye Dai-Qi; Liang Hong; Huang Zhong-Tao.Study on the Interaction Between the Active Phase and Support on V2O5/TiO2 Catalyst[J]. Acta Phys. -Chim. Sin., 1993,9(04): 501-508
143. Zhuang Hong-Hui; Wu Ding-Ming; Lu Can-Zhong; Tong Wen.Synthesis and Crystal Structure of (C5H7S2)2[Cu3I5][J]. Acta Phys. -Chim. Sin., 1993,9(04): 548-552
144. Wu Bing-Fang; Yan Xiu-Ying; Liu Qi-Wang; Liu Shu-Tang; Hu Xiang.Synthesis and Crystal Structure of Cluster (μ-SC6H5)(μ-P(SC6H5)2)Fe2(CO)6[J]. Acta Phys. -Chim. Sin., 1992,8(06): 749-752
145. Zeng Guang-Fu; Guo Xin; Wang Cui-Ying; Lin Yong-Hua; Li Han.Infrared Spectra and Crystal Structure of BIS-(Dimethoxylphosphato) Copper[J]. Acta Phys. -Chim. Sin., 1992,8(06): 778-782
146. Wang Zeng-Lin; Hu Ning-Hai; Niu Chun-Ji; Ni Jia-Zuan; Cui Ai-Li.Crystal Structure and Thermal Analysis of Erbium Complex with Benzene Acetic Acid[J]. Acta Phys. -Chim. Sin., 1992,8(05): 642-646
147. Du Shao-Bin; Wang Jin; Ma Fu-Tai; Zheng Hong-Yuan; Lou Hui; Jing Cheng-Heng.Correlation of Composition、Crystal Structure、Reducibility and Catalytic Oxidation Activity on La-Mn-Ni-O System[J]. Acta Phys. -Chim. Sin., 1992,8(05): 630-635
148. Fan Guang-Yu; Wang Huan-Zhong; Cui Xiu-Shan; Li Yun-Zheng; Zhu He-Sun.Crystal Structures of 1,2-Dimethyl-3-Indolmethyl-Idene Succinic Fulgide Anhydride and 1,2-Dimethyl-3-Indolylethylidene Succinic Fulgide Anhydride[J]. Acta Phys. -Chim. Sin., 1992,8(04): 545-549
149. Liu Yong-Sheng; Shu Ning-Cheng; Hu Ning-Hai.An Algebraic Method to Estimate General Type of Phases of Structure Factors[J]. Acta Phys. -Chim. Sin., 1992,8(02): 255-260
150. Li Jing-Hua; Zhang Gui-En.Investigation of the Kinetics and Mechanism of Decomposition of Ammonium Hydrogen Sulfate[J]. Acta Phys. -Chim. Sin., 1992,8(01): 123-127
151. Liu Xiao-Lan; Sun Ming; Miao Fang-Ming; Li Yu-Gui; Wang Jian-Ji; Han Yu-Zhen; Xu Xiao-Jie.Crystal and Molecular Structure of 1-Oxo-4-(Substituent)-1-Phospha-2,6,7-Trioxacyclo(2,2,2) Octane[J]. Acta Phys. -Chim. Sin., 1992,8(01): 100-108
152. Huang Ming-Sheng; Zhang Peng; Zhang Ying; Yang Hua-Hui; Zheng Lan-Sun.Synthesisi and Structure of a new Polynuclear Silver Complex [Ag4(dppe)3(NO3)4][J]. Acta Phys. -Chim. Sin., 1991,7(06): 694-698
153. Wu Ding-Quan; Mei Fu-Ming; Qu Song-Sheng; Du Yu-Min; Zhan Dong-Feng.Study on the Reaction of Laccase and Hydrogen Peroxide by Microcalorimetry[J]. Acta Phys. -Chim. Sin., 1991,7(04): 490-494
154. Jin Xiang-Lin; Tong You-Zhi; Xu Xiao-Jie; Tang You-Qi.The Synthesis and Crystal Structure of Thiocyanate-Bridged Bi-Copper(II) Macrocyclic Complex of 1,4,7,12,15,18-Hexaazacyclodocosane [Cu2(SCN)3(C16H38N6)]2(ClO4)2[J]. Acta Phys. -Chim. Sin., 1991,7(03): 323-328
155. Xin Min; Sun Xiao-Lin; Liu Qi-Wang; Hu Yu-Cai.The Crystal and Molecular Structure of β-Cyanoethyl-α-Ferrocenylhalogenbenzyl Ethers[J]. Acta Phys. -Chim. Sin., 1991,7(02): 136-139
156. Hu Sheng-Zhi; Chen Ming-Dan; Liu Xiao-Yun; Zhou Yuan-Lang.Crystal Structure and Molecular Mechanics Calculations of the Addition Product of Acetylacetone and Methyl 1-Naphthoate, C17H18O4[J]. Acta Phys. -Chim. Sin., 1991,7(02): 191-195
157. Hu Sheng-Zhi; Huang Ming-Sheng; Cheng Xian-En; Zhou Yuan-Lang.Crystal Structure and Molecular Mechanics Calculations of the Photodimerization Product of Acetylacetone, C10H16O4[J]. Acta Phys. -Chim. Sin., 1991,7(02): 196-201
158. Shangguan Guo-Qiang; Zhang Shu-Gong; Jin Zhong-Sheng; Liu Shu-Ying; Ni Jia-Zuan.Crystal and Molecular Structures and MS Analyse of β-Carboxylethyl (or α-methylethyl) Germanium Trichlorides[J]. Acta Phys. -Chim. Sin., 1991,7(02): 223-226
159. Yang Qing-Chuan; Li Yi-Li; Tang You-Qi; Fu Heng.Study on the Thermal Motion N-Phenylphthalimide and 2-Phenylquinoxaline in Solid State[J]. Acta Phys. -Chim. Sin., 1991,7(01): 77-81
160. QU Hong-Mei, CHONG Ze-Peng, CHEN Xu, MEN Yi-Can, SHEN Hai-Jiao.Synthesis and Properties of a Series of Dinaphthosiloles[J]. Acta Phys. -Chim. Sin., 0,(): 0-0
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