ISSN 1000-6818CN 11-1892/O6CODEN WHXUEU
Acta Phys Chim Sin >> 2017,Vol.33>> Issue(3)>> 563-572     doi: 10.3866/PKU.WHXB201612072         中文摘要
Preparation and Characterization of Pt-Ni-SnO2/C for Ethanol Oxidation Reaction
HUANG Ming-Hui1, JIN Bi-Yao1, ZHAO Lian-Hua1, SUN Shi-Gang2
1 Department of Chemistry, College of Science, Yanbian University, Yanji 133002, Jilin Province, P. R. China;
2 State Key Laboratory of Physical Chemistry of Solid Surfaces of Xiamen University, Xiamen 361005, Fujian Province, P. R. China
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A series of Pt/C, Pt-Ni1/3/C, Pt-SnO2/C and Pt-Nix-SnO2/C (x=1/4, 1/3, 2/3, 1) anode electro-catalysts have been synthesized by an improved Bönnemann method. The crystal structure, surface morphology and surface electronic structure were characterizated by X-ray diffraction (XRD), high resolution transmission electron microscope (HR-TEM) and X-ray photoelectron spectroscopy (XPS). The electro-catalytic activities were characterizated by linear sweep voltammetry (LSV) and amperometric current density-time (j-t) curve techniques for ethanol oxidation reaction (EOR). In situ spectroelectrochemical studies have been used to identity adsorbed reaction intermediates and products (in situ Fourier transform infrared spectroscopy, FT-IR). XRD and HR-TEM analysis revealed two phases in the ternary Pt-Ni-SnO2/C catalyst:Pt-Ni alloys and SnO2. XPS results show that the electronic structure of the Pt in Pt-Ni1/3-SnO2/C might be changed due to the addition of Ni. The activity of Pt-Ni-SnO2/C for EOR was found to be higher than that of Pt/C, Pt-Ni/C and Pt-SnO2/C catalysts. The incorporation of Ni and SnO2 did not significantly improve C-C bond breaking for complete oxidation of ethanol, but the synergy under the low potential (0.1 V) to strengthen the further oxidation of acetaldehyde, generate the acetic acid.

Keywords: Platinum   Nickel   Stannic oxide   Ethanol electricoxidation  
Received: 2016-10-12 Accepted: 2016-12-07 Publication Date (Web): 2016-12-07
Corresponding Authors: ZHAO Lian-Hua Email:

Fund: The project was supported by the Jilin Provincial Science and Technology Project of China (20120741) and Opening Foundation of State Key Laboratory of Physical Chemistry of Solid Surface of Xiamen University,China (201407)

Cite this article: HUANG Ming-Hui, JIN Bi-Yao, ZHAO Lian-Hua, SUN Shi-Gang. Preparation and Characterization of Pt-Ni-SnO2/C for Ethanol Oxidation Reaction[J]. Acta Phys. -Chim. Sin., 2017,33 (3): 563-572.    doi: 10.3866/PKU.WHXB201612072

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61. KONG De-Shuai, WANG Jian-Ming, PI Ou-Yang, SHAO Hai-Bo, ZHANG Jian-Qing.Electrochemical Fabrication and Pseudocapacitive Performance of a Porous Nanostructured Nickel-Based Complex Film Electrode[J]. Acta Phys. -Chim. Sin., 2011,27(04): 764-768
62. JIA Fei, WANG Zhou-Cheng.Electrochemical Study on Electroless Nickel Plating Using Sodium Borohydride as the Reductant[J]. Acta Phys. -Chim. Sin., 2011,27(03): 633-640
63. XU Jun-Ke, SHEN Li-Hong, ZHOU Wei, MA Jian-Xin.Mechanism of Biogas Reforming for Hydrogen Production over Ni-Co Bimetallic Catalyst[J]. Acta Phys. -Chim. Sin., 2011,27(03): 697-704
64. WANG Jia-Yong, BI Si-Wei, ZHAO Jun-Feng.Reaction Mechanisms between (Cl-nacnac)Pt(H) and a Terminal Alkyne[J]. Acta Phys. -Chim. Sin., 2011,27(03): 571-576
65. YU Li-Qiu, CHEN Shu-Li, CHANG Sha, LI Yun-Hu, GAO Yin-Yi, WANG Gui-Ling CAO Dian-Xue.Supercapacitance of NiCo2O4 Nanowire Arrays Grown on Nickel Foam[J]. Acta Phys. -Chim. Sin., 2011,27(03): 615-619
66. ZHANG Hai-Jun, ZHANG Xiao-Gang, YUAN Chang-Zhou, GAO Bo, SUN Kang, FU Qing-Bin, LU Xiang-Jun, JIANG Jian-Chun.Preparation of Water Soluble Chitosan-Based Porous Carbon/NiO Composites and Their Electrochemical Capacitive Behavior[J]. Acta Phys. -Chim. Sin., 2011,27(02): 455-460
67. SUN Li-Li, ZHAO Yue-Hong, HAN Qing-Zhen, WEN Hao.Solvent Effect in the Reaction between Bis[1,2-di(trifluoromethyl) ethylene-1,2-dithiolato] Nickel and Butadiene[J]. Acta Phys. -Chim. Sin., 2010,26(12): 3345-3350
68. WANG Yao-Qiong, WEI Zi-Dong, CAI Hong-Ying, ZHANG Qian, ZHAO Qiao-Ling.Pt/FTO Counter Electrode for Dye-Sensitized Solar Cells Prepared by Sputtering-Displacement[J]. Acta Phys. -Chim. Sin., 2010,26(11): 2957-2961
69. XIE Xiu-Juan, CHEN Wen-Kai, SUN Bao-Zhen, GUO Xin, ZHANG Yong-Fan.Adsorption Behavior of NO on Cu3Pt(111) Surface[J]. Acta Phys. -Chim. Sin., 2010,26(11): 3047-3051
70. SONG Li-Jun, MENG Hui-Min.Electrodeposition of Nanocrystalline Nickel Alloys and Their Hydrogen Evolution in Seawater[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2375-2380
71. SONG Hua,GUO Yun-Tao, LI Feng ,YU Hong-Kun.Preparation, Hydrodesulfurization and Hydrodenitrogenation Performance of a Ni2P/TiO2-Al2O3 Catalyst[J]. Acta Phys. -Chim. Sin., 2010,26(09): 2461-2467
72. LI Yong-Jun, ZHOU You-Chen, SUN Shi-Gang.Preparation of Core-Shell SiO2/Pt Particles via Layer-by-Layer Assembly and Their Electrooxidation and In-situ Electrochemical FTIR Spectra for CO[J]. Acta Phys. -Chim. Sin., 2010,26(07): 1773-1778
73. WU Jian, WANG Yu, HUANG Feng, YANG Yang, MENG Chang-Gong.Thermal Diffusion Synthesis and Characterization of SnO2 Clusters within ZSM-5 Crystals[J]. Acta Phys. -Chim. Sin., 2010,26(06): 1705-1710
74. WANG Xiao-Lei, PAN Xiang-Min, LIN Rui, KOU Su-Yuan, ZOU Wei-Bing, MA Jian-Xin.Dimethyl Ether Steam Reforming for Hydrogen Production over Cu-Ni/γ-Al2O3 Bi-Functional Catalyst[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1296-1304
75. ZHANG Hui-Juan, SONG Huai-He, ZHOU Ji-Sheng, ZHANG Hong-Kun, CHEN Xiao-Hong.Preparation and Electrochemical Properties of SnO2/Onion-Like Hollow Carbon Nanoparticle Composites as Anode Materials for Lithium-Ion Batteries[J]. Acta Phys. -Chim. Sin., 2010,26(05): 1259-1263
76. YIN Guo-Wei, WEI Wei, XU Jia, LI Zhi-Fen, WANG Bao-Huai, DU Wei-Hong.Interaction of Nickel(II) with Yeast Alcohol Dehydrogenase[J]. Acta Phys. -Chim. Sin., 2010,26(04): 1107-1112
77. JIANG Lei, HUANG Hui, WANG Chun-Tao, ZHANG Wen-Kui, GAN Yong-Ping, TAO Xin-Yong.Photoelectrochromic Properties of TiO2-xNx/NiO Bilayer Thin Films[J]. Acta Phys. -Chim. Sin., 2010,26(02): 299-303
78. ZANG Yang, HAO Xiao-Gang, WANG Zhong-De, ZHANG Zhong-Lin, LIU Shi-Bin.Copolymerization and Capacitive Performance of Composite Carbon Nanotubes/Polyaniline/Nickel Hexacyanoferrate Films[J]. Acta Phys. -Chim. Sin., 2010,26(02): 291-298
79. GAO Yin-Yi, CAO Dian-Xue, WANG Gui-Ling, YIN Cui-Lei.Catalytic Behavior of NiCo2O4 for H2O2 Electroreduction in Alkaline Medium[J]. Acta Phys. -Chim. Sin., 2010,26(01): 29-33
80. PANG Xu, MA Zheng-Qing, ZUO Lie.Sn Doped MnO2 Electrode Material for Supercapacitors[J]. Acta Phys. -Chim. Sin., 2009,25(12): 2433-2437
81. ZHAO Ya-Hua.Hydrolysis Mechanism of New Anticancer Drug Transplatin Analogues Containing One Nonplanar Heterocyclic Amine Ligand[J]. Acta Phys. -Chim. Sin., 2009,25(11): 2350-2356
82. ZHAO Yan-Chun, LAN Huang-Xian, TIAN Jian-Niao, YANG Xiu-Lin, WANG Feng-Yang.Electrocatalytic Oxidation of Methanol on Pt Nanoparticles Supported on Porous Poly(N-acetylaniline) Nanofibrils[J]. Acta Phys. -Chim. Sin., 2009,25(10): 2050-2054
83. CAO Yin-Liang, WANG Feng, LIU Jing-Jun, WANG Jian-Jun, ZHANG Liang-Hu, QIN Shi-Yong.Electrochemical Preparation and Electrocatalytic Mechanisms of Ni-S Active Cathode for Hydrogen Evolution[J]. Acta Phys. -Chim. Sin., 2009,25(10): 1979-1984
84. FANG Xiang, SHEN Pei-Kang.Mechanism of Ethanol Electrooxidation on Pd Electrode[J]. Acta Phys. -Chim. Sin., 2009,25(09): 1933-1938
85. LANG Bao, LI Xiu-Jin, JI Sheng-Fu, FABIEN Habimana, LI Cheng-Yue.Effect of La Promoter on the Structure and Performance of Ni/SBA-15 Catalyst in the Reforming of Simulated Biogas to Syngas[J]. Acta Phys. -Chim. Sin., 2009,25(08): 1611-1617
86. WANG Fang, LIU Jun-Hua, YIN Yuan-Qi, XU Xian-Lun.Palygorskite Supported Platinum Catalysts with High Activity and Selectivity for the Liquid-Phase Hydrogenation of para-Chloronitrobenzene[J]. Acta Phys. -Chim. Sin., 2009,25(08): 1678-1682
87. AI Xin-Peng, YUE Bao-Hua, WANG Xue-Guang, YANG Jun, LU Xiong-Gang, DING Wei-Zhong.Catalytic Conversion of Tar Components in Hot Coke Oven Gas over Ni/MgO-Al2O3 Catalysts[J]. Acta Phys. -Chim. Sin., 2009,25(08): 1517-1522
88. GAO Yun-Fang, YU Li-Li| LU Qing-Qing, MA Chun-An.Electrochemical Oxidation Behavior of Iodide on Platinum Electrode in Acid Solution[J]. Acta Phys. -Chim. Sin., 2009,25(07): 1421-1426
89. TAO Fei-Fei, XU Zheng.Effective Synthesis of Magnetic Metal Nickel Nanotubes[J]. Acta Phys. -Chim. Sin., 2009,25(05): 977-980
90. LI Xue-Ling, YUE Bao-Hua, WANG Xue-Guang, YU Fei, KONG Ling-Hua, LU Xiong-Gang, DING Wei-Zhong.Preparation of NiO/MgxSi1-xOy Catalysts and Their Application in Catalytic Cracking of Tar Components in Hot Coke Oven Gas[J]. Acta Phys. -Chim. Sin., 2009,25(04): 762-766
91. YANG Hong-Yan, GUO Pan-Pan, LI Wei-Shan.Electrodeposition Preparation and Activity of CO-Resistant Catalyst Pt-HxWO3 for Methanol Oxidation[J]. Acta Phys. -Chim. Sin., 2009,25(04): 719-723
92. MA Ruo-Biao, FU Yan-Bao, MA Xiao-Hua.Preparation and Electrochemical Performance of Tin-Dioxide Filled Multi-Walled Carbon Nanotubes[J]. Acta Phys. -Chim. Sin., 2009,25(03): 441-445
93. XU Jun-Ke; LI Zhao-Jing; WANG Ji-Hui; ZHOU Wei; MA Jian-Xin.Characterization and Analysis of Carbon Deposited on the Surface of Ni/Al2O3 Catalyst for Methane Dry Reforming[J]. Acta Phys. -Chim. Sin., 2009,25(02): 253-260
94. PAN Lei-Ming, ZHOU Zhi-You, CHEN De-Hun, SUN Shi-Gang.Electrochemical and In Situ FTIR Studies of Adsorption and Oxidation of Dimethyl Ether on Platinum Electrode[J]. Acta Phys. -Chim. Sin., 2008,24(10): 1739-1744
95. TANG Ya-Wen; MA Guo-Xian; ZHOU Yi-Ming; BAO Jian-Chun; LU Lu-De; LU Tian-Hong.Electrocatalytic Oxidation of Ethanol on Pt/C Catalysts with Different Pt Particle Sizes[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1615-1619
96. XU Jun-Ke; REN Ke-Wei; WANG Xiao-Lei; ZHOU Wei; PAN Xiang-Min; MA Jian-Xin.Effect of La2O3 on Ni/γ-Al2O3 Catalyst for Biogas Reforming to Hydrogen[J]. Acta Phys. -Chim. Sin., 2008,24(09): 1568-1572
97. RUAN Xiao-Yun; FANG Yun; FAN Ye.Preparation of Ultrafine Nickel Powders in SDS-PVP Aqueous Solution[J]. Acta Phys. -Chim. Sin., 2008,24(08): 1513-1518
98. ZHANG Jin; ZHANG Tong-Lai; YANG Li; ZHANG Jian-Guo; CUI Yan.Preparation, Crystal Structure and Thermal Decomposition Character of [Ni(CHZ)3]SO4·3H2O[J]. Acta Phys. -Chim. Sin., 2008,24(05): 760-766
99. WANG Lin; CHEN Shun-Quan; LIU Yuan.NiO/LaMnO3 Catalysts for Steam Reforming of Ethanol[J]. Acta Phys. -Chim. Sin., 2008,24(05): 849-854
100. ZHOU Jian-Hua; HE Jian-Ping; JI Ya-Jun; ZHAO Gui-Wang; ZHANG Chuan-Xiang; CHEN Xiu; WANG Tao.Influence of Hierarchical Porosity in Carbon Material on Electrocatalytic Property of Supported Pt Nanoparticles[J]. Acta Phys. -Chim. Sin., 2008,24(05): 839-843
101. CHEN Yu-Ting; ZHANG Hai-Yan; ZHANG Guo-Qing; CHEN Yi-Ming; ZHU Qing-Feng.Influence of Addition of Carbon Nanotubes in the Hydrogen Storage Alloy Electrode on the Performance of SC High Power Batteries[J]. Acta Phys. -Chim. Sin., 2008,24(03): 527-532
102. XU Xing-Zhong; YANG Jian-Feng; LI Xiao-Nian; YAN Xin-Huan.Hydrogenation of o-chloronitrobenzene over CNTs Supported Pt Catalyst Obtained by Laser Vaporization of Bulk Metal[J]. Acta Phys. -Chim. Sin., 2008,24(01): 121-126
103. CHENG Zhi-Peng; YANG Yi; WANG Yi; LI Miao-Miao; LI Feng-Sheng.Oxidation Ability of Nanocrystalline Ni-Coated Al Powders[J]. Acta Phys. -Chim. Sin., 2008,24(01): 152-156
104. MA Chun-An; WANG Xiao-Juan; LI Guo-Hua; LI Mei-Chao; CHEN Song.Electroreduction Characteristics of Nitromethane in Ionic Liquid BMImBF4[J]. Acta Phys. -Chim. Sin., 2007,23(11): 1719-1722
105. ZHONG Qi-Ling; ZHANG Bing; DING Yue-Min; LIU Yue-Long; RAO Gui-Shi; WANG Guo-Fu; REN Bin; TIAN Zhong-Qun.In-situ Surface-enhanced Raman Spectroscopic Investigation on Ethanol Electrooxidation in Different Media[J]. Acta Phys. -Chim. Sin., 2007,23(09): 1432-1436
106. YU Le; YAO Jia; FU Zheng-Wen.Laser Ablated Preparation of Noble Metal Nanoparticles in Liquid[J]. Acta Phys. -Chim. Sin., 2007,23(06): 945-949
107. FENG Rui-Xiang; CAO Yu-Liang; AI Xin-Ping; YANG Han-Xi.AgNi Alloy Used as Anodic Catalyst for Direct Borohydride Fuel Cells[J]. Acta Phys. -Chim. Sin., 2007,23(06): 932-934
108. ZHAO Hai-Jun; HOU Hai-Tao; CAO Jie-Ming ZHENG Ming-Bo; LIU Jing-Song; ZHANG Fang.Solvothermal Synthesis of Mesoporous SnO2 with Spongy Structure[J]. Acta Phys. -Chim. Sin., 2007,23(06): 959-963
109. PAN Shen-Min; ZHOU Qin; ZHAO Fa-Qiong; ZENG Bai-Zhao.Influence of m-4-m Structured Gemini Surfactants on the Adsorption-Stripping Voltammetric Behavior of Methylene Blue on a Platinum Electrode[J]. Acta Phys. -Chim. Sin., 2007,23(06): 964-968
110. REN Jun-Xia; ZHOU Zhen; YAN Jie.Effects of Yttrium-Doping on High-temperature Electrochemical Performances of Nickel Hydroxide Electrodes[J]. Acta Phys. -Chim. Sin., 2007,23(05): 738-742
111. TONG Shao-Ping;MA Chun-An;FEI Hui.Deactivation of Two Different Kinds of Anodes during the Degradation of Organics and Their Oxidative Mechanisms[J]. Acta Phys. -Chim. Sin., 2007,23(03): 424-428
112. ZHONG Qi-Ling;ZHANG Bing;DING Yue-Min;RAO Gui-Shi;WANG Guo-Fu;JIANG Yu-Xiong;REN Bin;TIAN Zhong-Qun.Microwave Radiation-Assisted Synthesis of Pt-CNTs[J]. Acta Phys. -Chim. Sin., 2007,23(03): 429-432
113. LI Cui-Ping;ZHAO Rui-Hong;GUO Fen;CHEN Jian-Feng.Preparation and Characterization of Ni Catalysts Supported on Organized Mesoporous Alumina[J]. Acta Phys. -Chim. Sin., 2007,23(02): 157-161
114. SHENG Jiang-Feng;MA Chun-An;ZHANG Cheng;LI Guo-Hua .Preparation of Tungsten Carbide-Supported Nano Platinum Catalyst and Its Electrocatalytic Activity for Hydrogen Evolution[J]. Acta Phys. -Chim. Sin., 2007,23(02): 181-186
115. YU Dan-Mei;CHEN Chang-Guo;SI Yu-Jun;ZHOU Shang-Qi;WANG Li.Study on the Electronic Structure of Doped Nickel Hydroxide Using the DV-Xα Method of Quantum Chemistry[J]. Acta Phys. -Chim. Sin., 2007,23(01): 27-31
116. ZHOU Hong-Wei;LI Huai-Xiang;JIANG Zheng-Wei;ZUO Xiang-Qing.Treatment of ZnS:Mn Phosphors by Partial Sublimation of SnO2:Sb Xerogel[J]. Acta Phys. -Chim. Sin., 2007,23(01): 88-91
117. FANG Li-Mei;LI Zhi-Jie;LIU Chun-Ming;ZU Xiao-Tao.Synthesis of Fe3+-modified SnO2 Nanoparticles by Hydrothermal Method[J]. Acta Phys. -Chim. Sin., 2006,22(10): 1212-1216
118. CHU Dao-Bao;YIN Xiao-Juan;FENG De-Xiang;LIN Hua-Shui;TIAN Zhao-Wu.Electrocatalytic Oxidation of Ethanol on Pt/nanoTiO2-CNT Complex Catalysts[J]. Acta Phys. -Chim. Sin., 2006,22(10): 1238-1242
119. ZOU Ji-Jun;LIU Chang-Jun.Preparation of NiO/SrTiO3 with Cold Plasma Treatment for PhotocatalyticWater Splitting[J]. Acta Phys. -Chim. Sin., 2006,22(08): 926-931
120. GAO Jie;WANG Shi-Zhong.Study of Ni Composite Anodes for Dimethyl Ether Fuel Cell[J]. Acta Phys. -Chim. Sin., 2006,22(07): 851-855
121. CHEN Hu;XU Xing-You;GAO Jian;YANG Xu-Jie;LU Lu-De;WANG Xin.Study on Crystal Structure of [Ni(phen)3](ClO4)2[J]. Acta Phys. -Chim. Sin., 2006,22(07): 856-859
122. ZHANG Yi-Wei;ZHOU Yu-Ming;QIU An-Ding;WANG Yu;XU Yi;WU Pei-Cheng.Effect of Na Addition on Catalytic Performance of PtSn/ZSM-5 Catalyst for Propane Dehydrogenation[J]. Acta Phys. -Chim. Sin., 2006,22(06): 672-678
123. SUN Yuan-Hua;ZHANG Tong-Lai;ZHANG Jian-Guo;YANG Li;QIAO Xiao-Jing.Kinetics of Flash Pyrolysis of [Co(CHZ3](ClO42 and [Ni(CHZ)3](ClO4)2[J]. Acta Phys. -Chim. Sin., 2006,22(06): 649-652
124. NI Wen-Bin;LIU Tian-Qing;GUO Rong.Effect of SDS on the Electrochemical Oscillation of Nickel in HNO3/Cl-/H2O Solution[J]. Acta Phys. -Chim. Sin., 2006,22(04): 502-506
125. ZHONG Qi-Ling; HUANG Peng; ZHANG Bing; YANG Xiong-Yuan; DING Yue-Min; ZHOU Hai-Hui; REN Bin; TIAN Zhong-Qun.SERS Study of the Electrooxidation of Formic Acid on Pt-Ru/GC[J]. Acta Phys. -Chim. Sin., 2006,22(03): 291-295
126. LIN Wei; ZHANG Yong-fan; LI Yi; CHEN Yong; LI Jun-qian.First Principle Studies on the Geometry and Electronic Structures of the SnO2(110) Surface[J]. Acta Phys. -Chim. Sin., 2006,22(01): 76-81
127. ZHANG Guo-Lin;CHUAI Yu-Tao;GUO Hai-Qing;ZOU De-Chun.Synthesis and Electrophosphorescence of a Red Platinum (II) Quinoxaline Complex[J]. Acta Phys. -Chim. Sin., 2005,21(12): 1407-1410
128. XU Liang-Qin; DU Zhan-He; FENG Jia-Min; LÜ Xiao-Li; GAO Qing-Yu.The Behavior of Electrochemical Oxidation of Thiosulfate on Platinum Electrode[J]. Acta Phys. -Chim. Sin., 2005,21(12): 1422-1425
129. ZHAO Peng; FANG Hui-jue; XUE Teng; QI Xi-min; LU Jia-xing.Diffusion Coefficients and Rate Constants of NiCl2(bpy)3 in DMF Determined by Chronocoulometry[J]. Acta Phys. -Chim. Sin., 2005,21(11): 1235-1239
130. TAO Xiao-Jun; LI Zhi-Wei; CHEN Hong-Jie; ZHANG Ping-Yu; ZHANG Zhi-Jun; WU Zhi-Shen; DANG Hong-Xin.A New Approach to Synthesize Nickel Nanoparticles[J]. Acta Phys. -Chim. Sin., 2005,21(05): 569-572
131. WU Mei-Yin; WANG Jian-Ming; ZHANG Jian-Qing; CAO Chu-Nan.Structure and Electrochemical Performance of Mn-substituted Nickel Hydroxide[J]. Acta Phys. -Chim. Sin., 2005,21(05): 523-527
132. WANG Xiao-Feng; WANG Da-Zhi; LIANG Ji.Pseudo-capacitance of Ultrafine Nickel Hydroxide Prepared by Sol-gel Method[J]. Acta Phys. -Chim. Sin., 2005,21(02): 117-122
133. TIAN Na;CHEN Wei;SUN Shi-Gang.Spectroscopic Characterization and Electrocatalytic Properties of Core-Shell Au-Pt Nanoparticles[J]. Acta Phys. -Chim. Sin., 2005,21(01): 74-78
134. Yang Fang-Zu;Ma Zhao-Hai;Huang Ling;Xu Shu-Kai;Zhou Shao-Min.Electrodeposition, Structure and Properties of an Amorphous Ni-W-B/ZrO2 Composite Coating[J]. Acta Phys. -Chim. Sin., 2004,20(12): 1411-1416
135. Liu Xiang-Yang;Zhang Zhong-Suo;Zhang Xing-Tang;Cheng Ke;Huang Ya-Bin;Wang De-Jun;Du Zu-Liang.Photovoltage Property about Heterojunction Composite Film with 1,4-bis (ferrocene) Thiophene and SnO2 Nanoparticles[J]. Acta Phys. -Chim. Sin., 2004,20(09): 1167-1171
136. Zhong Qi-Ling;Zhang Bin;Zhang Lei;Yang Xiong-Yuan;Huang Peng.In-situ SERS of Dissociative Adsorption and Oxidation of Ethanol on Roughed Platinum Electrodes[J]. Acta Phys. -Chim. Sin., 2004,20(09): 1163-1166
137. Fu Tie-Xiang;Tao Jun;Li Dan.Synthesis and Gas Sensitive Properties of Mixed-Ligand Complex Ni(mnt)(bipyO2) with Big Conjugate System[J]. Acta Phys. -Chim. Sin., 2004,20(08): 843-848
138. Liu Ying-Xin;Wei Zuo-Jun;Chen Ji-Xiang;Zhang Ji-Yan;Li Xin-Xue;Wei Xiong-Hui.Sol-gel Preparation,Characterization and Hydrogenation Property of Silica Supported Ni Catalyst[J]. Acta Phys. -Chim. Sin., 2004,20(07): 780-784
139. Wang Qin-Ping;Lü Xing-Mei;Chen Hong-Tao;Zhou Li-Hua;Chen Shu-Sen;Lü Dian-Zhen.Activity Coefficients of HCl in the Nickel Sulfate Solution[J]. Acta Phys. -Chim. Sin., 2004,20(02): 186-190
140. Chen Ji-Xiang;Qiu Ye-Jun;Zhang Ji-Yan;Su Wan-Hua.Influence of La2O3 and CeO2 Promoters on Physico-chemical Properties and Catalytic Performance of Ni/MgO Catalyst in Methane Reforming with Carbon Dioxide[J]. Acta Phys. -Chim. Sin., 2004,20(01): 76-80
141. Xu Zong-Xiang;Lin Jing-Dong;Ou Yan;Liao Dai-Wei.Preparation of Hollow Carbon Spheres by Catalytic Pyrolysis of C2H2[J]. Acta Phys. -Chim. Sin., 2003,19(11): 1035-1038
142. Li Chun-Lin;Fu Yi-Lu;Bian Guo-Zhu.Surface Basicity and Catalytic Performance on Ni/Ce-Zr-Al-O Catalyst for CO2+CH4 Reforming[J]. Acta Phys. -Chim. Sin., 2003,19(10): 902-906
143. Wang Shi-Zhong;Ishihara Tatsumi.Improvement of the Performance of Fuel Cells Anodes with Sm3+ Doped CeO2[J]. Acta Phys. -Chim. Sin., 2003,19(09): 844-848
144. Wang Shi-Zhong;Ishihara Tatsumi.Improvement of the Performance of Fuel Cells Anodes with Sm3+ Doped CeO2 Interlayer[J]. Acta Phys. -Chim. Sin., 2003,19(09): 849-853
145. Zeng Yue;Zheng Yang-Cun;Yi Jian-Long;Yu Shang-Ci;Yang Chun-Ming;Li Ze-Lin.Kinetics and Mechanism of Hypophosphite Electrooxidation on a Nickel Electrode[J]. Acta Phys. -Chim. Sin., 2003,19(08): 718-722
146. Gu Feng-Cai;Zhao Zhu-Xuan;Li Ying-Hui;Men Juan;Yan Ju-Ming;Liu Rui-Xian;Zhang Li-Hua.Preparation and Characterization of SurfaceModified SnO2 Nanocrystals[J]. Acta Phys. -Chim. Sin., 2003,19(07): 621-625
147. Zhao Yong-Xiang;Qin Xiao-Qin;Hou Xi-Cai;Xu Xian-Lun;Liu Dian-Sheng.Preparation,Characterization and Properties of Selective Hydrogenation on Ni-based Catalysts[J]. Acta Phys. -Chim. Sin., 2003,19(05): 450-454
148. Liu Yue;Liu Jia-Wen;Yang Xiao-Zhen.Cationic Reaction Mechanism for Ethylene Polymerization of New Nickel Catalysts[J]. Acta Phys. -Chim. Sin., 2002,18(12): 1068-1070
149. Zhou Xiao-Lei;Wang Bao-Huai;Li Zhi-Fen;Zeng Hui-Hui.Studies of the Effects of Anti-tumor Compounds on the Assembly and Melting Denaturation of Tubulin in vitro[J]. Acta Phys. -Chim. Sin., 2002,18(11): 1009-1013
150. Zhou Zhi-You;Sun Shi-Gang;Chen Sheng-Pei;Si Di;Gong Hui.Electrochemical In Situ Step-scan Time-resolved Microscope FTIR Spectroscopy[J]. Acta Phys. -Chim. Sin., 2002,18(11): 989-993
151. Ma Yan-Feng;Li Wei;Zhang Ming-Hui;Zhang Bao-Gui;Tao Ke-Yi.New Method of Preparing NiP and NiPB Amorphous Alloys Using Nickel Hypophosphite as Reactant[J]. Acta Phys. -Chim. Sin., 2002,18(10): 938-942
152. Zhou Xing-Fu;Han Ai-Jie;Chu Dao-Bao;Lin Chang-Jian;Tian Zhong-Qun.Preparation of Nanocrystalline NiO by Electrochemical Dissolution of Nickel[J]. Acta Phys. -Chim. Sin., 2002,18(07): 613-616
153. Zhu Jian-Xin;Li Jin-Hui;Nie Yong-Feng.Vacuum Thermal Recycling of Used Ni-Cd Batteries[J]. Acta Phys. -Chim. Sin., 2002,18(06): 536-539
154. Kong Jing-Lin;Xue Kuan-Hong;Shao Ying;He Chun-Jian;Chen Qiao-Ling.Measurements for the Kinetic Parameters of Electrocatalytic Oxidation of Ethanol at the Nickel Nanowire Electrode[J]. Acta Phys. -Chim. Sin., 2002,18(03): 268-271
155. Xu Yan-Qi;Cai Wei-Li;Wang Yin-Hai;Mou Ji-Mei.Fabrication and Characterization of Ordered Nanoporous Ni Membranes[J]. Acta Phys. -Chim. Sin., 2001,17(11): 991-994
156. Ng Seikweng;Hu Sheng-Zhi.Reformulation of two Ni(Ⅱ)-8-hydroxyquinoline complexes from Calculated Structure Factors[J]. Acta Phys. -Chim. Sin., 2001,17(11): 1040-1044
157. Zhong Shun-He;Chen Song-Zhe;Xin Xiu-Lan.Laser Stimulated Surface Reaction of C2H4 on Nickel Sulfate[J]. Acta Phys. -Chim. Sin., 2001,17(10): 936-939
158. Yang Yong-Lai;Xu Heng-Yong;Li Wen-Zhao.Study on Carbon Deposition of CH4,C2H6 and C2H4 Cracking over Ni-based Catalysts[J]. Acta Phys. -Chim. Sin., 2001,17(09): 773-775
159. Zhou Chang-Jun;Zhu Yue-Xiang;Xie You-Chang.Catalytic Combustion of Methane over Tin Dioxide Supported Silver Catalysts[J]. Acta Phys. -Chim. Sin., 2001,17(09): 850-854
160. Li Hong;Chao Hui;Jiang Xiong;Ji Liang-Nian.Comparative Study of the Electrochemical Behavior of the Central Ions of Four Ruthenium (Ⅱ) Complexes[J]. Acta Phys. -Chim. Sin., 2001,17(08): 728-732
161. Zhou Guo-Ding;Kamkin A N;Liao Qiang-Qiang.Photoelectrochemical Study of Copper-Nickel and Copper-Cobalt Electrodes in Alkaline Solution[J]. Acta Phys. -Chim. Sin., 2001,17(07): 614-618
162. Yang Zhi-Hong;Luo He-Kuan;Mao Bing-Quan;Tang Rui-Guo;Yu Ding-Sheng;Wang Gui-Hua.In Situ UVVis Studies on Nickel Catalyst for Ethylene Polymerization[J]. Acta Phys. -Chim. Sin., 2001,17(05): 460-464
163. Wang Yu;Liu Guan-Kun;He Feng-Rong;Tong Ye-Xiang.Electrodeposition of Ho-Ni Alloy from Dimethyformamide Bath[J]. Acta Phys. -Chim. Sin., 2001,17(03): 206-209
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