Acta Phys. -Chim. Sin. ›› 2023, Vol. 39 ›› Issue (8): 2301027.doi: 10.3866/PKU.WHXB202301027
Special Issue: Solid State Batteries
• REVIEW • Previous Articles
Designing High-Performance Sulfide-Based All-Solid-State Lithium Batteries: From Laboratory to Practical Application
Liu Yuankai1,2, Yu Tao1,2, Guo Shaohua1,2,*(
), Zhou Haoshen1,*()
- 1 College of Engineering and Applied Sciences, Nanjing University, Nanjing 210023, China
2 Shenzhen Research Institute of Nanjing University, Shenzhen 518000, Guangdong Province, China
-
Received:2023-01-16Accepted:2023-02-13Published:2023-03-23 -
Contact:Guo Shaohua, Zhou Haoshen E-mail:shguo@nju.edu.cn;hszhou@nju.edu.cn -
Supported by:The project was supported by the National Key R&D Program of China(2021YFA1202300);the National Natural Science Foundation of China(22239002);the National Natural Science Foundation of China(22075132);the Science and Technology Innovation Fund for Emission Peak and Carbon Neutrality of Jiangsu Province(BK20220034);the Natural Science Foundation of Jiangsu Province, China(BK20211556);the Shenzhen Science and Technology Innovation Committee(RCYX20200714114524165);the Shenzhen Science and Technology Innovation Committee(JCYJ20210324123002008);the Shenzhen Science and Technology Innovation Committee(2021Szvup055);the Open Fund of the Guangdong Provincial Key Laboratory of Advanced Energy Storage Materials(aesm2021xx)
Cite this article
Liu Yuankai, Yu Tao, Guo Shaohua, Zhou Haoshen. Designing High-Performance Sulfide-Based All-Solid-State Lithium Batteries: From Laboratory to Practical Application[J]. Acta Phys. -Chim. Sin. 2023, 39(8), 2301027. doi: 10.3866/PKU.WHXB202301027
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Fig 1
Radar chart presenting the most relevant properties of four typical SSE. The considered properties include ionic conductivity, mechanical propertied, processing cost, interface contact, electrochemical window, chemical window."
Fig 1
Fig 2
Schematic illustration of issues experienced in sulfide-based all-solid-state lithium batteries. For cathode/electrolyte interface, the mainly issues are the side reactions between solid electrolyte and cathode active material (CAM). For sulfide solid electrolyte, the mainly issue is the further improvement of ionic conductivity and air stability. For anode/electrolyte interface, the mainly issues are the lithium dendrite and side reactions between solid electrolyte and lithium metal."
Fig 2
Fig 3
(a) Schematic illustration of chlorination of lithium argyrodites on the SE/NCM cathode material Interface 67; (b) schematic illustration of sulfite modified Li-rich Mn-based oxide (LRMO) cathode material (Li1.2Mn0.54Co0.13Ni0.13O2) 68. (a) Adapted with permission from Ref. 67, Copyright 2019, Wiley-VCH; (b) Adapted with permission from Ref. 68, Copyright 2022, AAAS."
Fig 3
Fig 4
(a) Schematic illustration of space charge layer reflected by Li concentration on the cathode active material/SE interface 75; (b) DPC-STEM image of Li1.175Nb0.645Ti0.4O3(LNTO)-coated LCO; (c) schematic diagram of interfacial ion transportation on the LNTO@ LCO and LiNbO3 (LNO)@LCO 80; (d) schematic illustration of the influence of ferroelectric and paraelectric BaTiO3 coating on the interface with applied electric field; (e) comparison of cycling performance of all-solid-state batteries with bare LCO, ferroelectric BaTiO3, paraelectric BaTiO3 and paraelectric SrTiO3 81. (a) Adapted with permission from Ref. 75, Copyright 2014, American Chemical Society; (b, c) Adapted with permission from Ref. 80, Copyright 2022, Wiley-VCH; (d, e) Adapted with permission from Ref. 81, Copyright 2022, Wiley-VCH."
Fig 4
Fig 5
(a) The Li-ion migration pathways analyzed using the maximum entropy method (MEM); (b) influence of Br−/S2− site-disorder on the radial distribution functions of Li+ in 4d site 87; (c) explanation of the influence of Bi, O co-doped Li3PS4 on the air stability by Soft-Hard-Acid-Base theory 92; (d) influence of different cations in sulfide solid electrolyte on the hydrolysis reaction energy 93. (a, b) Adapted with permission from Ref. 87, Copyright 2021, Wiley-VCH; (c) Adapted with permission from Ref. 92, Copyright 2022, Wiley-VCH; (d) Adapted with permission from Ref. 93, Copyright 2022, Wiley-VCH."
Fig 5
Fig 6
(a) Schematic of the practical stability window of the LGPS electrolyte and the chemical potential of different alloy electrodes 99; (b) voltage profiles of Li-In alloy during the lithiation process 100; (c) schematic diagrams of the dynamic evolution and interfacial mechanism 101; (d) working mechanism of Ag–C anode and schematic diagrams of all-solid-state battery that comprises a Ag–C nanocomposite anode layer 103. (a) Adapted with permission from Ref. 99, Copyright 2022, AAAS; (b) Adapted with permission from Ref. 100, Copyright 2021, AAAS; (c) Adapted with permission from Ref. 101, Copyright 2022, American Chemical Society; (d) Adapted with permission from Ref. 103, Copyright 2020, Springer Nature."
Fig 6
Fig 7
(a) Schematic of the preparation of the LiI layer on the Li metal surface through a chemical iodine vapor deposition method; (b) critical current density analysis of Li/LiI/LGPS/LiI/Li symmetric battery 112; (c) illustration of in situ formation of the LixMg/LiF/polymer solid electrolyte interphase; (d) critical current density analysis of Li/LGPS/Li cells using LGPS with and without LiMg22 liquid electrolyte treatment 113. (a, b) Adapted with permission from Ref. 112, Copyright 2022, Royal Society of Chemistry; (c, d) Adapted with permission from Ref. 113, Copyright 2021, American Chemical Society."
Fig 7
Fig 8
(a) Schematic illustration of LPSC/LGPS(LSPS)/LPSC multilayer electrolyte; (b) cycling performance of all-solid-state batteries using LPSC/LSPS/LPSC multilayer electrolyte 120; (c) schematic illustration of all-solid-state batteries using LPSC electrolyte with and without PEGDME solid polymer electrolyte and their different influence on Li dendrite, self-discharge and humidity resistance; (d) galvanostatic charge-discharge performance of Li–Li symmetric batteries using LPSC electrolyte with different PEGDME solid polymer electrolyte addition 122. (a, b) Adapted with permission from Ref. 120, Copyright 2021, Springer Nature; (c, d) Adapted with permission from Ref. 122, Copyright 2021, Wiley-VCH."
Fig 8
Table 1
The performance of part of sulfide-based all-solid-state lithium batteries."
| Cathode/electrolyte/anode | Modification method | Current density/ (mA∙cm−2) | Initial capacity/ (mAh∙g−1) | Capacity retention | Ref. | |
| C/E | LNO@NCM712/Li5.5PS4.5Cl1.5/Li-In | LNO coating | 5C | 138.9 | 300 cycles, 88% | |
| LZO@NCM70/LPSC/Li-In | LZO coating | 1.5 | 110 | 650 cycles, 86.1% | ||
| LLTO@NCM532/LPSC/Li-In | LLTO coating | 0.1C | 135 | 200 cycles, 80% | ||
| C/E | LNTO@LCO/LPSC/Li-In | LNTO coating | 0.5C | 147.2 | 1000 cycles, 80% | |
| Li2RuO3/LPSC/Li-In | Li2RuO3 cathode | 0.8 | 210 | 1000 cycles, 90% | ||
| Li2SO4@LRMO/LICF-LPSC/Li-In | Sulfite coating of LRMO cathode | 1C | 130 | 300 cycles, 81.2% | ||
| E | NCM523/Li6.5Sb0.5Ge0.5S5I/ Li-In | Li6.5Sb0.5Ge0.5S5I electrolyte and Li3YCl6 catholyte | 4.77 | 164 | 50 cycles, 93.2% | |
| LNO@NCM712/ Li3.12P0.94Bi0.06S3.91O0.09I/Li | Bi, O co-doped Li3PS4 | 0.1C | 106.1 | 50 cycles, 83.2% | ||
| LNO@NCM622/oxysulfide-coated LPSC/Li-In | Oxysulfide layer on LPSC | 0.1 | 125.6 | 200 cycles, 64.77% | ||
| LFP/PVDF-HFP-Li7PS6 CSE/Li | PVDF-HFP-Li7PS6 CSE | 0.2C | 160 | 150 cycles, 98% | ||
| A/E | S/LGPS/Li0.8Al | Li-Al alloy anode | 0.36 | 1237 | 200 cycles, 93.29% | |
| LZO@LiNi0.9Co0.05Mn0.05O2/LPSC/Ag-C pouch cell | Ag-C anode | 3.4 | 146 | 1000 cycles, 89% | ||
| NCM811/LPSC/μ-Si | μ-Si anode | 5.0 | > 1250 | 500 cycles, 80% | ||
| Cl@S-NCM811/LPSC-CLA/Li | CuF2, LiNO3 additives in LPSC | 2.55 | 150 | 100 cycles, 69.4% | ||
| S/LGPS/LiI-Li | LiI layer on Li metal | 0.2 | 1360 | 150 cycles, 80.6% | ||
| LNO@LCO/LPSCl0.3F0.7 | F doping LPSC electrolyte | 0.13 | 115 | 50 cycles, 95% | ||
| NCM811/LPSC-LGPS-LPSC/Graphite-Li | LPSC-LGPS-LPSC multilayer electrolyte | 8.6 | 100 | 10000 cycles, 82% | ||
| LNO@LCO/PEGDME-LPSC/Li | PEGDME-LPSC CSE | 0.5 | 88 | 650 cycles 80% |
Table 1
Fig 9
(a) Schematic illustration of fabricating thin Li10GeP2S12 electrolyte membrane with nylon mesh support by slurry-casting technique; (b) comparison of cycling performance of all-solid-state batteries with and without gel polymer interlayer 139; (c) schematics of fabricating Fe7S8@C/LPSB composite electrodes by infiltration method; (d) rate performance of all-solid-state batteries using infiltration Fe7S8 as the cathode material 141. (a, b) Adapted with permission from Ref. 139, Copyright 2022, Elsevier Inc.; (c, d) Adapted with permission from Ref. 141, Copyright 2022, Wiley-VCH."
Fig 9
Fig 10
(a) Schematic illustration of the ultrathin Li5.4PS4.4Cl1.6 membrane fabrication 155; (b) illustrations of the morphological changes experienced by composite cathodes prepared with PTFE and with the ionomer before and after cycling; (c) cycling performance of all-solid-state batteries using composite cathode prepared without binder, with PTFE and with ionomer 156. (a) Adapted with permission from Ref. 155, Copyright 2021, American Chemical Society; (b, c) Adapted with permission from Ref. 156, Copyright 2022, American Chemical Society."
Fig 10
Fig 11
(a) Schematic illustration of liquid battery and solid battery interface contact; (b) schematic illustration of isostatic pressing 161. (b) Adapted with permission from Ref. 161, Copyright 2022, Elsevier Inc."
Fig 11
Fig 12
Illustration of influence of cathode active material load on the energy density of all-solid state battery."
Fig 12
Fig 13
Schematic illustration of the framework of this review."
Fig 13
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