阳极氧化物纳米孔道和TiO2纳米管形成机理的研究进展

doi:10.3866/PKU.WHXB201204093

Abstract

Abstract: Self-ordered porous anodic TiO₂ nanotubes and other porous anodic oxides (PAO) have received considerable attention because of their potential for high technological application in a number of fields. The anodization of valve metals has been widely investigated over the last eight decades. The formation mechanisms of hexagonal cells and nanotubes, however, have remained unclear until now. Simply reviewing the mechanisms of PAO formation was not the aim of this research and we were more interested in reviewing the forming processes of compact anodic oxides (CAO) and investigating the relationship between the PAO and CAO, to better understand the pore generating mechanisms. The present work introduces the differences between PAO and CAO films, as well as reviewing the traditional theories of PAO films and their deficiencies. Recent progress in the formation mechanism of PAO, including the viscous flow, breakdown, equifield strength, and oxygen bubbles models has been reviewed in detail. The perspective on future developments for the PAO forming mechanism has been tentatively discussed. Based on sufficient analysis of the latest findings, it has been proposed that several approaches may be employed for investigating the pore forming and self-ordering mechanisms. These new approaches include ultrasound-assisted anodizing, anodizing under vacuum or high pressure and adding sodium carbonate or a reducing agent to the PAO-forming electrolytes. An investigation of changes in the current and anodizing efficiencies would also be an effective approach for better understanding the physical nature of fieldassisted dissolution (FAD).

Key words: Compact anodic oxide, Porous anodic oxide, Formation mechanism, Anodization, Self-ordering

ZHU Xu-Fei, HAN Hua, SONG Ye, DUAN Wen-Qiang. Research Progress in Formation Mechanism of TiO₂ Nanotubes and Nanopores in Porous Anodic Oxide[J]. Acta Phys. -Chim. Sin. 2012, 28(06), 1291-1305. doi: 10.3866/PKU.WHXB201204093

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Research Progress in Formation Mechanism of TiO₂ Nanotubes and Nanopores in Porous Anodic Oxide

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Research Progress in Formation Mechanism of TiO₂ Nanotubes and Nanopores in Porous Anodic Oxide